Crystallography Open Database

Information card for entry 4337127

Preview

Coordinates	4337127.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C31.13 H31 B2 Co5.11 O11.13 Rh2
Calculated formula	C31.14 H31 B2 Co5.12 O11.14 Rh2
Title of publication	A Novel Heterometallic μ9-Boride Cluster: Synthesis and Structural Characterization of [(η(5)-C5Me5Rh)2{Co6(CO)12}(μ-H)(BH)B].
Authors of publication	Roy, Dipak Kumar; Barik, Subrat Kumar; Mondal, Bijan; Varghese, Babu; Ghosh, Sundargopal
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	2
Pages of publication	667 - 669
a	21.5552 ± 0.0004 Å
b	10.3266 ± 0.0001 Å
c	17.3114 ± 0.0003 Å
α	90°
β	107.77 ± 0.002°
γ	90°
Cell volume	3669.53 ± 0.11 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0606
Residual factor for significantly intense reflections	0.0596
Weighted residual factors for significantly intense reflections	0.1368
Weighted residual factors for all reflections included in the refinement	0.1372
Goodness-of-fit parameter for all reflections included in the refinement	1.352
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179474 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/71.	4337127.cif
106175	2014-03-15	cif/ Adding structures of 4337127, 4337128, 4337129 via cif-deposit CGI script.	4337127.cif