#------------------------------------------------------------------------------ #$Date: 2012-02-24 10:01:01 +0200 (Fri, 24 Feb 2012) $ #$Revision: 34320 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/32/18/4321893.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4321893 loop_ _publ_author_name 'Peter Comba' 'Sergey P. Gavrish' 'Robert W. Hay' 'Peter Hilfenhaus' 'Yaroslaw D. Lampeka' 'Philip Lightfoot' 'Alexander Peters' _publ_section_title ; Structural Variation of Dinuclear Transition Metal Compounds with a Common Type of Ligand: Solid State and Solution Structures and Model Studies ; _journal_name_full 'Inorganic Chemistry' _journal_volume 38 _journal_page_first 1416 _journal_page_last 1421 _journal_year 1999 _chemical_formula_sum 'C18 H42 N8 Ni2 O10' _chemical_formula_weight 647.98 _space_group_IT_number 15 _symmetry_cell_setting monoclinic _symmetry_Int_Tables_number 15 _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90 _cell_angle_beta 112.52(3) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 23.505(7) _cell_length_b 8.118(7) _cell_length_c 15.578(7) _cell_volume 2746(3) #------------------------------------------------------------------------------ loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_sigma _refln_F_calc _refln_observed_status 1 1 0 274.32 0.97 267.38 o 2 0 -2 186.97 0.35 195.11 o 0 0 2 127.05 0.34 127.62 o 1 1 -1 16.35 0.40 10.01 o 1 1 1 106.70 0.36 101.63 o 1 1 -2 12.51 0.41 15.37 o 3 1 -1 54.76 0.38 54.24 o 4 0 -2 333.88 1.18 343.82 o 4 0 0 116.70 0.39 113.41 o 3 1 0 13.64 0.35 12.99 o 2 0 2 264.19 0.42 263.16 o 3 1 -2 174.47 0.41 178.62 o 1 1 2 141.20 0.41 138.10 o 3 1 1 71.79 0.43 69.48 o 1 1 -3 193.46 0.45 201.43 o 3 1 -3 201.75 0.47 199.47 o 0 2 0 30.33 0.49 25.54 o 5 1 -1 94.23 0.45 90.51 o 5 1 -2 37.51 0.48 34.39 o 0 2 1 83.07 0.47 87.34 o 2 0 -4 415.63 1.36 444.29 o 6 0 -2 26.57 0.52 21.77 o 1 1 3 50.36 0.48 48.92 o 5 1 0 14.27 0.45 11.81 o 3 1 2 64.57 0.47 59.80 o 2 2 -1 93.26 0.47 86.92 o 2 2 0 24.00 0.53 25.98 o 4 0 -4 369.15 1.43 367.69 o 4 0 2 49.37 0.49 47.63 o 5 1 -3 40.43 0.51 38.52 o 6 0 0 61.31 0.48 56.62 o 0 0 4 7.68 0.43 4.51 o 2 2 -2 80.72 0.49 82.54 o 2 2 1 50.46 0.50 49.33 o 0 2 2 54.11 0.50 57.00 o 3 1 -4 326.88 1.48 334.76 o 1 1 -4 133.26 0.50 141.00 o 5 1 1 74.45 0.50 71.99 o 4 2 -1 28.02 0.53 24.47 o 4 2 -2 18.12 0.43 16.35 o 4 2 0 72.95 0.51 69.06 o 6 0 -4 178.36 0.53 184.69 o 5 1 -4 96.21 0.54 86.06 o 2 2 -3 58.60 0.54 62.57 o 2 2 2 125.48 0.52 121.55 o 3 1 3 64.99 0.52 63.97 o 0 2 3 171.72 0.52 169.62 o 7 1 -2 15.67 0.48 17.71 o 1 1 4 30.72 0.57 34.25 o 2 0 4 56.92 0.53 57.74 o 7 1 -1 85.45 0.52 86.31 o 4 2 -3 25.40 0.59 31.82 o 4 2 1 113.85 0.53 112.97 o 7 1 -3 39.99 0.55 38.76 o 5 1 2 9.74 0.44 8.91 o 8 0 -2 98.83 0.54 99.18 o 3 1 -5 135.07 0.55 129.97 o 7 1 0 150.20 0.54 151.67 o 6 0 2 33.65 0.58 32.30 o 1 1 -5 43.85 0.58 41.90 o 2 2 -4 78.16 0.57 77.52 o 6 2 -2 103.02 0.55 100.52 o 6 2 -1 62.89 0.55 60.71 o 2 2 3 196.75 0.55 190.37 o 5 1 -5 7.00 0.74 