Crystallography Open Database

Information card for entry 4333292

Preview

Coordinates	4333292.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C16 H36 N O14.33 P0.33 Sn0.33 W3.67
Calculated formula	C16 H36 N O14.3333 P0.333333 Sn0.34 W3.66
Title of publication	A New Method for the Synthesis of Organopolyoxometalate Hybrid Compounds
Authors of publication	Bar-Nahum, Itsik; Ettedgui, Jessica; Konstantinovski, Leonid; Kogan, Vladimir; Neumann, Ronny
Journal of publication	Inorganic Chemistry
Year of publication	2007
Journal volume	46
Journal issue	14
Pages of publication	5798 - 5804
a	23.268 ± 0.003 Å
b	23.268 ± 0.003 Å
c	46.969 ± 0.009 Å
α	90°
β	90°
γ	120°
Cell volume	22022 ± 6 Å³
Cell temperature	120 ± 2 K
Ambient diffraction temperature	120 ± 2 K
Number of distinct elements	7
Space group number	167
Hermann-Mauguin space group symbol	R -3 c :H
Hall space group symbol	-R 3 2"c
Residual factor for all reflections	0.1144
Residual factor for significantly intense reflections	0.0806
Weighted residual factors for significantly intense reflections	0.2184
Weighted residual factors for all reflections included in the refinement	0.2407
Goodness-of-fit parameter for all reflections included in the refinement	1.113
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179435 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/32.	4333292.cif
98908	2014-01-30	cif/ Adding structures of 4333292 via cif-deposit CGI script.	4333292.cif