Crystallography Open Database

Information card for entry 4320373

4320372 << 4320373 >> 4320374

Preview

Coordinates	4320373.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C52 H118 Cl0 K N8 O9 Si4 U2
Calculated formula	C52 H100 K N8 O9 Si4 U2
Title of publication	Reaction of the Uranyl(VI) Ion (UO22+) with a Triamidoamine Ligand: Preparation and Structural Characterization of a Mixed-Valent Uranium(V/VI) Oxo-Imido Dimer
Authors of publication	Paul B. Duval; Carol J. Burns; Wayne E. Buschmann; David L. Clark; David E. Morris; Brian L. Scott
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	5491 - 5496
a	12.1144 ± 0.0006 Å
b	12.6084 ± 0.0006 Å
c	14.5072 ± 0.0007 Å
α	101.374 ± 0.001°
β	103.757 ± 0.001°
γ	109.34 ± 0.001°
Cell volume	1936.6 ± 0.16 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0524
Residual factor for significantly intense reflections	0.0446
Weighted residual factors for significantly intense reflections	0.1315
Weighted residual factors for all reflections included in the refinement	0.1366
Goodness-of-fit parameter for all reflections included in the refinement	1.303
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179306 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/03.	4320373.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320373.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320373.cif
17281	2011-04-06	../uploads/cif-deposit/cod/cif Adding structures of 4320373 via cif-deposit CGI script.	4320373.cif