#------------------------------------------------------------------------------ #$Date: 2012-02-24 10:01:01 +0200 (Fri, 24 Feb 2012) $ #$Revision: 34320 $ #$URL: file:///home/coder/svn-repositories/cod/hkl/4/32/27/4322704.hkl $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4322704 loop_ _publ_author_name 'Matthias M\"uller' 'V. Cliff Williams' 'Linda H. Doerrer' 'Michael A. Leech' 'Sax A. Mason' 'Malcolm L. H. Green' 'Keith Prout' _publ_contact_author ; Linda H. Doerrer Inorganic Chemistry Laboratory University of Oxford South Parks Road Oxford OX1 3QR, UK ; _publ_contact_author_email ' linda.doerrer@chem.ox.ac.uk ' _publ_contact_author_fax ' 01865 272 690 ' _publ_contact_author_phone ' 01865 272 675 ' _publ_section_title ; Syntheses of the Uranium Complexes [U{N(SiMe3)2}2{N(SiMe3)(SiMe2CH2B(C6F5)3)}] and [U{C(Ph)(NSiMe3)2}2{\m3-BH4}2]. Determination of Hydrogen Positions by Single-Crystal X-ray and Neutron Diffraction ; _journal_name_full 'Inorganic Chemistry' _journal_page_first 1315 _journal_page_last 1323 _journal_volume 37 _journal_year 1998 _chemical_formula_sum 'C26 H54 B2 N4 Si4 U' _chemical_formula_weight 794.74 _space_group_IT_number 15 _symmetry_cell_setting monoclinic _symmetry_space_group_name_Hall '-C 2yc' _symmetry_space_group_name_H-M 'C 1 2/c 1' _cell_angle_alpha 90 _cell_angle_beta 98.804(2) _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 21.613(1) _cell_length_b 9.233(1) _cell_length_c 18.132(1) _cell_volume 3575.7(5) # NOTE Fc on scale of Fo, 0.19572 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_meas _refln_F_calc _refln_F_sigma 2 0 0 48.68 45.65 1.26 4 0 0 25.30 24.62 0.49 6 0 0 29.95 30.75 0.49 8 0 0 77.32 81.61 0.78 10 0 0 52.28 54.18 0.56 12 0 0 46.87 48.49 0.45 14 0 0 55.48 56.90 0.50 16 0 0 37.86 36.77 0.38 18 0 0 37.72 37.18 0.45 20 0 0 16.51 16.11 0.26 22 0 0 36.49 33.88 0.50 1 1 0 14.69 13.24 0.20 3 1 0 23.02 22.11 0.24 5 1 0 41.41 41.03 0.32 7 1 0 43.09 43.13 0.34 9 1 0 33.12 32.45 0.28 11 1 0 8.43 7.25 0.09 13 1 0 15.61 15.33 0.12 15 1 0 20.95 19.96 0.18 17 1 0 5.86 5.06 0.13 19 1 0 28.17 27.62 0.29 21 1 0 27.59 26.38 0.37 23 1 0 13.75 13.58 0.17 25 1 0 3.71 3.55 0.17 0 2 0 18.47 18.38 0.23 2 2 0 27.05 26.03 0.26 4 2 0 6.66 5.93 0.13 6 2 0 14.05 14.12 0.15 8 2 0 33.90 33.78 0.24 