Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4320180
Preview
| Coordinates | 4320180.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | As2 Cs6.25 Mn2.37 O81.5 W18.63 |
|---|---|
| Calculated formula | As2 Cs6.25 Mn2.38 Na O81.5 W18.62 |
| Title of publication | Synthesis and Characterization of Copper-, Zinc-, Manganese-, and Cobalt-Substituted Dimeric Heteropolyanions, [(α-XW~9~O~33~)~2~M~3~(H~2~O)~3~]^n-^ (n = 12, X = As^III^, Sb^III^, M = Cu^2+^, Zn^2+^; n = 10, X = Se^IV^, Te^IV^, M = Cu^2+^) and [(α-AsW~9~O~33~)~2~WO(H~2~O)M~2~(H~2~O)~2~]^10-^ (M = Zn^2+^, Mn^2+^, Co^2+^) |
| Authors of publication | Ulrich Kortz; Noha K. Al-Kassem; Masha G. Savelieff; Nisrine A. Al Kadi; Masahiro Sadakane |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2001 |
| Journal volume | 40 |
| Pages of publication | 4742 - 4749 |
| a | 12.5139 ± 0.0011 Å |
| b | 19.1754 ± 0.0017 Å |
| c | 17.2199 ± 0.0016 Å |
| α | 90° |
| β | 95.838 ± 0.002° |
| γ | 90° |
| Cell volume | 4110.6 ± 0.6 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 5 |
| Space group number | 11 |
| Hermann-Mauguin space group symbol | P 1 21/m 1 |
| Hall space group symbol | -P 2yb |
| Residual factor for all reflections | 0.1174 |
| Residual factor for significantly intense reflections | 0.1054 |
| Weighted residual factors for significantly intense reflections | 0.238 |
| Weighted residual factors for all reflections included in the refinement | 0.2447 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.269 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 176467 (current) | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4320180.cif |
| 120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4320180.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4320180.cif |
| 17079 | 2011-04-01 | ../uploads/cif-deposit/cod/cif Adding structures of 4320180 via cif-deposit CGI script. |
4320180.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.