2.92 o 7 1 -4 79.07 0.57 83.08 o 4 2 -4 127.98 0.58 125.80 o 4 2 2 94.71 0.56 91.07 o 8 0 -4 157.94 0.58 155.70 o 8 0 0 235.16 0.56 238.10 o 6 2 -3 203.21 0.56 202.34 o 6 2 0 106.19 0.56 104.33 o 0 2 4 113.31 0.56 108.90 o 1 3 0 82.05 0.56 82.99 o 3 1 4 202.26 0.57 198.30 o 1 3 -1 74.13 0.57 77.31 o 7 1 1 75.87 0.56 76.25 o 1 3 1 26.33 0.62 24.41 o 5 1 3 24.46 0.62 23.93 o 4 0 -6 184.63 0.58 188.30 o 1 1 5 31.49 0.61 33.21 o 4 0 4 225.06 0.58 220.20 o 1 3 -2 61.76 0.59 58.16 o 2 0 -6 17.17 0.51 18.02 o 3 3 -1 121.00 0.58 115.69 o 7 1 -5 95.42 0.60 90.71 o 6 2 -4 59.05 0.60 59.59 o 6 2 1 27.06 0.64 27.48 o 3 3 -2 43.37 0.62 42.34 o 6 0 -6 223.80 0.61 228.42 o 9 1 -2 46.41 0.60 46.89 o 1 3 2 65.20 0.59 62.24 o 3 1 -6 20.08 0.55 16.56 o 9 1 -3 71.98 0.59 72.78 o 2 2 -5 33.87 0.65 35.10 o 2 2 4 22.02 0.72 22.42 o 4 2 -5 148.36 0.61 152.61 o 4 2 3 36.46 0.63 37.47 o 3 3 1 86.33 0.60 84.80 o 5 1 -6 188.21 0.61 193.13 o 9 1 -1 58.97 0.60 57.94 o 7 1 2 81.06 0.60 77.77 o 0 0 6 114.14 0.59 111.81 o 1 3 -3 106.33 0.59 108.01 o 9 1 -4 46.85 0.63 46.59 o 1 1 -6 113.62 0.60 119.05 o 8 2 -2 63.44 0.60 60.39 o 3 3 -3 80.97 0.60 83.80 o 8 2 -3 18.10 0.55 17.63 o 0 2 5 15.92 0.47 11.53 o 8 2 -1 118.01 0.60 120.40 o 5 3 -1 112.51 0.60 108.71 o 10 0 -2 217.40 0.61 220.00 o 5 3 -2 174.18 0.60 173.21 o 6 2 -5 57.92 0.66 57.42 o 6 2 2 64.67 0.62 62.82 o 9 1 0 40.51 0.63 41.54 o 1 3 3 159.19 0.61 157.97 o 5 3 0 77.18 0.61 69.45 o 3 3 2 128.30 0.61 125.57 o 7 1 -6 160.55 0.64 158.05 o 10 0 -4 86.29 0.63 85.30 o 3 1 5 30.24 0.70 26.39 o 8 0 -6 67.85 0.65 65.38 o 8 0 2 246.80 0.62 240.57 o 5 1 4 88.79 0.62 85.90 o 8 2 -4 29.27 0.71 34.12 o 5 3 -3 166.11 0.61 166.26 o 8 2 0 72.06 0.62 73.16 o 3 3 -4 38.78 0.67 35.88 o 1 1 6 45.00 0.64 41.63 o 1 3 -4 8.47 0.67 5.26 o 5 3 1 8.17 0.65 9.21 o 4 2 -6 117.84 0.65 120.57 o 4 2 4 104.10 0.63 104.39 o 2 0 6 142.34 0.63 144.25 o 10 0 0 152.01 0.62 150.81 o 6 0 4 247.85 0.64 246.91 o 2 2 -6 35.87 0.71 35.38 o 9 1 1 11.40 0.53 13.17 o 7 1 3 7.74 0.68 9.44 o 2 2 5 40.59 0.67 36.26 o 5 3 -4 51.13 0.65 49.06 o 5 1 -7 88.10 0.66 84.76 o 8 2 -5 18.61 0.61 21.76 o 3 1 -7 131.83 0.64 132.80 o 8 2 1 14.03 0.48 9.73 o 3 3 3 44.96 0.68 43.86 o 6 2 -6 78.97 0.67 82.10 o 6 2 3 122.48 0.64 116.90 o 7 3 -2 47.11 0.66 45.86 o 1 3 4 56.69 0.65 56.40 o 7 3 -1 48.44 0.65 51.04 o 9 1 -6 28.95 0.76 27.54 o 7 3 -3 139.16 0.64 134.19 o 5 3 2 10.32 0.58 8.41 o 0 2 6 80.10 0.65 79.63 o 7 1 -7 20.65 0.61 15.30 o 1 1 -7 36.04 0.73 33.77 o 11 1 -2 89.54 0.65 91.83 o 10 0 -6 24.47 0.80 30.97 o 3 3 -5 109.79 0.68 115.67 o 7 3 0 68.92 0.66 69.87 o 11 1 -4 109.06 0.66 107.00 o 10 2 -3 67.26 0.66 67.85 o 0 4 0 10.31 0.62 2.79 o 10 2 -2 95.28 0.65 97.53 o 1 3 -5 20.60 0.59 15.55 o 0 4 1 159.98 0.66 158.93 o 5 3 -5 85.96 0.68 87.54 o 7 3 -4 13.09 0.50 6.17 o 11 1 -1 92.09 0.65 87.55 o 5 1 5 19.72 0.64 22.50 o 9 1 2 198.11 0.66 190.48 o 2 4 0 47.71 0.70 44.29 o 2 4 -1 199.80 0.66 194.75 o 10 2 -4 11.59 0.53 11.74 o 3 1 6 9.89 0.66 17.76 o 8 2 -6 67.42 0.69 