10 2 0 22.65 22.87 0.20 12 2 0 8.44 8.21 0.11 14 2 0 3.73 3.63 0.17 16 2 0 18.71 18.39 0.17 18 2 0 21.92 21.33 0.19 20 2 0 24.05 23.81 0.26 22 2 0 7.36 7.41 0.15 24 2 0 7.16 7.00 0.23 26 2 0 7.80 7.85 0.24 1 3 0 64.74 63.79 0.44 3 3 0 52.42 51.53 0.43 5 3 0 45.91 44.97 0.42 7 3 0 59.27 58.04 0.45 9 3 0 39.54 39.15 0.29 11 3 0 53.73 52.68 0.37 13 3 0 55.31 55.54 0.39 15 3 0 43.64 43.48 0.32 17 3 0 29.74 29.57 0.32 19 3 0 25.45 25.43 0.26 21 3 0 41.28 41.12 0.33 23 3 0 27.12 26.61 0.29 25 3 0 26.10 25.27 0.45 0 4 0 48.87 47.83 0.49 2 4 0 10.44 10.17 0.16 4 4 0 13.26 13.06 0.16 6 4 0 35.97 35.15 0.28 8 4 0 45.02 45.06 0.29 10 4 0 11.35 10.74 0.14 12 4 0 16.73 15.94 0.16 14 4 0 26.99 26.83 0.24 16 4 0 19.90 19.36 0.20 18 4 0 22.30 22.37 0.21 20 4 0 22.35 22.09 0.30 22 4 0 20.99 20.74 0.30 24 4 0 6.03 6.21 0.21 1 5 0 3.16 3.08 0.33 3 5 0 21.26 21.73 0.22 5 5 0 17.42 17.77 0.17 7 5 0 7.38 7.41 0.19 9 5 0 20.17 19.59 0.18 11 5 0 14.35 14.11 0.16 13 5 0 5.31 5.32 0.22 15 5 0 4.63 4.46 0.23 17 5 0 17.28 16.61 0.21 19 5 0 15.46 15.65 0.22 21 5 0 4.14 4.16 0.27 23 5 0 8.82 9.29 0.21 0 6 0 49.39 48.60 0.50 2 6 0 54.53 54.38 0.43 4 6 0 38.21 38.42 0.29 6 6 0 30.80 30.44 0.24 8 6 0 28.56 28.29 0.26 10 6 0 44.38 44.71 0.37 12 6 0 41.23 41.22 0.30 14 6 0 31.71 31.07 0.26 16 6 0 31.60 31.66 0.34 18 6 0 28.61 27.92 0.35 20 6 0 23.09 23.04 0.29 22 6 0 20.64 20.71 0.26 1 7 0 17.49 16.96 0.20 3 7 0 30.13 30.39 0.28 5 7 0 28.75 29.47 0.27 7 7 0 30.64 30.57 0.29 9 7 0 20.53 20.41 0.21 11 7 0 16.06 16.12 0.20 13 7 0 21.53 21.28 0.23 15 7 0 15.97 15.84 0.19 17 7 0 14.98 14.36 0.23 19 7 0 17.85 18.25 0.26 21 7 0 23.86 24.13 0.33 0 8 0 2.35 0.00 0.79 2 8 0 7.92 8.15 0.27 4 8 0 9.63 9.74 0.24 6 8 0 5.18 5.58 0.32 8 8 0 7.42 7.13 0.26 10 8 0 16.20 15.96 0.23 12 8 0 3.26 3.04 0.51 14 8 0 1.73 0.00 0.81 16 8 0 5.33 5.42 0.31 18 8 0 9.41 10.00 0.27 1 9 0 25.27 25.35 0.30 3 9 0 29.61 29.83 0.35 5 9 0 36.15 36.09 0.37 7 9 0 22.92 22.71 0.28 9 9 0 31.37 31.19 0.32 11 9 0 34.25 33.93 0.37 13 9 0 19.88 19.72 0.26 15 9 0 20.48 20.63 0.30 17 9 0 26.25 30.99 0.50 0 10 0 15.85 15.50 0.38 2 10 0 18.39 18.90 0.27 4 10 0 31.78 31.95 0.30 6 10 0 11.71 11.60 0.29 8 10 0 14.86 15.11 0.26 10 10 0 21.70 21.30 0.28 12 10 0 20.18 20.42 0.26 1 11 0 5.71 5.62 0.40 3 11 0 3.41 4.00 