Crystallography Open Database

Information card for entry 4320352

4320351 << 4320352 >> 4320353

Preview

Coordinates	4320352.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C26 H88.5 N8 O2.25 Re8 S40 Se8
Calculated formula	C26 H84 N8 O2.25 Re8 S40 Se8
Title of publication	The Mixed Polychalcogenorhenate(IV) Anions [Re4Q4(S3)4(S4)2]4- (Q = Se, Te): Syntheses and Crystal Structures of [NMe4]5[Me2NH2]3[Re4Se4(S3)4(S4)2]2.2.25H2O and [NH4]4[Re4Te4(S3)4(S4)2].8H2O
Authors of publication	Yuri V. Mironov; Michael A. Pell; Thomas E. Albrecht-Schmitt; James A. Ibers
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	5472 - 5474
a	12.5552 ± 0.0012 Å
b	38.397 ± 0.004 Å
c	19.4653 ± 0.0019 Å
α	90°
β	93.135 ± 0.002°
γ	90°
Cell volume	9369.8 ± 1.6 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1414
Residual factor for significantly intense reflections	0.056
Weighted residual factors for significantly intense reflections	0.0976
Weighted residual factors for all reflections included in the refinement	0.1228
Goodness-of-fit parameter for all reflections included in the refinement	1.102
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179306 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/03.	4320352.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320352.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320352.cif
17256	2011-04-06	../uploads/cif-deposit/cod/cif Adding structures of 4320352 via cif-deposit CGI script.	4320352.cif