Crystallography Open Database

Information card for entry 4327622

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Structure parameters

Formula	C24 H40 Br Li Mg N2 O2 Si2
Calculated formula	C24 H40 Br Li Mg N2 O2 Si2
Title of publication	Synthesis and Structural Characterization of Metalated 1,8-Bis(silylamino)naphthalene Derivatives
Authors of publication	Christian H. Galka; Dominique J. M. Trösch; Ina Rüdenauer; Lutz H. Gade; Ian Scowen; Mary McPartlin
Journal of publication	Inorganic Chemistry
Year of publication	2000
Journal volume	39
Pages of publication	4615 - 4620
a	11.6817 ± 0.0011 Å
b	11.7292 ± 0.0015 Å
c	22.157 ± 0.003 Å
α	90°
β	94.625 ± 0.007°
γ	90°
Cell volume	3026 ± 0.6 Å³
Cell temperature	299 ± 2 K
Ambient diffraction temperature	299 ± 2 K
Number of distinct elements	8
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1737
Residual factor for significantly intense reflections	0.0698
Weighted residual factors for significantly intense reflections	0.1291
Weighted residual factors for all reflections included in the refinement	0.1538
Goodness-of-fit parameter for all reflections included in the refinement	0.926
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
301838 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 4/32/ Each referenced PubChem compound corresponds to the full crystal structure.	4327622.cif
179379	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/76.	4327622.cif
120105	2014-07-12	Adding DOIs to range 4/32 structures.	4327622.cif
61454	2012-07-04	cif/ Adding structures of 4327622 via cif-deposit CGI script.	4327622.cif