Crystallography Open Database

Information card for entry 4343324

Preview

Coordinates	4343324.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	Fe14 Ge4 H290 Na24 O311 P6 Rb4 W36
Calculated formula	Fe14 Ge4 Na14 O201 P4 Rb7 W36
Title of publication	Tetradecanuclear Iron(III)-Oxo Nanoclusters Stabilized by Trilacunary Heteropolyanions.
Authors of publication	Ibrahim, Masooma; Haider, Ali; Xiang, Yixian; Bassil, Bassem S.; Carey, Akina M.; Rullik, Lisa; Jameson, Geoffrey B.; Doungmene, Floriant; Mbomekallé, Israël M; Oliveira, Pedro de; Mereacre, Valeriu; Kostakis, George E.; Powell, Annie K.; Kortz, Ulrich
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	13
Pages of publication	6136 - 6146
a	22.69 ± 0.002 Å
b	27.943 ± 0.003 Å
c	18.793 ± 0.002 Å
α	90°
β	90°
γ	90°
Cell volume	11915 ± 2 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	8
Space group number	59
Hermann-Mauguin space group symbol	P m m n
Hall space group symbol	-P 2ab 2a
Residual factor for all reflections	0.0712
Residual factor for significantly intense reflections	0.066
Weighted residual factors for significantly intense reflections	0.1596
Weighted residual factors for all reflections included in the refinement	0.1626
Goodness-of-fit parameter for all reflections included in the refinement	1.072
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176429 (current)	2016-02-13	cif/ (antanas@kurmis) Replacing _cod_chemical_formula_sum_orig tag with _cod_original_formula_sum tag in multiple entries since the replaced tag is deprecated according to the COD CIF dictionary.	4343324.cif
141321	2015-07-08	cif/ Updating files of 4343322, 4343323, 4343324 Original log message: Adding full bibliography for 4343322--4343324.cif.	4343324.cif
139160	2015-06-14	cif/ Adding structures of 4343324 via cif-deposit CGI script.	4343324.cif