Crystallography Open Database

Information card for entry 4327296

Preview

Coordinates	4327296.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C14 H13 Mo N O5
Calculated formula	C14 H13 Mo N O5
Title of publication	Synthesis, Structure, and Characterization of Molybdenum(VI) Imido Complexes with N-Salicylidene-2-aminophenol
Authors of publication	Martin Minelli; Frances Namuswe; Daniel Jeffrey; Amy L. Morrow; Ilia A. Guzei; Dale Swenson; Eberhard Bothe; Thomas Weyhermüller
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Pages of publication	5455 - 5464
a	11.4839 ± 0.0006 Å
b	6.7543 ± 0.0004 Å
c	17.5715 ± 0.0009 Å
α	90°
β	92.878 ± 0.005°
γ	90°
Cell volume	1361.23 ± 0.13 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0444
Residual factor for significantly intense reflections	0.0326
Weighted residual factors for significantly intense reflections	0.0692
Weighted residual factors for all reflections included in the refinement	0.0736
Goodness-of-fit parameter for all reflections included in the refinement	1.069
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179375 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/72.	4327296.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327296.cif
61012	2012-06-20	cif/ Adding structures of 4327296 via cif-deposit CGI script.	4327296.cif