Crystallography Open Database

Information card for entry 4343340

Preview

Coordinates	4343340.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C33 H39 Cl4 N O5 Ru
Calculated formula	C33 H39 Cl3.992 N O5 Ru
Title of publication	Synthesis and Antiproliferative Activity of New Ruthenium Complexes with Ethacrynic-Acid-Modified Pyridine and Triphenylphosphine Ligands.
Authors of publication	Agonigi, Gabriele; Riedel, Tina; Zacchini, Stefano; Păunescu, Emilia; Pampaloni, Guido; Bartalucci, Niccolò; Dyson, Paul J.; Marchetti, Fabio
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	13
Pages of publication	6504 - 6512
a	14.2454 ± 0.0011 Å
b	10.6848 ± 0.0008 Å
c	23.3046 ± 0.0018 Å
α	90°
β	98.582 ± 0.001°
γ	90°
Cell volume	3507.5 ± 0.5 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	6
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/c 1
Hall space group symbol	-P 2ybc
Residual factor for all reflections	0.063
Residual factor for significantly intense reflections	0.0479
Weighted residual factors for significantly intense reflections	0.141
Weighted residual factors for all reflections included in the refinement	0.1574
Goodness-of-fit parameter for all reflections included in the refinement	1.039
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	4343340.cif
141345	2015-07-08	cif/ Updating files of 4343340 Original log message: Adding full bibliography for 4343340.cif.	4343340.cif
139223	2015-06-16	cif/ Adding structures of 4343340 via cif-deposit CGI script.	4343340.cif