Crystallography Open Database

Information card for entry 4334956

Preview

Coordinates	4334956.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C36 H66 B N3 P Rh Si2
Calculated formula	C36 H66 B N3 P Rh Si2
Title of publication	Synthesis and Structure of a Carbene-Stabilized Boraallene Coordinated to Rhodium
Authors of publication	Holger Braunschweig; Qing Ye; Krzysztof Radacki
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	5639 - 5641
a	10.6199 ± 0.0017 Å
b	13.047 ± 0.002 Å
c	15.053 ± 0.002 Å
α	75.854 ± 0.007°
β	86.561 ± 0.007°
γ	76.536 ± 0.007°
Cell volume	1966.9 ± 0.5 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	7
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0314
Residual factor for significantly intense reflections	0.0256
Weighted residual factors for significantly intense reflections	0.0623
Weighted residual factors for all reflections included in the refinement	0.0706
Goodness-of-fit parameter for all reflections included in the refinement	0.938
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179452 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/49.	4334956.cif
100842	2014-02-07	cif/ Adding structures of 4334956 via cif-deposit CGI script.	4334956.cif