63.39 o 10 2 -1 127.33 0.66 130.01 o 8 2 2 109.25 0.66 110.04 o 11 1 -5 56.32 0.69 56.44 o 2 4 -2 15.92 0.50 12.22 o 2 4 1 202.03 0.67 194.75 o 0 4 2 66.61 0.69 66.75 o 3 3 4 19.28 0.58 16.98 o 4 2 -7 30.56 0.78 30.69 o 7 3 1 39.47 0.69 42.22 o 4 0 -8 63.33 0.68 69.66 o 4 2 5 50.55 0.71 51.75 o 7 1 4 55.98 0.69 50.71 o 12 0 -4 22.69 0.62 25.22 o 12 0 -2 209.76 0.67 210.32 o 4 0 6 28.21 0.74 27.37 o 6 0 -8 50.06 0.70 49.91 o 9 1 -7 37.94 0.76 38.87 o 5 3 3 42.43 0.72 46.52 o 6 2 -7 12.96 0.56 2.36 o 10 2 -5 36.49 0.72 38.05 o 2 2 -7 143.18 0.68 151.88 o 1 3 5 35.63 0.72 34.96 o 4 4 -1 109.94 0.68 104.66 o 11 1 0 138.16 0.67 139.01 o 2 2 6 34.42 0.73 34.31 o 10 2 0 48.88 0.69 50.16 o 6 2 4 22.27 0.58 20.84 o 7 3 -5 39.74 0.71 34.41 o 4 4 -2 60.41 0.70 57.37 o 4 4 0 77.94 0.70 74.59 o 2 0 -8 54.15 0.70 60.32 o 5 1 -8 161.20 0.69 166.08 o 2 4 -3 121.65 0.68 118.01 o 2 4 2 7.61 0.89 1.59 o 10 0 2 251.61 0.68 245.55 o 9 3 -2 30.26 0.76 32.68 o 11 1 -6 100.04 0.70 101.85 o 3 1 -8 115.07 0.69 119.37 o 3 3 -6 34.02 0.81 31.47 o 9 3 -3 55.79 0.70 56.37 o 0 4 3 173.77 0.68 169.61 o 8 0 -8 10.87 0.66 6.58 o 5 3 -6 7.29 0.93 9.45 o 4 4 -3 81.48 0.69 81.20 o 7 1 -8 83.67 0.71 85.32 o 9 3 -1 60.28 0.70 64.91 o 4 4 1 167.75 0.69 167.57 o 8 0 4 42.27 0.75 37.91 o 7 3 2 9.21 0.69 9.20 o 8 2 -7 68.77 0.72 74.47 o 9 1 3 35.38 0.75 34.76 o 0 2 7 47.92 0.72 46.91 o 9 3 -4 40.50 0.71 35.84 o 8 2 3 142.35 0.69 141.69 o 10 2 -6 11.13 0.61 9.17 o 10 2 1 69.89 0.70 68.84 o 12 0 -6 74.32 0.72 77.14 o 12 0 0 229.37 0.69 224.65 o 1 1 -8 31.02 0.81 26.38 o 9 3 0 19.30 0.59 17.76 o 2 4 -4 38.07 0.75 41.73 o 0 0 8 91.41 0.70 86.97 o 6 4 -1 28.84 0.82 27.80 o 6 4 -2 58.24 0.73 51.53 o 2 4 3 120.05 0.70 117.60 o 7 3 -6 72.73 0.73 71.61 o 3 3 5 25.08 0.80 27.50 o 4 4 -4 14.26 0.55 10.05 o 4 4 2 42.72 0.73 37.61 o 5 1 6 168.71 0.71 160.34 o 5 3 4 72.10 0.72 73.32 o 6 4 -3 171.88 0.70 171.52 o 9 3 -5 26.55 0.83 30.04 o 6 4 0 53.00 0.73 53.28 o 9 1 -8 75.05 0.74 77.33 o 11 1 -7 64.34 0.73 59.55 o 0 4 4 28.83 0.82 28.04 o 12 2 -3 32.26 0.78 32.90 o 13 1 -3 54.91 0.73 56.53 o 3 1 7 90.93 0.71 92.74 o 13 1 -4 123.73 0.71 122.92 o 4 2 -8 79.79 0.73 82.82 o 10 0 -8 143.49 0.73 148.84 o 7 1 5 44.36 0.74 44.26 o 12 2 -4 70.51 0.72 70.17 o 12 2 -2 35.09 0.77 36.23 o 1 3 6 78.24 0.72 79.05 o 4 2 6 30.21 0.78 23.48 o 6 2 -8 91.77 0.74 90.83 o 13 1 -2 107.95 0.71 107.88 o 6 2 5 6.47 0.93 1.40 o 13 1 -5 119.06 0.72 114.88 o 7 3 3 69.12 0.72 65.74 o 9 3 1 67.41 0.72 71.15 o 6 4 -4 9.19 0.76 5.52 o 10 2 -7 75.95 0.75 74.41 o 6 0 6 211.46 0.72 202.40 o 6 4 1 54.53 0.74 54.06 o 2 2 -8 89.97 0.73 94.69 o 12 2 -5 75.72 0.74 74.61 o 2 2 7 13.91 0.48 11.64 o 5 3 -7 14.57 0.58 9.95 o 3 3 -7 178.14 0.73 181.77 o 10 2 2 49.45 0.75 48.20 o 11 1 2 29.41 0.79 31.71 o 1 1 8 110.54 0.72 110.34 o 13 1 -1 28.13 0.80 22.58 o 2 4 -5 41.61 0.77 44.38 o 2 4 4 42.22 0.77 38.42 o 4 4 -5 141.65 0.73 147.20 o 8 2 -8 33.62 0.86 31.78 o 5 1 -9 20.60 0.68 20.50 o 4 4 3 27.39 0.87 25.88 o 9 3 -6 64.63 0.76 62.23 o 