0.66 5 11 0 3.29 4.48 0.62 7 11 0 2.97 2.20 0.67 -25 1 1 17.91 16.93 0.20 -23 1 1 29.18 27.94 0.30 -21 1 1 27.98 27.17 0.37 -19 1 1 24.53 24.19 0.23 -17 1 1 28.97 28.27 0.25 -15 1 1 32.96 33.40 0.28 -13 1 1 40.76 41.64 0.36 -11 1 1 40.99 40.91 0.30 -9 1 1 52.74 53.88 0.40 -7 1 1 28.61 29.35 0.23 -5 1 1 29.72 29.59 0.26 -3 1 1 41.82 40.90 0.41 -1 1 1 96.80 94.99 0.85 1 1 1 62.46 58.02 0.59 3 1 1 30.99 30.29 0.31 5 1 1 49.40 49.76 0.38 7 1 1 40.71 41.60 0.34 9 1 1 34.66 34.06 0.38 11 1 1 40.00 40.34 0.38 13 1 1 45.71 45.79 0.32 15 1 1 31.38 30.57 0.25 17 1 1 31.74 31.16 0.29 19 1 1 31.25 30.39 0.26 21 1 1 26.09 24.48 0.44 -26 2 1 17.05 16.19 0.26 -24 2 1 16.50 15.77 0.21 -22 2 1 36.89 36.02 0.35 -20 2 1 37.18 36.51 0.32 -18 2 1 26.82 26.50 0.24 -16 2 1 35.18 34.70 0.30 -14 2 1 40.08 41.07 0.34 -12 2 1 22.00 22.10 0.19 -10 2 1 46.42 45.41 0.48 -8 2 1 58.81 59.76 0.46 -6 2 1 46.76 46.93 0.40 -4 2 1 51.89 50.83 0.42 -2 2 1 70.64 70.08 0.69 0 2 1 42.76 41.91 0.37 2 2 1 29.24 28.74 0.28 4 2 1 49.98 49.58 0.47 6 2 1 59.87 60.58 0.45 8 2 1 63.07 63.03 0.46 10 2 1 28.99 28.75 0.21 12 2 1 48.38 48.88 0.32 14 2 1 28.49 28.51 0.27 16 2 1 24.06 23.82 0.23 18 2 1 28.20 28.50 0.27 20 2 1 49.58 48.31 0.38 22 2 1 22.17 21.75 0.29 24 2 1 21.28 19.91 0.38 -25 3 1 2.05 1.58 0.37 -23 3 1 13.75 13.63 0.23 -21 3 1 4.89 4.67 0.24 -19 3 1 10.02 9.70 0.16 -17 3 1 3.90 3.97 0.22 -15 3 1 13.79 14.20 0.17 -13 3 1 12.69 12.55 0.15 -11 3 1 3.39 3.46 0.21 -9 3 1 1.61 0.87 0.37 -7 3 1 16.73 16.16 0.18 -5 3 1 3.66 2.02 0.23 -3 3 1 15.76 14.27 0.16 -1 3 1 5.95 6.02 0.18 1 3 1 17.21 16.81 0.16 3 3 1 10.69 10.08 0.15 5 3 1 16.02 15.46 0.15 7 3 1 11.30 10.89 0.14 9 3 1 14.52 14.30 0.18 11 3 1 14.70 14.38 0.15 13 3 1 17.77 17.76 0.16 15 3 1 1.58 0.00 0.41 17 3 1 0.00 0.00 0.00 19 3 1 6.36 7.00 0.14 21 3 1 1.45 0.00 0.41 23 3 1 3.74 3.60 0.35 25 3 1 4.00 4.20 0.25 -24 4 1 25.08 24.50 0.33 -22 4 1 21.64 21.71 0.30 -20 4 1 23.35 23.68 0.28 -18 4 1 23.45 23.01 0.23 -16 4 1 21.31 21.36 0.25 -14 4 1 21.56 21.40 0.19 -12 4 1 42.28 41.70 0.31 -10 4 1 41.84 41.49 0.30 -8 4 1 30.96 30.65 0.26 -6 4 1 29.33 29.01 0.26 -4 4 1 26.46 26.48 0.23 -2 4 1 45.78 44.56 0.34 0 4 1 46.18 45.31 0.38 2 4 1 41.22 40.86 0.32 4 4 1 30.44 30.51 0.26 6 4 1 35.97 35.21 0.27 8 4 1 30.72 31.09 0.25 10 4 