Crystallography Open Database
- COD Home
- Accessing COD Data
- Add Your Data
- Documentation
Information card for entry 4322448
Preview
Coordinates | 4322448.cif |
---|---|
Original paper (by DOI) | HTML |
Formula | C57 H60 Cl4 P6 Pd2 |
---|---|
Calculated formula | C57 H60 Cl4 P6 Pd2 |
Title of publication | A Sterically Enforced Bent Form of an Edge-Sharing Dipalladium(II) Complex Attained by a Linked-Bisphosphido Bridge |
Authors of publication | Tsutomu Mizuta; Shizuka Aoki; Koji Nakayama; Katsuhiko Miyoshi |
Journal of publication | Inorganic Chemistry |
Year of publication | 1999 |
Journal volume | 38 |
Pages of publication | 4361 - 4364 |
a | 22.196 ± 0.0004 Å |
b | 22.551 ± 0.0004 Å |
c | 11.394 ± 0.0001 Å |
α | 90° |
β | 90° |
γ | 90° |
Cell volume | 5703.18 ± 0.15 Å3 |
Cell temperature | 200.2 K |
Ambient diffraction temperature | 200.2 K |
Number of distinct elements | 5 |
Space group number | 33 |
Hermann-Mauguin space group symbol | P n a 21 |
Hall space group symbol | P 2c -2n |
Residual factor for significantly intense reflections | 0.0343 |
Weighted residual factors for significantly intense reflections | 0.0392 |
Goodness-of-fit parameter for significantly intense reflections | 3.964 |
Diffraction radiation wavelength | 0.7107 Å |
Diffraction radiation type | MoKα |
Has coordinates | Yes |
Has disorder | Yes |
Has Fobs | No |
Revision | Date | Message | Files |
---|---|---|---|
200883 (current) | 2017-09-14 | cif/4/32/24/ Specifying alternative Cl atoms, adding attached implicit hydrogens to dichloromethane moiety of entry 4322448. |
4322448.cif |
176467 | 2016-02-16 | cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4. |
4322448.cif |
130086 | 2015-01-23 | cod/ (robertas@burundukas) The 'cif_fix_values' program was applied to CIFs that have generated the validation messages containing tag '_exptl_crystal_density_meas'. 16946 CIFs had a values that were perceived as 'not measured' and they were changed to '?'. The total of 17089 CIFs was changed. Those that were not corrected by 'cif_fix_values' were reformatted by the parser (e.g. a doi tag was moved to another place). The processing command was: mysql -u cod_reader -h www.crystallography.net cod -e \ 'select distinct codid from validation \ where message like \ "%tag%_exptl_crystal_density_meas'\''%"' -NB \ | xargs -i sh -c 'cif_fix_values {} \ | cif_filter --add-cif-header {} \ | sponge {}' |
4322448.cif |
120105 | 2014-07-12 | Adding DOIs to range 4/32 structures. | 4322448.cif |
34330 | 2012-02-24 | cif/4/ Reorganising CIF range 4 into a prefix tree. |
4322448.cif |
20720 | 2011-06-13 | ../uploads/cif-deposit/cod/cif Adding structures of 4322448 via cif-deposit CGI script. |
4322448.cif |
All data in the COD and the database itself are dedicated to the
public domain and licensed under the
CC0
License
.
Users of the data should acknowledge the original authors of the
structural data.