8 2 4 37.54 0.82 31.11 o 9 1 4 73.44 0.73 66.72 o 11 3 -3 17.58 0.50 24.04 o 14 0 -4 173.24 0.74 176.18 o 7 1 -9 36.55 0.85 40.09 o 13 1 -6 92.67 0.74 90.30 o 2 0 8 127.42 0.73 123.76 o 7 3 -7 124.12 0.75 129.36 o 1 3 -7 76.97 0.75 81.43 o 8 4 -2 37.76 0.76 33.94 o 11 3 -2 84.83 0.73 80.62 o 3 1 -9 35.48 0.79 36.45 o 11 3 -4 8.67 0.83 11.99 o 8 4 -3 69.46 0.73 66.89 o 0 4 5 104.90 0.74 100.97 o 12 2 -6 85.24 0.75 86.24 o 8 4 -1 112.68 0.73 118.62 o 11 1 -8 68.45 0.77 73.51 o 12 2 0 69.47 0.74 71.39 o 6 4 -5 55.87 0.76 50.96 o 14 0 -2 45.89 0.79 51.97 o 6 4 2 13.16 0.57 9.44 o 0 2 8 10.52 0.66 9.23 o 11 3 -1 30.02 0.86 31.29 o 9 3 2 38.70 0.78 40.03 o 3 3 6 10.84 0.62 7.91 o 13 1 0 74.54 0.75 70.34 o 8 4 -4 12.18 0.60 13.49 o 8 4 0 15.63 0.53 15.73 o 11 3 -5 122.96 0.74 123.30 o 12 0 -8 8.81 0.74 4.89 o 9 1 -9 39.19 0.85 40.08 o 1 5 0 64.20 0.76 65.84 o 12 0 2 26.07 0.82 27.44 o 14 0 -6 92.82 0.76 87.90 o 1 5 -1 96.64 0.75 98.59 o 10 2 -8 39.68 0.83 43.42 o 1 1 -9 39.92 0.83 42.25 o 7 3 4 14.59 0.54 15.13 o 13 1 -7 12.41 0.65 12.97 o 10 0 4 120.08 0.75 117.77 o 1 5 1 10.15 0.70 7.56 o 10 2 3 8.57 0.88 13.41 o 9 3 -7 120.51 0.77 120.78 o 5 1 7 81.76 0.77 78.38 o 4 4 -6 51.08 0.82 47.39 o 1 3 7 8.90 0.75 3.50 o 4 4 4 18.82 0.56 17.80 o 11 3 0 42.54 0.80 42.71 o 2 4 -6 12.13 0.70 10.08 o 1 5 -2 22.68 0.68 21.88 o 3 5 -1 100.46 0.76 96.20 o 6 2 -9 37.62 0.85 36.48 o 7 1 6 133.08 0.75 135.17 o 11 1 3 48.77 0.79 47.01 o 2 4 5 99.08 0.76 98.92 o 12 2 -7 32.31 0.86 32.90 o 4 2 -9 16.32 0.54 14.84 o 6 2 6 64.68 0.77 64.87 o 4 2 7 29.81 0.83 29.62 o 5 3 -8 19.00 0.56 18.73 o 12 2 1 99.10 0.76 97.82 o 8 4 -5 35.89 0.81 38.07 o 3 1 8 50.89 0.80 48.88 o 3 5 -2 24.47 0.67 24.66 o 8 4 1 21.40 0.64 19.58 o 11 3 -6 12.05 0.67 5.80 o 1 5 2 26.09 0.61 26.09 o 3 3 -8 54.34 0.82 60.91 o 6 4 3 100.55 0.76 102.79 o 3 5 1 93.32 0.76 93.93 o 8 2 -9 9.56 0.92 9.40 o 6 0 -10 36.23 0.84 35.22 o 7 3 -8 24.44 0.71 21.11 o 8 2 5 56.01 0.79 48.54 o 14 0 0 94.68 0.76 97.71 o 2 2 -9 49.54 0.79 49.68 o 14 2 -4 115.26 0.76 115.62 o 14 2 -3 57.62 0.77 57.25 o 1 5 -3 104.03 0.78 102.97 o 2 2 8 23.61 0.65 26.90 o 9 1 5 39.40 0.84 38.07 o 9 3 3 86.02 0.77 84.27 o 4 0 -10 47.18 0.80 43.86 o 3 5 -3 57.53 0.78 54.48 o 4 0 8 108.61 0.77 113.87 o 8 0 -10 152.16 0.78 158.39 o 15 1 -4 137.38 0.77 140.32 o 10 4 -3 44.92 0.80 46.10 o 5 5 -1 16.42 0.55 16.61 o 10 4 -2 9.04 0.83 7.78 o 11 3 1 123.14 0.77 121.29 o 14 2 -5 15.74 0.57 15.74 o 15 1 -3 28.54 0.91 27.77 o 5 5 -2 36.40 0.86 36.79 o 8 0 6 142.64 0.77 145.21 o 13 1 -8 34.89 0.84 33.52 o 1 3 -8 11.60 0.70 9.51 o 5 1 -10 11.34 0.71 13.23 o 15 1 -5 37.61 0.84 36.49 o 7 1 -10 101.74 0.79 103.27 o 1 5 3 123.02 0.77 121.66 o 5 5 0 34.09 0.86 33.70 o 3 5 2 15.42 0.55 16.28 o 10 4 -4 8.53 0.78 4.14 o 8 4 -6 55.64 0.82 56.28 o 10 4 -1 55.64 0.79 57.02 o 5 3 6 29.05 0.88 29.11 o 8 4 2 46.36 0.84 43.86 o 15 1 -2 39.85 0.84 45.74 o 5 5 -3 46.69 0.81 48.61 o 12 2 -8 19.94 0.58 19.60 o 9 3 -8 12.47 0.75 15.49 o 11 3 -7 36.46 0.87 36.28 o 2 0 -10 75.45 0.79 83.26 o 13 3 -3 109.51 0.78 113.61 o 10 2 -9 25.56 0.71 23.43 o 3 1 -10 79.66 0.79 84.67 o 3 3 7 18.34 0.60 15.84 o 12 2 2 7.32 1.02 6.77 o 14 2 -6 41.41 0.86 42.33 o 4 4 -7 52.41 0.85 52.37 o 13 3 -4 26.43 0.65 26.31 o 15 1 -6 41.73 0.86 44.50 o 3 5 -4 45.33 0.84 43.96 o 4 4 5 111.73 0.78 109.85 o 7 3 5 70.17 0.80 68.88 o 14 2 -1 97.60 0.78 99.77 o 10 2 4 85.61 0.80 86.82 o 5 5 1 97.48 0.80 98.68 o 9 1 -10 130.65 0.81 136.10 o 10 0 -10 12.52 0.68 12.72 o 13 3 -2 37.40 0.83 39.80 o 0 2 9 23.08 0.66 20.38 o 6 4 -7 70.88 0.82 71.82 o 10 4 -5 41.04 0.84 42.22 o 2 4 -7 120.35 0.80 123.94 o 2 4 6 7.14 0.98 3.36 o 10 4 0 11.62 0.72 9.04 o 13 3 -5 27.98 0.88 30.44 o 13 1 2 59.60 0.79 59.46 o 11 1 4 86.32 0.79 86.75 o 5 5 -4 39.80 0.84 38.16 o 15 1 -1 47.48 0.83 47.92 o 16 0 -4 94.87 0.81 95.43 o 3 5 3 26.31 0.63 22.93 o 11 3 2 35.23 0.85 35.31 o 1 3 8 57.15 0.81 55.45 o 13 3 -1 42.05 0.86 47.83 o 1 5 4 46.18 0.84 45.75 o 7 5 -2 9.03 0.85 11.07 o 5 3 -9 86.00 0.83 85.88 o 7 5 -1 65.67 0.80 67.55 o 6 2 -10 43.59 0.86 44.49 o 14 2 -7 71.26 0.82 70.59 o 9 3 4 11.26 0.78 10.12 o 5 1 8 29.28 0.95 34.01 o 7 5 -3 80.50 0.80 83.84 o 1 1 -10 99.57 0.80 106.50 o 7 1 7 11.37 0.79 8.70 o 5 5 2 38.85 0.88 35.53 o 6 2 7 76.78 0.82 82.35 o 14 2 0 52.47 0.86 52.69 o 7 3 -9 70.28 0.83 71.29 o 13 3 -6 68.97 0.83 63.87 o 8 4 -7 56.19 0.86 62.60 o 0 4 7 46.48 0.85 46.46 o 4 2 -10 13.78 0.62 13.43 o 3 3 -9 13.28 0.67 9.83 o 8 4 3 99.37 0.80 96.87 o 16 0 -6 29.90 0.93 25.31 o 4 2 8 16.79 0.59 20.24 o 3 5 -5 102.88 0.79 103.72 o 0 0 10 49.53 0.85 51.74 o 7 5 0 53.85 0.85 53.33 o 8 2 -10 95.88 0.83 97.54 o 16 0 -2 72.30 0.81 75.63 o 10 4 1 167.79 0.80 165.58 o 11 1 -10 18.23 0.61 19.04 o 11 3 -8 38.23 0.91 35.47 o 8 2 6 55.07 0.82 55.33 o 1 5 -5 45.08 0.85 43.35 o 3 1 9 43.89 0.90 40.88 o 5 5 -5 127.63 0.80 130.93 o 12 2 -9 41.32 0.86 42.38 o 15 1 0 32.07 0.91 29.98 o 12 0 -10 50.48 0.87 50.17 o 13 3 0 49.86 0.85 48.03 o 12 2 3 94.20 0.81 91.62 o 12 0 4 78.26 0.82 86.26 o 9 3 -9 31.94 0.92 27.14 o 2 2 -10 45.66 0.88 50.40 o 6 0 8 18.37 0.59 20.98 o 12 4 -3 110.58 0.81 112.13 o 14 0 2 60.23 0.81 58.16 o 2 2 9 33.25 0.94 38.99 o 3 5 4 37.61 0.89 38.21 o 7 5 1 31.99 0.91 31.86 o 4 4 -8 17.26 0.64 17.76 o 15 1 -8 52.69 0.87 51.97 o 1 3 -9 49.93 0.86 51.81 o 12 4 -4 15.09 0.63 14.44 o 12 4 -2 27.99 0.70 25.58 o 13 3 -7 70.59 0.84 69.84 o 4 4 6 43.41 0.89 42.72 o 10 2 -10 75.39 0.86 76.04 o 14 2 -8 42.15 0.90 40.45 o 5 3 7 115.94 0.82 115.44 o 5 5 3 65.82 0.83 65.27 o 13 1 3 77.99 0.82 78.46 o 6 4 5 12.87 0.68 9.29 o 1 5 5 98.07 0.82 97.73 o 7 1 -11 24.98 0.75 24.11 o 10 2 5 89.65 0.82 93.70 o 7 3 6 19.42 0.63 20.55 o 11 3 3 77.93 0.84 76.85 o 5 1 -11 43.28 0.88 45.09 o 7 5 -5 32.34 0.92 32.02 o 10 4 -7 76.00 0.83 73.92 o 2 4 -8 12.44 0.72 15.43 o 12 4 -5 56.92 0.84 61.90 o 2 4 7 16.45 0.62 12.87 o 3 3 8 37.56 0.92 36.90 o 12 4 -1 40.07 0.90 43.13 o 16 2 -4 51.22 0.86 52.65 o 9 5 -2 15.53 0.57 12.59 o 11 1 5 39.04 0.92 35.95 o 9 5 -3 10.93 0.75 6.70 o 16 2 -5 53.83 0.88 61.28 o 9 1 -11 17.34 0.66 18.93 o 16 2 -3 23.93 0.74 25.20 o 8 4 -8 8.16 1.11 5.10 o 13 3 1 44.32 0.92 42.87 o 5 5 -6 19.76 0.58 23.97 o 10 0 6 21.99 0.60 20.31 o 9 5 -1 80.81 0.83 79.90 o 15 1 1 29.46 0.91 31.22 o 7 5 2 39.81 0.90 38.45 o 13 1 -10 57.77 0.88 58.39 o 16 0 -8 31.72 0.95 26.75 o 17 1 -4 23.54 0.75 22.38 o 9 3 5 93.02 0.84 89.15 o 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17.24 o 11 7 -12 36.16 0.93 31.65 o 17 7 -9 18.65 0.86 16.95 o 25 3 -11 13.03 1.20 13.51 o 27 1 -4 38.07 0.96 39.32 o 15 7 3 18.59 0.80 16.51 o 7 1 -18 15.33 0.99 19.23 o 23 5 -3 13.35 1.08 12.06 o 9 9 -2 34.30 0.98 34.91 o 6 0 -18 19.91 0.82 19.71 o 5 3 -17 13.81 1.10 18.51 o 20 2 6 52.62 1.27 53.81 o 3 9 -6 17.71 0.92 19.98 o 9 5 11 49.32 1.28 45.96 o 9 9 -3 21.68 0.82 20.88 o 22 2 4 33.37 1.00 35.78 o 2 2 -17 10.76 1.30 7.83 o 5 9 -6 22.90 0.81 23.12 o 13 7 5 15.73 1.01 18.42 o 27 1 -10 27.87 0.92 25.52 o 6 8 -10 12.27 1.10 9.51 o 15 3 -17 15.29 1.03 6.36 o 22 4 -13 25.76 0.78 26.78 o 7 5 12 20.00 0.89 17.90 o 21 3 -15 13.54 1.19 14.71 o 7 9 2 36.12 0.98 36.85 o 12 6 -14 19.66 0.90 19.85 o 14 8 0 29.50 0.85 29.87 o 20 6 -10 10.33 1.41 7.41 o 3 1 16 22.86 0.82 23.81 o 11 5 10 18.56 0.91 18.19 o 4 6 -14 21.50 0.81 19.12 o 4 8 -10 13.61 1.11 14.61 o 9 9 -4 36.51 0.94 38.85 o 1 9 -6 47.53 1.26 46.64 o 23 3 2 17.28 0.97 17.62 o 4 8 8 33.27 1.00 33.83 o 8 8 -10 34.58 1.00 32.14 o 18 2 -17 17.72 0.93 18.59 o 19 3 -16 15.39 1.04 13.71 o 20 6 0 30.89 0.79 29.92 o 16 6 -13 19.98 0.83 20.42 o 10 2 -18 12.21 1.16 6.43 o 12 6 8 18.64 0.91 17.66 o 19 7 -5 15.17 1.09 15.13 o 8 8 6 36.22 0.94 33.30 o 18 6 -12 24.02 0.82 21.45 o 22 0 -16 28.28 0.90 25.63 o 9 7 8 46.11 1.27 45.85 o 9 9 0 22.68 0.78 20.83 o 15 7 -11 22.25 0.84 17.16 o 12 2 -18 28.79 0.83 24.18 o 24 4 -11 20.97 0.86 23.59 o 5 7 10 35.95 0.99 34.56 o 17 7 1 27.60 0.85 27.56 o 19 7 -6 38.18 0.96 39.48 o 7 9 -6 36.14 1.00 38.12 o 24 2 -14 22.20 0.86 22.17 o 3 9 5 18.36 0.97 17.23 o 27 1 -3 13.25 1.10 14.27 o 25 1 1 16.57 0.96 16.35 o 10 2 13 29.87 0.99 30.04 o 5 5 13 40.84 1.28 36.67 o 5 9 4 47.83 1.27 47.41 o 8 2 -18 10.50 1.23 14.70 o 19 5 4 12.29 1.09 8.49 o 18 6 3 17.93 0.92 19.27 o 24 4 -1 13.05 1.24 12.33 o 2 4 15 29.59 0.84 24.78 o 9 3 13 17.51 0.89 17.32 o 9 9 -5 11.52 1.34 12.85 o 1 7 -12 24.69 0.77 25.80 o 5 1 -18 20.73 0.83 16.79 o 11 3 12 12.88 1.23 16.86 o 19 7 -3 39.91 0.95 41.22 o 2 8 -10 21.00 0.89 20.12 o 12 2 12 22.17 0.82 23.85 o 13 7 -12 37.21 0.99 36.71 o 13 5 9 37.82 1.01 35.65 o 16 0 10 44.81 1.28 46.06 o 1 9 6 39.60 1.28 37.89 o 24 2 2 16.50 0.93 14.65 o 10 8 -10 16.08 0.99 17.34 o 25 3 -12 15.43 1.05 14.36 o 4 0 -18 18.22 0.92 14.53 o 17 7 -10 30.23 0.89 33.08 o 28 0 -8 29.45 0.84 26.68 o 14 2 -18 20.77 0.92 23.73 o 22 6 -5 31.18 0.89 31.53 o 26 2 -12 23.91 0.84 23.11 o 28 0 -6 14.49 1.05 16.95 o 11 7 7 23.58 0.84 23.40 o 3 3 -17 30.66 0.87 27.42 o 4 0 16 45.11 1.42 44.04 o 3 7 11 10.20 1.24 8.08 o 13 3 11 12.32 1.19 11.00 o 1 5 -15 29.98 0.84 33.00 o 22 