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Information card for entry 4320632
Preview
| Coordinates | 4320632.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Chemical name | Tetraphenylarsonium trans-bis(heptacyanomolybdenum(IV) -u-oxo-)bis(ethylenediammine)Osmate(VI) |
|---|---|
| Formula | C118 H108 As4 Mo2 N18 O11 Os |
| Calculated formula | C118 H106.5 As4 Mo2 N18 O10.5 Os |
| Title of publication | Reaction of [Os(en)2O2]2+ with Photolyzed [Mo(CN)8]4- in Water |
| Authors of publication | R. Kent Murmann; Charles L. Barnes |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2001 |
| Journal volume | 40 |
| Pages of publication | 6514 - 6517 |
| a | 10.978 ± 0.005 Å |
| b | 13.17 ± 0.005 Å |
| c | 40.322 ± 0.017 Å |
| α | 93.501 ± 0.007° |
| β | 95.994 ± 0.007° |
| γ | 95.638 ± 0.008° |
| Cell volume | 5755 ± 4 Å3 |
| Cell temperature | 173 ± 2 K |
| Ambient diffraction temperature | 173 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0759 |
| Residual factor for significantly intense reflections | 0.0639 |
| Weighted residual factors for significantly intense reflections | 0.1214 |
| Weighted residual factors for all reflections included in the refinement | 0.1265 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.262 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 192777 (current) | 2017-03-02 | cod/ Correcting misspelt data item names by using the 'cod_correct_tags' script and the replacement file 'data/replacement-values/replacement_tags.lst' from the 'cod-tools' repository (rev. 5000). The correction was mainly focused on removing misspelt versions of the '_symmetry_Int_Tables' and '_space_group_IT_number' data items. |
4320632.cif |
| 179309 | 2016-03-23 | cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/06. |
4320632.cif |
| 120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4320632.cif |
| 34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4320632.cif |
| 17828 | 2011-04-10 | ../uploads/cif-deposit/cod/cif Adding structures of 4320632 via cif-deposit CGI script. |
4320632.cif |
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Users of the data should acknowledge the original authors of the
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