1 37.74 37.09 0.31 12 4 1 28.87 28.42 0.26 14 4 1 30.94 30.87 0.35 16 4 1 29.22 28.87 0.31 18 4 1 24.64 24.71 0.27 20 4 1 17.46 17.60 0.23 22 4 1 25.54 25.18 0.31 24 4 1 18.65 18.68 0.32 -23 5 1 23.85 23.88 0.37 -21 5 1 27.70 27.53 0.29 -19 5 1 28.84 28.63 0.27 -17 5 1 35.73 35.29 0.36 -15 5 1 35.76 35.44 0.30 -13 5 1 35.05 35.21 0.34 -11 5 1 24.46 24.45 0.21 -9 5 1 45.39 44.54 0.35 -7 5 1 35.79 35.92 0.30 -5 5 1 52.14 51.81 0.38 -3 5 1 43.12 43.35 0.31 -1 5 1 56.97 55.77 0.44 1 5 1 31.53 31.05 0.26 3 5 1 35.20 35.34 0.31 5 5 1 48.99 48.76 0.37 7 5 1 47.03 46.96 0.37 9 5 1 41.70 41.05 0.43 11 5 1 30.22 30.18 0.28 13 5 1 41.68 41.13 0.36 15 5 1 22.40 21.85 0.26 17 5 1 30.77 31.04 0.37 19 5 1 28.82 28.87 0.38 21 5 1 32.51 32.49 0.42 23 5 1 21.55 21.39 0.23 -22 6 1 9.19 9.22 0.23 -20 6 1 1.00 0.00 1.15 -18 6 1 6.56 6.45 0.24 -16 6 1 11.00 10.71 0.20 -14 6 1 13.34 13.35 0.19 -12 6 1 2.39 2.50 0.42 -10 6 1 11.86 12.10 0.18 -8 6 1 18.15 18.11 0.18 -6 6 1 3.00 2.46 0.37 -4 6 1 12.26 12.12 0.18 -2 6 1 15.34 15.05 0.18 0 6 1 17.74 17.73 0.19 2 6 1 12.77 12.32 0.18 4 6 1 10.71 10.55 0.18 6 6 1 10.05 9.86 0.19 8 6 1 1.55 0.00 0.68 10 6 1 4.27 3.58 0.29 12 6 1 17.37 17.14 0.18 14 6 1 16.37 16.40 0.20 16 6 1 6.43 6.29 0.25 18 6 1 4.06 4.30 0.32 20 6 1 6.07 6.16 0.24 22 6 1 2.35 2.59 0.47 -21 7 1 12.71 13.21 0.27 -19 7 1 20.32 20.38 0.31 -17 7 1 14.19 14.24 0.22 -15 7 1 11.97 12.25 0.20 -13 7 1 27.07 26.60 0.28 -11 7 1 43.86 43.59 0.34 -9 7 1 22.73 22.41 0.23 -7 7 1 8.98 9.04 0.23 -5 7 1 11.55 12.07 0.20 -3 7 1 30.98 30.48 0.25 -1 7 1 26.06 25.70 0.25 1 7 1 40.78 40.86 0.37 3 7 1 32.44 32.69 0.28 5 7 1 13.59 13.53 0.19 7 7 1 14.10 13.91 0.20 9 7 1 25.33 25.53 0.27 11 7 1 22.61 22.36 0.26 13 7 1 18.44 18.01 0.22 15 7 1 36.69 36.06 0.40 17 7 1 22.21 21.32 0.28 19 7 1 10.32 10.88 0.23 21 7 1 8.07 8.97 0.22 -18 8 1 37.33 36.63 0.32 -16 8 1 30.81 30.08 0.36 -14 8 1 21.22 20.88 0.25 -12 8 1 20.65 20.39 0.23 -10 8 1 26.66 26.28 0.28 -8 8 1 36.08 35.46 0.32 -6 8 1 44.22 44.28 0.41 -4 8 1 41.38 41.19 0.34 -2 8 1 27.77 27.48 0.28 0 8 1 26.40 26.06 0.24 2 8 1 29.75 29.90 0.28 4 8 1 27.45 28.11 0.28 6 8 1 36.15 36.09 0.32 8 8 1 43.47 42.91 0.33 10 8 1 39.36 39.22 0.37 12 8 1 19.51 19.40 0.24 14 8 1 15.79 15.46 0.25 16 8 1 25.77 25.34 0.33 18 8 1 28.06 28.54 