Crystallography Open Database

Information card for entry 4332567

Preview

Coordinates	4332567.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54 H66.5 Cl2.5 Co4 N9 Na O30
Calculated formula	C54 H57 Cl2.5 Co4 N9 Na O30.01
Title of publication	Two Chiral Metal Clusters Derived from Nucleophilic Addition ofl-proline to Di-2-pyridyl Ketone
Authors of publication	Li, Yamin; Xiang, Shengchang; Sheng, Tianlu; Zhang, Jianjun; Hu, Shengmin; Fu, Ruibiao; Huang, Xihe; Wu, Xintao
Journal of publication	Inorganic Chemistry
Year of publication	2006
Journal volume	45
Journal issue	17
Pages of publication	6577 - 6579
a	23.917 ± 0.003 Å
b	23.917 ± 0.003 Å
c	23.917 ± 0.003 Å
α	90°
β	90°
γ	90°
Cell volume	13681 ± 3 Å³
Cell temperature	130.15 K
Ambient diffraction temperature	130.15 K
Number of distinct elements	7
Space group number	198
Hermann-Mauguin space group symbol	P 21 3
Hall space group symbol	P 2ac 2ab 3
Residual factor for all reflections	0.0696
Residual factor for significantly intense reflections	0.0671
Weighted residual factors for significantly intense reflections	0.1841
Weighted residual factors for all reflections included in the refinement	0.1883
Goodness-of-fit parameter for all reflections included in the refinement	1.087
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4332567.cif
98390	2014-01-30	cif/ Adding structures of 4332567 via cif-deposit CGI script.	4332567.cif