Crystallography Open Database

Information card for entry 4333272

Preview

Coordinates	4333272.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C54.5 H162 Ag3 B33 Cl N3 P3 Sn3
Calculated formula	C54.5 H162 Ag3 B33 Cl N3 P3 Sn3
Title of publication	Silver aggregation caused by Stanna-closo-dodecaborate coordination: syntheses, solid-state structures and theoretical studies.
Authors of publication	Hagen, Siegbert; Schubert, Hartmut; Maichle-Mössmer, Cäcilia; Pantenburg, Ingo; Weigend, Florian; Wesemann, Lars
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	16
Pages of publication	6775 - 6784
a	15.7176 ± 0.0017 Å
b	16.8227 ± 0.0015 Å
c	21.692 ± 0.002 Å
α	99.861 ± 0.008°
β	97.8 ± 0.008°
γ	116.129 ± 0.007°
Cell volume	4926.8 ± 0.9 Å³
Cell temperature	173 K
Ambient diffraction temperature	173 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.159
Residual factor for significantly intense reflections	0.0884
Weighted residual factors for significantly intense reflections	0.1161
Weighted residual factors for all reflections included in the refinement	0.1345
Goodness-of-fit parameter for all reflections included in the refinement	1.113
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179435 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/32.	4333272.cif
116746	2014-06-13	cif/ Updating files of 4333271, 4333272, 4333273, 4333274 Original log message: Adding full bibliography for 4333271--4333274.cif.	4333272.cif
98893	2014-01-30	cif/ Adding structures of 4333272 via cif-deposit CGI script.	4333272.cif