Crystallography Open Database

Information card for entry 4322680

Preview

Coordinates	4322680.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H60 Cl2 Fe N18 Ni3 O8
Calculated formula	C72 H180 Cl6 Fe3 N54 Ni9 O48
Title of publication	Bimetallic Assemblies [Ni(L)2]3[Fe(CN)6]X2 (L = Ethylenediamine, Trimethylenediamine; X = PF6-, ClO4-) with a Three-Dimensional Network Extended through FeII-CN-NiII Linkages
Authors of publication	Nobuo Fukita; Masaaki Ohba; Hisashi Ōkawa; Kenji Matsuda; Hiizu Iwamura
Journal of publication	Inorganic Chemistry
Year of publication	1998
Journal volume	37
Pages of publication	842 - 848
a	14.337 ± 0.002 Å
b	14.3372 Å
c	17.294 ± 0.004 Å
α	90°
β	90°
γ	120°
Cell volume	3078.6 ± 0.8 Å³
Cell temperature	20 K
Ambient diffraction temperature	20 K
Number of distinct elements	7
Space group number	148
Hermann-Mauguin space group symbol	R -3 :H
Hall space group symbol	-R 3
Residual factor for significantly intense reflections	0.024
Weighted residual factors for significantly intense reflections	0.022
Goodness-of-fit parameter for significantly intense reflections	3.59
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4322680.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4322680.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4322680.cif
21566	2011-06-23	../uploads/cif-deposit/cod/cif Adding structures of 4322680 via cif-deposit CGI script.	4322680.cif