0.37 -17 9 1 4.40 3.87 0.54 -15 9 1 9.14 9.20 0.26 -13 9 1 18.77 18.50 0.28 -11 9 1 8.47 8.28 0.28 -9 9 1 10.95 10.79 0.23 -7 9 1 2.07 0.00 0.70 -5 9 1 8.12 8.39 0.31 -3 9 1 4.00 3.61 0.47 -1 9 1 13.66 13.79 0.24 1 9 1 12.56 12.94 0.24 3 9 1 15.80 15.84 0.23 5 9 1 14.98 15.20 0.24 7 9 1 2.83 2.72 0.62 9 9 1 2.61 0.00 0.77 11 9 1 6.72 6.78 0.28 13 9 1 21.32 20.77 0.30 15 9 1 14.05 14.38 0.27 -12 10 1 26.27 26.54 0.41 -10 10 1 17.33 17.63 0.26 -8 10 1 9.03 8.88 0.38 -6 10 1 15.72 15.92 0.24 -4 10 1 16.09 16.27 0.27 -2 10 1 10.67 10.92 0.32 0 10 1 20.44 20.11 0.26 2 10 1 25.05 25.17 0.31 4 10 1 20.53 20.78 0.27 6 10 1 5.97 6.76 0.50 8 10 1 12.00 11.81 0.27 10 10 1 19.38 19.34 0.29 12 10 1 15.72 16.21 0.31 -7 11 1 24.53 25.58 0.32 -5 11 1 33.34 33.79 0.42 -3 11 1 34.58 35.11 0.35 -1 11 1 11.36 11.62 0.33 1 11 1 21.93 22.68 0.32 3 11 1 31.54 32.22 0.41 5 11 1 20.75 21.06 0.33 7 11 1 24.44 25.22 0.30 -26 0 2 25.52 24.13 0.42 -24 0 2 41.80 39.22 0.44 -22 0 2 47.73 46.89 0.70 -20 0 2 15.29 15.49 0.25 -18 0 2 42.29 41.43 0.48 -16 0 2 24.55 24.72 0.32 -14 0 2 45.86 47.49 0.53 -12 0 2 46.60 47.46 0.47 -10 0 2 75.32 79.96 0.66 -8 0 2 47.17 49.87 0.57 -6 0 2 16.77 17.24 0.28 -4 0 2 28.58 29.30 0.50 -2 0 2 75.34 76.33 0.90 0 0 2 93.25 93.47 1.16 2 0 2 46.03 47.27 0.80 8 0 2 12.81 12.14 0.21 10 0 2 49.72 47.91 0.57 12 0 2 58.66 56.86 0.70 14 0 2 40.13 37.10 0.50 -25 1 2 6.19 5.91 0.19 -23 1 2 12.71 12.49 0.23 -21 1 2 19.11 18.76 0.20 -19 1 2 17.72 17.73 0.21 -17 1 2 32.26 31.75 0.31 -15 1 2 25.13 25.69 0.20 -13 1 2 6.72 6.31 0.13 -11 1 2 11.45 10.84 0.13 -9 1 2 32.98 32.33 0.30 -7 1 2 4.94 4.56 0.14 -5 1 2 28.56 28.57 0.25 -3 1 2 88.05 90.98 0.66 -1 1 2 19.45 19.12 0.23 1 1 2 10.85 10.69 0.13 3 1 2 4.40 3.92 0.10 5 1 2 58.93 59.98 0.39 7 1 2 55.36 55.98 0.45 9 1 2 34.42 34.39 0.24 11 1 2 35.38 37.00 0.31 13 1 2 26.64 24.25 0.26 15 1 2 8.97 8.42 0.16 17 1 2 7.28 6.80 0.13 19 1 2 34.16 31.35 0.39 -26 2 2 8.03 8.00 0.19 -24 2 2 3.05 3.57 0.30 -22 2 2 3.59 3.44 0.31 -20 2 2 20.77 20.42 0.20 -18 2 2 13.44 13.32 0.16 -16 2 2 23.90 24.03 0.21 -14 2 2 16.10 15.55 0.15 -12 2 2 15.89 15.86 0.14 -10 2 2 18.35 17.91 0.16 -8 2 2 10.13 10.34 0.11 -6 2 2 29.63 29.38 0.22 -4 2 2 39.04 38.47 0.37 -2 2 2 40.58 39.45 0.35 0 2 2 20.46 19.60 0.22 2 2 2 18.08 17.32 