Crystallography Open Database

Information card for entry 4328425

Preview

Coordinates	4328425.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C45 H108 N6 O9 Ru3 Si12 Sn3
Calculated formula	C45 H108 N6 O9 Ru3 Si12 Sn3
Title of publication	Synthesis of Mixed Tin-Ruthenium and Tin-Germanium-Ruthenium Carbonyl Clusters from [Ru3(CO)12] and Diaminometalenes (M = Sn, Ge)
Authors of publication	Javier A. Cabeza; Pablo García-Álvarez; Diego Polo
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	2569 - 2576
a	14.924 ± 0.0002 Å
b	14.924 ± 0.0002 Å
c	20.755 ± 0.0004 Å
α	90°
β	90°
γ	120°
Cell volume	4003.35 ± 0.11 Å³
Cell temperature	297 ± 2 K
Ambient diffraction temperature	297 ± 2 K
Number of distinct elements	7
Space group number	176
Hermann-Mauguin space group symbol	P 63/m
Hall space group symbol	-P 6c
Residual factor for all reflections	0.0493
Residual factor for significantly intense reflections	0.0458
Weighted residual factors for significantly intense reflections	0.1279
Weighted residual factors for all reflections included in the refinement	0.1319
Goodness-of-fit parameter for all reflections included in the refinement	1.084
Diffraction radiation wavelength	1.5418 Å
Diffraction radiation type	CuKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179387 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/84.	4328425.cif
77391	2013-03-26	cif/ Adding structures of 4328425 via cif-deposit CGI script.	4328425.cif