6 -7 26.10 0.79 25.20 o 3 9 -7 9.62 1.50 11.16 o 10 4 -17 37.65 0.99 32.36 o 21 1 6 32.97 1.00 33.62 o 22 6 -4 36.03 1.01 36.15 o 26 0 0 42.34 1.38 44.58 o 2 6 13 15.84 0.92 17.45 o 16 8 -4 23.37 0.82 21.81 o 19 7 -2 26.22 0.78 24.89 o 26 2 -1 27.21 0.90 31.50 o 6 2 -18 17.21 0.96 17.75 o 11 1 13 28.89 0.84 28.32 o 16 8 -5 11.24 1.23 10.63 o 19 5 -14 10.16 1.26 6.35 o 23 1 4 36.39 0.95 36.54 o 8 4 -17 22.90 0.82 18.29 o 20 4 -15 36.34 1.05 34.97 o 9 1 14 19.01 0.84 19.76 o 12 4 -17 19.60 0.90 21.61 o 6 2 15 10.70 1.29 8.89 o 9 7 -13 14.93 1.09 16.68 o 10 4 12 13.51 1.03 16.05 o 15 7 4 19.70 0.86 21.24 o 19 7 -8 19.71 0.92 20.82 o 21 3 5 38.79 0.97 40.60 o 23 5 -1 34.31 0.97 32.69 o 1 9 -7 11.28 1.43 11.00 o 22 6 -8 28.21 0.92 27.27 o 11 9 -2 37.51 1.02 39.46 o 13 1 12 43.08 1.30 43.25 o 17 5 -15 24.98 0.79 19.40 o 11 9 -4 21.41 0.80 20.24 o 16 8 -2 36.31 0.96 38.20 o 27 3 -7 38.94 1.03 40.56 o 20 4 5 37.73 0.99 38.41 o 18 0 -18 20.47 0.84 13.89 o 17 7 2 13.70 1.15 12.51 o 28 0 -10 23.94 0.81 22.93 o 27 3 -6 12.14 1.25 12.40 o 5 3 15 13.08 1.11 9.83 o 18 4 -16 11.18 1.30 10.40 o 22 2 -16 20.29 0.86 18.04 o 21 5 -13 31.70 0.87 27.67 o 25 3 0 13.69 1.16 15.79 o 27 3 -8 15.59 1.01 13.43 o 19 1 8 23.97 0.85 23.89 o 7 1 15 13.97 1.08 13.18 o 9 9 2 42.86 1.32 40.26 o 19 3 7 16.95 0.97 15.01 o 11 7 -13 16.72 0.96 17.14 o 23 5 -11 26.39 0.80 26.44 o 28 0 -4 29.53 0.85 30.15 o 13 7 6 31.42 0.80 28.53 o 26 4 -7 11.92 1.32 10.99 o 26 4 -6 10.50 1.27 11.33 o 1 7 12 46.10 1.35 46.81 o 14 4 -17 13.18 1.09 5.82 o 23 1 -16 13.67 1.08 14.42 o 11 9 -5 23.10 0.81 22.37 o 12 8 4 49.44 1.31 44.85 o 11 3 -18 13.76 1.26 14.58 o 6 8 8 12.38 1.09 12.21 o 14 8 2 34.77 1.00 37.76 o 15 7 -12 16.56 0.98 17.72 o 18 4 7 44.73 1.32 43.24 o 10 6 -15 13.78 1.09 9.15 o 22 2 5 42.60 1.37 41.78 o 27 3 -9 26.93 0.82 28.39 o 26 4 -5 13.58 1.14 13.85 o 16 2 10 34.90 0.99 35.54 o 28 2 -7 30.89 0.92 31.20 o 15 1 11 16.01 1.06 16.66 o 19 7 -9 15.66 0.93 13.91 o 25 3 -13 13.33 1.06 6.78 o 8 6 11 23.86 0.78 23.58 o 17 7 -11 14.99 1.16 17.09 o 4 2 -18 15.94 0.96 10.47 o 9 9 -7 13.64 1.16 14.66 o 28 2 -8 21.66 0.92 20.94 o 4 8 9 13.52 1.17 15.12 o 21 3 -16 19.74 0.94 17.79 o 22 6 -2 10.61 1.38 11.10 o 1 9 7 8.71 1.44 2.87 o 2 0 -18 24.48 0.83 29.33 o 11 9 0 23.35 0.84 23.30 o 10 6 10 25.79 0.85 27.57 o 16 6 -14 9.98 1.40 7.46 o 24 2 -15 22.18 0.87 16.27 o 18 6 4 36.57 0.98 37.00 o 4 2 16 9.73 1.34 11.33 o 26 0 -14 13.31 1.08 5.56 o 6 6 -15 28.66 0.84 26.56 o 5 9 -8 27.13 0.85 30.29 o 26 4 -9 18.04 1.02 19.76 o 6 6 12 26.59 0.78 23.90 o 26 2 0 30.55 0.89 31.55 o 12 6 -15 29.59 0.94 28.04 o 11 9 -6 32.73 1.06 32.36 o 3 9 -8 34.67 0.97 35.98 o 16 6 6 12.18 1.06 9.98 o 19 5 5 24.08 0.79 25.66 o 23 3 -15 18.93 0.89 10.40 o 5 1 16 26.02 0.86 26.04 o 28 2 -5 18.20 1.03 17.48 o 7 7 10 13.77 1.10 10.66 o 10 0 14 15.92 0.90 11.85 o 20 6 -12 23.89 0.82 22.24 o 24 2 3 16.59 1.09 21.79 o 27 3 -10 14.21 1.20 15.30 o 1 5 15 30.15 0.99 28.71 o 4 4 -17 28.76 0.90 30.13 o 19 1 -18 14.75 1.05 11.16 o 