Crystallography Open Database

Information card for entry 4338663

Preview

Coordinates	4338663.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C24 H51 Br N5 Ta
Calculated formula	C24 H51 Br N5 Ta
Title of publication	Volatility and High Thermal Stability in Tantalum Complexes Containing Imido, Amidinate, and Halide or Dialkylamide Ligands
Authors of publication	Wiedmann, Monika K.; Heeg, Mary Jane; Winter, Charles H.
Journal of publication	Inorganic chemistry
Year of publication	2009
Journal volume	48
Journal issue	12
Pages of publication	5382 - 5391
a	11.8983 ± 0.0004 Å
b	16.3458 ± 0.0006 Å
c	15.0157 ± 0.0005 Å
α	90°
β	94.221 ± 0.002°
γ	90°
Cell volume	2912.44 ± 0.17 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	5
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.034
Residual factor for significantly intense reflections	0.0289
Weighted residual factors for significantly intense reflections	0.0716
Weighted residual factors for all reflections included in the refinement	0.0738
Goodness-of-fit parameter for all reflections included in the refinement	1.037
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
210068 (current)	2018-08-23	cif/4/ Updating bibliography in entries 4302375-4302376, 4338662-4338663. Marking entries 4302375-4302376 as duplicates of entries 4338663, 4338662.	4338663.cif
179489	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/86.	4338663.cif
114782	2014-05-29	cif/ Adding structures of 4338662, 4338663 via cif-deposit CGI script.	4338663.cif