Crystallography Open Database

Information card for entry 4321891

Preview

Coordinates	4321891.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H54 Bi Li N6 Te2
Calculated formula	C24 H54 Bi1.036 N6 Te2
Title of publication	Homoleptic Bismuth and Antimony Complexes of the Tripodal [Te(NtBu)3]2- Anion
Authors of publication	Tristram Chivers; Masood Parvez; Gabriele Schatte; Glenn P. A. Yap
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	1380 - 1381
a	9.833 ± 0.004 Å
b	34.665 ± 0.009 Å
c	10.099 ± 0.004 Å
α	90°
β	103.497 ± 0.005°
γ	90°
Cell volume	3347 ± 2 Å³
Cell temperature	203 ± 2 K
Ambient diffraction temperature	203 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.0848
Residual factor for significantly intense reflections	0.046
Weighted residual factors for significantly intense reflections	0.0844
Weighted residual factors for all reflections included in the refinement	0.0902
Goodness-of-fit parameter for all reflections included in the refinement	0.908
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179321 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/18.	4321891.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321891.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321891.cif
19733	2011-05-25	../uploads/cif-deposit/cod/cif Adding structures of 4321891 via cif-deposit CGI script.	4321891.cif