Crystallography Open Database

Information card for entry 4339737

Preview

Coordinates	4339737.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C48 H28 Ca0.19 La N4 O10
Calculated formula	C48 H28 Ca0.193 La N4 O10
Title of publication	Porphyrin framework solids. Synthesis and structure of hybrid coordination polymers of tetra(carboxyphenyl)porphyrins and lanthanide-bridging ions.
Authors of publication	Muniappan, Sankar; Lipstman, Sophia; George, Sumod; Goldberg, Israel
Journal of publication	Inorganic chemistry
Year of publication	2007
Journal volume	46
Journal issue	14
Pages of publication	5544 - 5554
a	13.8138 ± 0.0002 Å
b	33.7925 ± 0.0007 Å
c	9.8548 ± 0.0003 Å
α	90°
β	92.8627 ± 0.0013°
γ	90°
Cell volume	4594.51 ± 0.18 Å³
Cell temperature	110 ± 2 K
Ambient diffraction temperature	110 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.1064
Residual factor for significantly intense reflections	0.0487
Weighted residual factors for significantly intense reflections	0.1076
Weighted residual factors for all reflections included in the refinement	0.1204
Goodness-of-fit parameter for all reflections included in the refinement	0.914
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179500 (current)	2016-03-23	cif/4/33/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 4/33/97.	4339737.cif
117510	2014-06-15	cif/ Adding structures of 4339737, 4339738, 4339739, 4339740, 4339741, 4339742, 4339743 via cif-deposit CGI script.	4339737.cif