Crystallography Open Database

Information card for entry 4344099

Preview

Coordinates	4344099.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H50 N2 Si Sr
Calculated formula	C30 H50 N2 Si Sr
Title of publication	Alkaline-Earth-Metal-Induced Liberation of Rare Allotropes of Elemental Silicon and Germanium from N-Heterocyclic Metallylenes.
Authors of publication	Blom, Burgert; Said, Amro; Szilvási, Tibor; Menezes, Prashanth W.; Tan, Gengwen; Baumgartner, Judith; Driess, Matthias
Journal of publication	Inorganic chemistry
Year of publication	2015
Journal volume	54
Journal issue	17
Pages of publication	8840 - 8848
a	19.5728 ± 0.0014 Å
b	21.5363 ± 0.0009 Å
c	15.4426 ± 0.0006 Å
α	90°
β	90°
γ	90°
Cell volume	6509.5 ± 0.6 Å³
Cell temperature	150 ± 2 K
Ambient diffraction temperature	150 ± 2 K
Number of distinct elements	5
Space group number	60
Hermann-Mauguin space group symbol	P b c n
Hall space group symbol	-P 2n 2ab
Residual factor for all reflections	0.1806
Residual factor for significantly intense reflections	0.0997
Weighted residual factors for significantly intense reflections	0.23
Weighted residual factors for all reflections included in the refinement	0.288
Goodness-of-fit parameter for all reflections included in the refinement	1.115
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
176428 (current)	2016-02-13	Replaced deprecated COD CIF data names with their more modern alternatives. The _cod_cif_authors_sg_Hall and _cod_cif_authors_sg_H-M data items were renamed to _cod_original_sg_symbol_Hall and _cod_cif_authors_sg_H-M respectively.	4344099.cif
160524	2015-10-06	cif/ Updating files of 4344097, 4344098, 4344099 Original log message: Adding full bibliography for 4344097--4344099.cif.	4344099.cif
153683	2015-08-27	cif/ Adding structures of 4344099 via cif-deposit CGI script.	4344099.cif