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Information card for entry 4333604
Preview
| Coordinates | 4333604.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Formula | C30 H30 F6 N4 O2 Os P |
|---|---|
| Calculated formula | C30 H23 F6 N4 O4.5 Os P |
| Title of publication | C-H Bond Activation of the Methyl Group of the Supporting Ligand in an Osmium(III) Complex upon Reaction with H2O2: Formation of an Organometallic Osmium(IV) Complex |
| Authors of publication | Hideki Sugimoto; Kenji Ashikari; Shinobu Itoh |
| Journal of publication | Inorganic Chemistry |
| Year of publication | 2013 |
| Journal volume | 52 |
| Pages of publication | 543 - 545 |
| a | 11.9045 ± 0.0005 Å |
| b | 14.6137 ± 0.0008 Å |
| c | 20.9467 ± 0.0011 Å |
| α | 90° |
| β | 90° |
| γ | 90° |
| Cell volume | 3644.1 ± 0.3 Å3 |
| Cell temperature | 108 K |
| Ambient diffraction temperature | 108 K |
| Number of distinct elements | 7 |
| Space group number | 62 |
| Hermann-Mauguin space group symbol | P n m a |
| Hall space group symbol | -P 2ac 2n |
| Residual factor for significantly intense reflections | 0.0543 |
| Weighted residual factors for all reflections included in the refinement | 0.1355 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.301 |
| Diffraction radiation wavelength | 0.71075 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179439 (current) | 2016-03-23 | cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/36. |
4333604.cif |
| 99400 | 2014-01-31 | cif/ Adding structures of 4333604 via cif-deposit CGI script. |
4333604.cif |
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Users of the data should acknowledge the original authors of the
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