Crystallography Open Database

Information card for entry 4323784

Preview

Coordinates	4323784.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H31 Cl N O P Pd
Calculated formula	C24 H31 Cl N O P Pd
Title of publication	First Resolution of a Free Fluorophosphine Chiral at Phosphorus. Resolution and Reactions of Free and Coordinated (\±)-Fluorophenylisopropylphosphine
Authors of publication	Michael Pabel; Anthony C. Willis; S. Bruce Wild
Journal of publication	Inorganic Chemistry
Year of publication	1996
Journal volume	35
Pages of publication	1244 - 1249
a	10.444 ± 0.003 Å
b	12.146 ± 0.003 Å
c	19.047 ± 0.004 Å
α	90°
β	90°
γ	90°
Cell volume	2416.2 ± 1 Å³
Cell temperature	296.2 K
Ambient diffraction temperature	296.2 K
Number of distinct elements	7
Space group number	19
Hermann-Mauguin space group symbol	P 21 21 21
Hall space group symbol	P 2ac 2ab
Residual factor for significantly intense reflections	0.026
Weighted residual factors for significantly intense reflections	0.029
Goodness-of-fit parameter for significantly intense reflections	1.54
Diffraction radiation wavelength	0.7107 Å
Diffraction radiation type	MoKalpha
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176432 (current)	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	4323784.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4323784.cif
34330	2012-02-24	cif/4/ Reorganising CIF range 4 into a prefix tree.	4323784.cif
24033	2011-08-12	../uploads/cif-deposit/cod/cif Adding structures of 4323784 via cif-deposit CGI script.	4323784.cif