0.17 4 2 2 7.01 5.94 0.12 6 2 2 15.23 15.32 0.17 8 2 2 46.73 45.74 0.33 10 2 2 24.97 25.35 0.24 12 2 2 19.33 19.22 0.15 14 2 2 8.92 8.71 0.10 16 2 2 10.81 10.52 0.12 18 2 2 21.60 20.72 0.30 20 2 2 18.73 18.05 0.27 22 2 2 21.86 20.57 0.35 -25 3 2 25.16 24.13 0.34 -23 3 2 37.75 37.15 0.41 -21 3 2 36.83 36.39 0.31 -19 3 2 29.31 29.26 0.31 -17 3 2 22.65 22.24 0.23 -15 3 2 36.11 36.24 0.27 -13 3 2 38.43 38.51 0.28 -11 3 2 63.89 63.98 0.46 -9 3 2 51.32 52.77 0.40 -7 3 2 49.47 49.21 0.38 -5 3 2 41.65 40.92 0.30 -3 3 2 64.65 64.29 0.46 -1 3 2 62.04 61.12 0.44 1 3 2 12.47 12.93 0.14 3 3 2 68.50 67.98 0.48 5 3 2 56.90 56.38 0.46 7 3 2 48.44 47.13 0.35 9 3 2 21.98 21.29 0.16 11 3 2 42.91 42.05 0.32 13 3 2 39.27 38.72 0.28 15 3 2 37.33 37.41 0.34 17 3 2 36.64 36.26 0.41 19 3 2 33.52 33.45 0.28 21 3 2 30.76 30.58 0.57 23 3 2 18.64 18.51 0.36 25 3 2 26.57 26.38 0.35 -24 4 2 15.52 15.69 0.28 -22 4 2 15.03 14.94 0.22 -20 4 2 6.54 6.62 0.22 -18 4 2 23.32 23.44 0.23 -16 4 2 36.64 36.24 0.31 -14 4 2 26.97 26.66 0.26 -12 4 2 6.92 6.47 0.17 -10 4 2 32.36 32.15 0.30 -8 4 2 24.81 24.54 0.20 -6 4 2 32.67 31.76 0.31 -4 4 2 33.70 33.97 0.30 -2 4 2 44.75 44.26 0.30 0 4 2 29.08 27.89 0.23 2 4 2 12.88 12.57 0.16 4 4 2 32.79 32.65 0.28 6 4 2 24.17 24.43 0.22 8 4 2 24.12 24.12 0.22 10 4 2 28.02 28.15 0.23 12 4 2 44.72 43.80 0.36 14 4 2 9.39 9.28 0.15 16 4 2 12.51 11.96 0.14 18 4 2 29.59 29.70 0.29 20 4 2 24.82 24.26 0.26 22 4 2 17.74 17.87 0.36 24 4 2 18.39 18.44 0.36 -23 5 2 5.11 5.39 0.29 -21 5 2 14.33 14.76 0.21 -19 5 2 14.86 15.00 0.22 -17 5 2 4.86 4.95 0.26 -15 5 2 7.78 8.13 0.19 -13 5 2 25.14 24.71 0.25 -11 5 2 4.42 3.89 0.26 -9 5 2 11.06 11.48 0.16 -7 5 2 15.46 15.59 0.17 -5 5 2 40.27 40.12 0.48 -3 5 2 9.97 9.90 0.17 -1 5 2 4.24 3.90 0.31 1 5 2 22.94 22.82 0.19 3 5 2 10.26 10.33 0.18 5 5 2 6.47 5.48 0.21 7 5 2 21.89 22.42 0.22 9 5 2 30.15 30.35 0.25 11 5 2 14.55 14.18 0.17 13 5 2 7.29 7.14 0.17 15 5 2 6.95 6.45 0.18 17 5 2 7.48 7.49 0.19 19 5 2 7.87 7.78 0.18 21 5 2 16.83 16.92 0.29 23 5 2 13.58 13.84 0.20 -22 6 2 24.70 24.91 0.31 -20 6 2 29.57 29.26 0.43 -18 6 2 24.57 24.59 0.27 -16 6 2 25.47 25.06 0.27 -14 6 2 33.22 32.78 0.30 -12 6 2 43.45 43.17 0.34 -10 6 2 35.18 35.43 0.27 -8 6 2 36.48 36.24 0.31 -6 6 2 31.18 31.72 0.29 -4 6 2 26.94 26.86 0.22 -2 6 