Crystallography Open Database

Information card for entry 4336649

Preview

Coordinates	4336649.cif
Original paper (by DOI)	HTML

Structure parameters

Common name	compound-4
Formula	Ag Ge2 Na5 S7
Calculated formula	Ag Ge2 Na5 S7
Title of publication	Mild Solvothermal Syntheses of Thioargentates A-Ag-S (A = K, Rb, Cs) and A-Ag-Ge-S (A = Na, Rb): Crucial Role of Excess Sulfur
Authors of publication	Chi Zhang; Kai-Ni Wang; Min Ji; Yong-Lin An
Journal of publication	Inorganic Chemistry
Year of publication	2013
Journal volume	52
Pages of publication	12367 - 12371
a	9.1456 ± 0.0018 Å
b	10.2611 ± 0.0019 Å
c	14.863 ± 0.003 Å
α	90°
β	104.315 ± 0.002°
γ	90°
Cell volume	1351.5 ± 0.5 Å³
Cell temperature	296 ± 2 K
Ambient diffraction temperature	296 ± 2 K
Number of distinct elements	4
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.029
Residual factor for significantly intense reflections	0.027
Weighted residual factors for significantly intense reflections	0.0751
Weighted residual factors for all reflections included in the refinement	0.0767
Goodness-of-fit parameter for all reflections included in the refinement	1.136
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4336649.cif
102656	2014-02-21	cif/ Adding structures of 4336649 via cif-deposit CGI script.	4336649.cif