Crystallography Open Database

Information card for entry 4328992

Preview

Coordinates	4328992.cif
Original paper (by DOI)	HTML

Structure parameters

Chemical name	tetra-(4-ethoxycarbonyl benzoate)- dirhodium (II,II),chloroform solvate
Formula	C42 H38 Cl6 O16 Rh2
Calculated formula	C42 H38 Cl6 O16 Rh2
Title of publication	Dirhodium Paddlewheel with Functionalized Carboxylate Bridges: New Building Block for Self-Assembly and Immobilization on Solid Support
Authors of publication	D. Krishna Kumar; Alexander S. Filatov; Margaret Napier; Jinyu Sun; Evgeny V. Dikarev; Marina A. Petrukhina
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	4855 - 4861
a	22.3558 ± 0.0015 Å
b	16.8627 ± 0.0011 Å
c	16.408 ± 0.0011 Å
α	90°
β	92.8 ± 0.001°
γ	90°
Cell volume	6178.1 ± 0.7 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0414
Residual factor for significantly intense reflections	0.0341
Weighted residual factors for significantly intense reflections	0.0978
Weighted residual factors for all reflections included in the refinement	0.1005
Goodness-of-fit parameter for all reflections included in the refinement	1.195
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179392 (current)	2016-03-23	cif/4/32/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/32/89.	4328992.cif
78032	2013-04-01	cif/ Adding structures of 4328992 via cif-deposit CGI script.	4328992.cif