Crystallography Open Database

Information card for entry 4320477

4320476 << 4320477 >> 4320478

Preview

Coordinates	4320477.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	COopp2epz(2)
Formula	C19 H21 Cl2 Co N2 O2 P
Calculated formula	C19 H21 Cl2 Co N2 O2 P
Title of publication	Tethered Pyrazolyl Phosphinate: Pyrazolyl-N- and Phosphoryl-O-Metal Coordination in Ph2P(O){OCH2CH2(3,5-Me2Pz)}
Authors of publication	Savariraj Kingsley; Vadapalli Chandrasekhar; Christopher D. Incarvito; Matthew K. Lam; Arnold L. Rheingold
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	5890 - 5896
a	9.751 ± 0.006 Å
b	18.126 ± 0.002 Å
c	11.946 ± 0.003 Å
α	90°
β	95.31 ± 0.03°
γ	90°
Cell volume	2102.4 ± 1.4 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1813
Residual factor for significantly intense reflections	0.0542
Weighted residual factors for significantly intense reflections	0.1027
Weighted residual factors for all reflections included in the refinement	0.141
Goodness-of-fit parameter for all reflections included in the refinement	0.988
Diffraction radiation wavelength	0.71069 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179307 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/04.	4320477.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320477.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320477.cif
17673	2011-04-09	../uploads/cif-deposit/cod/cif Adding structures of 4320477 via cif-deposit CGI script.	4320477.cif