2 38.14 37.50 0.34 0 6 2 52.17 52.21 0.42 2 6 2 52.17 52.96 0.37 4 6 2 37.14 37.09 0.30 6 6 2 30.35 29.58 0.26 8 6 2 39.88 39.56 0.31 10 6 2 36.69 35.99 0.31 12 6 2 25.73 25.07 0.25 14 6 2 35.87 35.10 0.32 16 6 2 37.39 37.41 0.39 18 6 2 27.08 26.52 0.35 20 6 2 19.11 19.38 0.25 22 6 2 17.99 18.28 0.24 -21 7 2 17.09 17.22 0.30 -19 7 2 21.24 21.22 0.27 -17 7 2 21.08 20.63 0.27 -15 7 2 27.06 26.90 0.29 -13 7 2 9.99 9.62 0.22 -11 7 2 19.91 19.60 0.22 -9 7 2 23.96 23.75 0.23 -7 7 2 26.80 26.95 0.24 -5 7 2 26.99 27.22 0.25 -3 7 2 27.53 27.74 0.25 -1 7 2 27.93 28.00 0.23 1 7 2 17.64 17.68 0.21 3 7 2 30.84 30.41 0.27 5 7 2 20.48 20.47 0.21 7 7 2 38.01 38.14 0.35 9 7 2 22.56 22.68 0.22 11 7 2 29.17 28.91 0.29 13 7 2 19.06 18.92 0.23 15 7 2 17.42 17.59 0.28 17 7 2 20.27 20.17 0.25 19 7 2 18.02 17.77 0.27 21 7 2 16.34 17.05 0.67 -18 8 2 5.52 6.12 0.31 -16 8 2 2.57 0.00 0.68 -14 8 2 5.68 5.63 0.28 -12 8 2 14.19 14.56 0.22 -10 8 2 8.69 8.63 0.24 -8 8 2 4.46 3.61 0.34 -6 8 2 5.02 4.83 0.29 -4 8 2 16.22 16.02 0.22 -2 8 2 4.07 4.23 0.40 0 8 2 10.45 10.42 0.23 2 8 2 10.20 10.10 0.24 4 8 2 7.35 7.17 0.30 6 8 2 8.50 8.59 0.24 8 8 2 15.57 15.71 0.23 10 8 2 4.71 5.43 0.35 12 8 2 2.43 3.14 0.54 14 8 2 12.12 12.17 0.23 16 8 2 8.60 8.61 0.24 18 8 2 3.03 3.48 0.49 -17 9 2 22.31 23.31 0.30 -15 9 2 16.05 16.05 0.27 -13 9 2 36.93 36.84 0.41 -11 9 2 23.10 23.27 0.27 -9 9 2 20.99 20.54 0.24 -7 9 2 35.68 35.64 0.37 -5 9 2 37.30 36.91 0.47 -3 9 2 24.04 23.84 0.28 -1 9 2 22.40 22.52 0.27 1 9 2 36.98 37.16 0.37 3 9 2 20.53 20.39 0.25 5 9 2 29.47 29.10 0.29 7 9 2 23.12 23.16 0.27 9 9 2 36.49 36.28 0.43 11 9 2 20.06 19.98 0.25 13 9 2 18.04 18.43 0.26 15 9 2 26.95 27.26 0.39 -12 10 2 18.16 18.36 0.25 -10 10 2 20.14 20.29 0.25 -8 10 2 23.59 22.98 0.28 -6 10 2 22.69 22.69 0.28 -4 10 2 23.42 23.10 0.30 -2 10 2 11.14 11.21 0.28 0 10 2 26.78 26.95 0.36 2 10 2 31.58 31.67 0.38 4 10 2 16.87 17.03 0.27 6 10 2 15.38 15.57 0.25 8 10 2 21.16 21.42 0.33 10 10 2 17.75 18.13 0.31 12 10 2 15.06 15.58 0.28 -7 11 2 2.07 0.00 0.75 -5 11 2 2.14 0.00 0.86 -3 11 2 2.97 0.74 0.59 -1 11 2 4.39 4.06 0.53 1 11 2 3.82 3.99 0.65 3 11 2 5.94 6.08 0.41 5 11 2 2.77 0.00 0.72 7 11 2 3.95 4.44 0.49 -27 1 3 15.82 15.84 0.36 -25 1 3 25.24 24.28 0.32 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