Crystallography Open Database

Information card for entry 4338676

Preview

Coordinates	4338676.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C129 H156 Si6
Calculated formula	C129 H156 Si6
Title of publication	Isolable 1,1-disubstituted silole dianion: a homogeneous two-electron-transfer reducing reagent.
Authors of publication	Han, Zhengang; Li, Jianfeng; Hu, Hongfan; Zhang, Jianying; Cui, Chunming
Journal of publication	Inorganic chemistry
Year of publication	2014
Journal volume	53
Journal issue	12
Pages of publication	5890 - 5892
a	11.813 ± 0.002 Å
b	15.658 ± 0.003 Å
c	16.713 ± 0.003 Å
α	84.56 ± 0.03°
β	79.12 ± 0.03°
γ	81.76 ± 0.03°
Cell volume	2997.2 ± 1 Å³
Cell temperature	113.15 K
Ambient diffraction temperature	113.15 K
Number of distinct elements	3
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.1437
Residual factor for significantly intense reflections	0.0789
Weighted residual factors for significantly intense reflections	0.1976
Weighted residual factors for all reflections included in the refinement	0.241
Goodness-of-fit parameter for all reflections included in the refinement	0.959
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176467 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 4.	4338676.cif
119112	2014-07-05	cif/ Updating files of 4338675, 4338676 Original log message: Adding full bibliography for 4338675--4338676.cif.	4338676.cif
114971	2014-05-31	cif/ Adding structures of 4338675, 4338676 via cif-deposit CGI script.	4338676.cif