Crystallography Open Database

Information card for entry 4321970

4321969 << 4321970 >> 4321971

Preview

Coordinates	4321970.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C34 H42 N8 Ni2 O8
Calculated formula	C34 H42 N9 Ni2 O12
Title of publication	Monoprotic Tetradentate N3O-Donor Ligands and Their Cu(II) and Ni(II) Complexes
Authors of publication	Hongyan Luo; Jem-Mau Lo; Phillip E. Fanwick; Joseph G. Stowell; Mark A. Green
Journal of publication	Inorganic Chemistry
Year of publication	1999
Journal volume	38
Pages of publication	2071 - 2078
a	13.849 ± 0.0004 Å
b	13.6093 ± 0.0004 Å
c	19.5583 ± 0.0005 Å
α	90°
β	92.336 ± 0.002°
γ	90°
Cell volume	3683.19 ± 0.18 Å³
Cell temperature	296 K
Ambient diffraction temperature	296 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for significantly intense reflections	0.054
Weighted residual factors for all reflections included in the refinement	0.154
Goodness-of-fit parameter for all reflections included in the refinement	1.093
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MO-Kα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179322 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/19.	4321970.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4321970.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4321970.cif
19834	2011-05-26	../uploads/cif-deposit/cod/cif Adding structures of 4321970 via cif-deposit CGI script.	4321970.cif