Crystallography Open Database

Information card for entry 4330282

Preview

Coordinates	4330282.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C32 H72 Cl6 N2 Pu
Calculated formula	C32 H72 Cl6 N2 Pu
Title of publication	[N(n-Bu)4]2[Pu(NO3)6] and [N(n-Bu)4]2[PuCl6]: Starting Materials To Facilitate Nonaqueous Plutonium(IV) Chemistry
Authors of publication	Sean D. Reilly; Brian L. Scott; Andrew J. Gaunt
Journal of publication	Inorganic Chemistry
Year of publication	2012
Journal volume	51
Pages of publication	9165 - 9167
a	16.29 ± 0.003 Å
b	15.74 ± 0.003 Å
c	17.984 ± 0.003 Å
α	90°
β	112.77 ± 0.002°
γ	90°
Cell volume	4251.8 ± 1.3 Å³
Cell temperature	141 ± 2 K
Ambient diffraction temperature	141 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.043
Residual factor for significantly intense reflections	0.0352
Weighted residual factors for significantly intense reflections	0.0883
Weighted residual factors for all reflections included in the refinement	0.0902
Goodness-of-fit parameter for all reflections included in the refinement	1.889
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179405 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/02.	4330282.cif
79534	2013-04-05	cif/ Adding structures of 4330282 via cif-deposit CGI script.	4330282.cif