12 6 9 14.88 1.12 16.13 o 25 1 -15 15.73 1.00 14.94 o 16 8 -8 19.19 0.85 18.53 o 19 7 0 38.06 0.98 37.58 o 2 8 10 21.64 0.82 20.85 o 9 5 12 15.85 1.03 17.48 o 20 6 2 25.05 0.81 26.89 o 21 5 3 11.67 1.29 12.08 o 16 4 -17 19.16 0.91 15.10 o 17 3 9 17.63 0.88 16.41 o 0 10 0 25.90 0.85 27.60 o 18 2 -18 20.25 0.87 13.86 o 25 5 -5 20.14 0.88 18.73 o 4 6 -15 15.25 0.98 10.02 o 28 2 -10 16.17 1.10 15.42 o 1 9 -8 11.82 1.26 9.95 o 17 5 7 40.86 1.25 38.71 o 0 10 1 15.64 1.00 18.42 o 14 0 12 34.20 1.00 34.20 o 22 6 -1 18.89 0.86 18.65 o 25 5 -8 22.98 0.83 23.17 o 4 6 13 16.53 0.98 16.45 o 11 7 8 17.70 0.83 14.24 o 15 7 5 22.42 0.79 21.65 o 2 10 0 16.57 0.93 16.59 o 2 10 -1 24.70 0.81 24.57 o 14 8 -10 16.63 1.00 14.86 o 19 7 -10 12.02 1.21 7.20 o 28 2 -4 27.04 0.79 26.88 o 17 1 10 52.48 1.32 53.75 o 27 3 -3 27.87 0.90 29.15 o 24 4 1 36.78 1.05 39.44 o 25 3 1 32.78 1.04 34.34 o 26 4 -3 27.28 0.77 27.82 o 5 9 6 40.69 1.02 42.75 o 19 5 -15 28.48 0.77 23.90 o 9 9 -8 39.21 1.30 36.13 o 11 9 -7 14.28 1.16 13.79 o 14 6 -15 19.09 0.93 20.63 o 24 0 4 21.66 0.81 23.14 o 2 10 -2 16.23 0.93 16.06 o 3 9 7 17.55 0.99 14.62 o 18 2 9 24.22 0.78 24.04 o 12 8 -11 13.61 1.11 12.02 o 13 9 -4 14.14 1.05 12.59 o 1 1 -18 26.31 0.81 28.24 o 27 3 -11 19.83 0.92 17.16 o 13 5 10 8.71 1.40 2.24 o 23 1 5 20.46 0.93 23.00 o 21 5 -14 13.33 1.16 11.58 o 21 7 -5 14.95 1.14 13.93 o 13 9 -2 18.88 0.90 16.66 o 20 4 -16 11.20 1.31 10.18 o 21 7 -6 30.86 0.89 32.71 o 25 5 -9 16.11 1.09 17.33 o 14 6 8 19.02 0.90 17.17 o 3 7 12 21.29 0.88 20.10 o 4 10 -1 8.91 1.46 5.21 o 2 2 17 15.03 1.04 11.88 o 6 0 16 14.02 1.10 14.63 o 13 9 -5 13.01 1.14 13.69 o 20 0 8 16.56 0.97 19.06 o 21 7 -4 31.39 0.89 33.25 o 4 10 -2 35.11 1.04 37.18 o 17 7 -12 14.43 1.08 9.58 o 9 7 -14 26.42 0.80 22.69 o 28 2 -11 20.25 0.95 18.94 o 2 10 2 27.84 0.91 29.91 o 2 10 -3 14.80 1.11 15.08 o 21 3 6 14.87 1.09 18.23 o 0 8 11 11.04 1.33 12.82 o 21 7 -7 26.62 0.86 22.96 o 15 7 -13 11.23 1.48 10.97 o 11 9 2 9.11 1.42 6.18 o 1 9 8 35.33 1.01 35.51 o 11 3 13 38.67 0.99 39.94 o 0 10 3 20.55 0.89 19.93 o 28 2 -3 14.94 1.13 14.82 o 13 7 7 14.40 1.16 14.66 o 23 3 4 13.91 1.07 17.49 o 27 1 0 25.53 0.79 25.63 o 18 6 -14 10.34 1.31 10.17 o 10 2 14 19.43 0.95 22.22 o 23 5 1 25.95 0.80 27.15 o 2 4 -17 23.48 0.86 18.29 o 26 2 1 12.01 1.39 16.57 o 9 3 14 15.14 1.04 15.96 o 0 0 18 48.06 1.53 45.65 o 25 5 -3 32.39 1.02 34.71 o 12 2 13 26.28 0.81 26.13 o 4 10 1 24.02 0.81 23.11 o 6 8 -12 31.27 0.89 27.94 o 9 9 4 25.50 0.78 28.20 o 22 2 -17 18.49 0.95 10.46 o 8 8 -12 17.81 0.90 19.98 o 18 8 -6 29.51 0.92 32.11 o 2 6 -15 24.50 0.84 26.05 o 14 2 -19 16.02 1.06 11.03 o 21 7 -3 10.21 1.54 12.08 o 25 1 3 15.55 1.02 17.53 o 11 7 -14 25.53 0.85 25.52 o 13 9 -6 30.21 0.87 32.92 o 5 7 -14 24.01 0.81 23.11 o 9 5 -17 24.05 0.81 19.08 o 8 8 8 38.42 1.04 38.59 o 13 3 12 18.68 0.91 18.71 o 11 5 -17 17.58 0.91 18.88 o 20 6 -13 23.87 0.80 19.00 o 18 6 5 15.60 1.05 15.50 o 25 5 -10 14.03 1.10 12.44 o 18 4 -17 14.91 1.07 13.30 o 18 4 -17 14.91 1.07 13.30 o