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Information card for entry 4318999
Preview
| Coordinates | 4318999.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C72 H60 Ag2 As4 N2 O4 |
|---|---|
| Calculated formula | C72 H60 Ag2 As4 N2 O4 |
| Title of publication | Variable Coordination Modes of NO2- in a Series of Ag(I) Complexes Containing Triorganophosphines, -arsines, and -stibines. Syntheses, Spectroscopic Characterization (IR, 1H and 31P NMR, Electrospray Ionization Mass), and Structures of [AgNO2(R3E)x] Adducts (E = P, As, Sb, x = 1-3) |
| Authors of publication | Augusto Cingolani; Effendy; Maura Pellei; Claudio Pettinari; Carlo Santini; Brian W. Skelton; Allan H. White |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2002 |
| Journal volume | 41 |
| Pages of publication | 6633 - 6645 |
| a | 18.5301 ± 0.0007 Å |
| b | 14.084 ± 0.0005 Å |
| c | 14.1379 ± 0.0005 Å |
| α | 61.087 ± 0.001° |
| β | 79.547 ± 0.001° |
| γ | 77.195 ± 0.001° |
| Cell volume | 3137.5 ± 0.2 Å3 |
| Cell temperature | 150 K |
| Ambient diffraction temperature | 150 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.063 |
| Residual factor for significantly intense reflections | 0.03 |
| Weighted residual factors for all reflections | 0.026 |
| Weighted residual factors for all reflections included in the refinement | 0.023 |
| Goodness-of-fit parameter for all reflections | 0.961 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.089 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176432 (current) | 2016-02-14 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries. |
4318999.cif |
| 120093 | 2014-07-12 | Adding DOIs to range 4/31 structures. | 4318999.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4318999.cif |
| 15727 | 2011-03-17 | ../uploads/cif-deposit/cod/cif Adding structures of 4318999 via cif-deposit CGI script. |
4318999.cif |
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Users of the data should acknowledge the original authors of the
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