Crystallography Open Database

Information card for entry 4335617

Preview

Coordinates	4335617.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	B3 H2 O7.5 Pb2
Calculated formula	B3 H2 O7.5 Pb2
Title of publication	Pb2B3O5.5(OH)2 and [Pb3(B3O7)](NO3): Facile Syntheses of New Lead(II) Borates by Simply Changing the pH Values of the Reaction Systems
Authors of publication	Jun-Ling Song; Chun-Li Hu; Xiang Xu; Fang Kong; Jiang-Gao Mao
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	8979 - 8986
a	11.5824 ± 0.0007 Å
b	11.7664 ± 0.0007 Å
c	4.5657 ± 0.0002 Å
α	90°
β	90°
γ	90°
Cell volume	622.23 ± 0.06 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	34
Hermann-Mauguin space group symbol	P n n 2
Hall space group symbol	P 2 -2n
Residual factor for all reflections	0.0242
Residual factor for significantly intense reflections	0.0217
Weighted residual factors for significantly intense reflections	0.0385
Weighted residual factors for all reflections included in the refinement	0.0394
Goodness-of-fit parameter for all reflections included in the refinement	0.994
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4335617.cif
101552	2014-02-14	cif/ Adding structures of 4335617 via cif-deposit CGI script.	4335617.cif