Crystallography Open Database

Information card for entry 4321128

Preview

Coordinates	4321128.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H34 N7 P3
Calculated formula	C16 H34 N7 P3
Title of publication	Syntheses and Structures of Heterobicyclic Bis(tert-butylamido)cyclodiphosph(III)azane Compounds Having Phosphorus(III) and Arsenic(III) Centers
Authors of publication	Ingo Schranz; Luke P. Grocholl; Lothar Stahl; Richard J. Staples; Alison Johnson
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	3037 - 3041
a	9.496 ± 0.007 Å
b	12.455 ± 0.007 Å
c	10.043 ± 0.006 Å
α	90°
β	97.23 ± 0.04°
γ	90°
Cell volume	1178.4 ± 1.3 Å³
Cell temperature	213 ± 2 K
Ambient diffraction temperature	213 ± 2 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.081
Residual factor for significantly intense reflections	0.0499
Weighted residual factors for significantly intense reflections	0.1073
Weighted residual factors for all reflections included in the refinement	0.1216
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179314 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/11.	4321128.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321128.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321128.cif
18476	2011-04-30	../uploads/cif-deposit/cod/cif Adding structures of 4321128 via cif-deposit CGI script.	4321128.cif