Crystallography Open Database

Information card for entry 4320653

4320652 << 4320653 >> 4320654

Preview

Coordinates	4320653.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	bis{1,5-dimethyl-3(6-methyl-2-pyridn-2-yl)-6-oxo-verdazyl}copper(I) hexafluorophosphate
Formula	C20 H24 Cu F6 N10 O2 P
Calculated formula	C20 H24 Cu F6 N10 O2 P
Title of publication	Weak Magnetic Coupling of Coordinated Verdazyl Radicals through Diamagnetic Metal Ions. Synthesis, Structure, and Magnetism of a Homoleptic Copper(I) Complex
Authors of publication	Tosha M. Barclay; Robin G. Hicks; Martin T. Lemaire; Laurence K. Thompson
Journal of publication	Inorganic Chemistry
Year of publication	2001
Journal volume	40
Pages of publication	6521 - 6524
a	27.269 ± 0.003 Å
b	27.269 ± 0.003 Å
c	15.498 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	11524 ± 2 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	7
Space group number	142
Hermann-Mauguin space group symbol	I 41/a c d :2
Hall space group symbol	-I 4bd 2c
Residual factor for all reflections	0.1007
Residual factor for significantly intense reflections	0.0541
Weighted residual factors for significantly intense reflections	0.1516
Weighted residual factors for all reflections included in the refinement	0.1864
Goodness-of-fit parameter for all reflections included in the refinement	1.034
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179309 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/06.	4320653.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4320653.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4320653.cif
17849	2011-04-10	../uploads/cif-deposit/cod/cif Adding structures of 4320653 via cif-deposit CGI script.	4320653.cif