#------------------------------------------------------------------------------ #$Date: 2016-03-24 14:32:51 +0200 (Thu, 24 Mar 2016) $ #$Revision: 179667 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/20/4512072.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4512072 loop_ _publ_author_name '\/Oien, Sigurd' 'Wragg, David' 'Reinsch, Helge' 'Svelle, Stian' 'Bordiga, Silvia' 'Lamberti, Carlo' 'Lillerud, Karl Petter' _publ_section_title ; Detailed Structure Analysis of Atomic Positions and Defects in Zirconium Metal--Organic Frameworks ; _journal_issue 11 _journal_name_full 'Crystal Growth & Design' _journal_page_first 5370 _journal_paper_doi 10.1021/cg501386j _journal_volume 14 _journal_year 2014 _chemical_formula_moiety 'n[(C34.94 H17.47 O32 Zr6), 29.74(O)]' _chemical_formula_sum 'C34.94 H17.47 O61.74 Zr6' _chemical_formula_weight 1972.51 _chemical_name_common UiO-66 _chemical_name_systematic ; Zr(IV) terephthalate metal-organic framework ; _space_group_crystal_system cubic _space_group_IT_number 225 _space_group_name_Hall '-F 4 2 3' _space_group_name_H-M_alt 'F m -3 m' _symmetry_space_group_name_Hall '-F 4 2 3' _symmetry_space_group_name_H-M 'F m -3 m' _atom_sites_solution_hydrogens geom _audit_creation_date 2014-04-30 _audit_creation_method ; Olex2 1.2 (compiled 2014.03.20 svn.r2914 for OlexSys, GUI svn.r4816) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 20.7465(2) _cell_length_b 20.7465(2) _cell_length_c 20.7465(2) _cell_measurement_reflns_used 6384 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 33.645 _cell_measurement_theta_min 2.970 _cell_volume 8929.65(15) _computing_cell_refinement 'APEX2 v2013.6--2 (Bruker AXS)' _computing_data_collection 'APEX2 v2013.6--2 (Bruker AXS)' _computing_data_reduction 'SAINT v8.34A (Bruker, 2013)' _computing_molecular_graphics 'Diamond v3.2i (Brandenburg, 2012)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'APEX2 v2013.6--2 (Bruker AXS)' _diffrn_ambient_temperature 100.0 _diffrn_detector 'CCD area detector' _diffrn_detector_area_resol_mean 13.6986 _diffrn_detector_type 'Marmosaic 225' _diffrn_measured_fraction_theta_full 0.987 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_device '\k-geometry diffractometer' _diffrn_measurement_device_type 'MD2 microdiffractometer with MK3 mini-kappa' _diffrn_measurement_method '\f scans' _diffrn_radiation_collimation 'Rh-coated Si focusing mirrors' _diffrn_radiation_monochromator 'Silicon 111' _diffrn_radiation_probe x-ray _diffrn_radiation_type synchrotron _diffrn_radiation_wavelength 0.760 _diffrn_reflns_av_R_equivalents 0.0370 _diffrn_reflns_av_unetI/netI 0.0168 _diffrn_reflns_Laue_measured_fraction_full 0.987 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_limit_h_max 29 _diffrn_reflns_limit_h_min -28 _diffrn_reflns_limit_k_max 22 _diffrn_reflns_limit_k_min -27 _diffrn_reflns_limit_l_max 27 _diffrn_reflns_limit_l_min -29 _diffrn_reflns_number 12999 _diffrn_reflns_point_group_measured_fraction_full 0.987 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_theta_full 27.129 _diffrn_reflns_theta_max 32.828 _diffrn_reflns_theta_min 2.970 _diffrn_source synchrotron _diffrn_source_type 'Wiggler, Station I911-3, MAX II, MAXLAB' _exptl_absorpt_coefficient_mu 0.928 _exptl_absorpt_correction_T_max 0.7467 _exptl_absorpt_correction_T_min 0.6050 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details ; SADABS-2012/1 (Bruker,2012) was used for absorption correction. wR2(int) was 0.0651 before and 0.0499 after correction. The Ratio of minimum to maximum transmission is 0.8102. The \l/2 correction factor is 0.0015. ; _exptl_crystal_colour 'clear colourless' _exptl_crystal_colour_lustre clear _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.443 _exptl_crystal_description octahedral _exptl_crystal_F_000 3779 _exptl_crystal_size_max 0.01 _exptl_crystal_size_mid 0.01 _exptl_crystal_size_min 0.01 _refine_diff_density_max 0.395 _refine_diff_density_min -0.370 _refine_diff_density_rms 0.078 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.113 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 53 _refine_ls_number_reflns 739 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.113 _refine_ls_R_factor_all 0.0244 _refine_ls_R_factor_gt 0.0233 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0456P)^2^+20.2522P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0710 _refine_ls_wR_factor_ref 0.0714 _reflns_Friedel_coverage 0.000 _reflns_number_gt 701 _reflns_number_total 739 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cg501386j_si_001.cif _cod_data_source_block 66cpub_a _cod_depositor_comments 'Adding full bibliography for 4512072--4512074.cif.' _cod_original_cell_volume 8929.7(3) _cod_database_code 4512072 #BEGIN Tags that were not found in dictionaries: _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups 2. Others Sof(O1A)=0.16667*(1-FVAR(2)) Sof(O1B)=0.16667*FVAR(2) Sof(O2B)=0.5*(1-FVAR(3)) Sof(C2)=Sof(C1)=0.25*FVAR(3) Sof(O2A)=Sof(C3)=Sof(H3)=0.5*FVAR(3) 3.a Aromatic/amide H refined with riding coordinates: C3(H3) ; _shelx_res_file ; TITL 66Cpub in Fm-3m CELL 0.76 20.7465 20.7465 20.7465 90 90 90 ZERR 4 0.0002 0.0002 0.0002 0 0 0 LATT 4 SYMM -X,-Y,+Z SYMM -X,+Y,-Z SYMM +X,-Y,-Z SYMM +Z,+X,+Y SYMM +Z,-X,-Y SYMM -Z,-X,+Y SYMM -Z,+X,-Y SYMM +Y,+Z,+X SYMM -Y,+Z,-X SYMM +Y,-Z,-X SYMM -Y,-Z,+X SYMM +Y,+X,-Z SYMM -Y,-X,-Z SYMM +Y,-X,+Z SYMM -Y,+X,+Z SYMM +X,+Z,-Y SYMM -X,+Z,+Y SYMM -X,-Z,-Y SYMM +X,-Z,+Y SYMM +Z,+Y,-X SYMM +Z,-Y,+X SYMM -Z,+Y,+X SYMM -Z,-Y,-X SFAC C H O Zr DISP C 0.004 0.002 13.247 DISP H -0 0 0.627 DISP O 0.014 0.007 38.676 DISP Zr -1.967 0.657 2986.787 UNIT 135.56544 67.78272 242.21952 24 L.S. 50 PLAN 20 TEMP -173.15 REM Solution 1 R1 0.126 Rweak 0.010, Alpha = 0.0511 in Fm-3m BOND BOND $H LIST 4 MORE -1 CONF fmap 2 acta SHEL 999 0.7 REM D:/frames/guest/SOE_Lund_1747full/work/66Cpub_a.hkl WGHT 0.045600 20.252201 FVAR 0.13774 0.53542 0.72693 ZR1 4 0.000000 0.000000 0.119748 10.12500 0.01006 0.01006 = 0.00498 0.00000 0.00000 0.00000 PART 2 O1B 3 -0.067367 -0.067367 0.067367 20.16667 0.01516 0.01516 = 0.01516 0.00203 0.00203 -0.00203 PART 0 PART 1 O2A 3 0.093954 0.000000 0.170228 30.50000 0.01470 0.03634 = 0.00952 0.00000 -0.00520 0.00000 PART 0 O3 3 -0.151092 -0.151092 0.151092 0.09259 0.25736 0.25736 = 0.25736 0.04831 0.04831 -0.04831 O4 3 -0.210849 -0.210849 0.210849 10.16667 0.77697 0.77697 = 0.77697 0.28323 0.28323 -0.28323 PART 2 O2B 3 0.082528 0.000000 0.188245 -30.50000 0.05199 0.02321 = 0.02949 0.00000 -0.02968 0.00000 PART 0 PART 1 C2 1 0.202791 0.000000 0.202791 30.25000 0.01430 0.05448 = 0.01430 0.00000 -0.01092 0.00000 C3 1 0.267124 0.000000 0.185342 30.50000 0.01617 0.13088 = 0.01511 0.00000 -0.00783 0.00000 AFIX 43 H3 2 0.278907 0.000000 0.141094 30.50000 -1.20000 AFIX 0 O1A 3 -0.050478 -0.050478 0.050478 -20.16667 0.00557 0.00557 = 0.00557 0.00026 0.00026 -0.00026 C1 1 0.151795 0.000000 0.151795 30.25000 0.01197 0.02998 = 0.01197 0.00000 -0.00799 0.00000 PART 0 O6 3 0.396496 0.103504 0.103504 0.13303 0.71996 0.71996 = 0.71996 0.38990 -0.38990 -0.38990 O5 3 0.373414 0.000000 0.000000 0.22727 0.57711 1.44807 = 1.44807 0.00000 0.00000 0.00000 HKLF 4 REM 66Cpub in Fm-3m REM R1 = 0.0233 for 701 Fo > 4sig(Fo) and 0.0244 for all 739 data REM 53 parameters refined using 0 restraints END WGHT 0.0433 23.4769 REM Highest difference peak 0.395, deepest hole -0.370, 1-sigma level 0.078 Q1 1 -0.2500 -0.2500 0.1704 10.25000 0.05 0.37 Q2 1 0.1678 -0.0723 0.1678 10.50000 0.05 0.34 Q3 1 0.3318 0.0000 0.0000 10.12500 0.05 0.33 Q4 1 -0.1820 -0.1820 0.1820 10.16667 0.05 0.31 Q5 1 0.0288 0.0000 0.1391 10.50000 0.05 0.30 Q6 1 -0.0922 -0.0922 0.0922 10.16667 0.05 0.28 Q7 1 0.1816 0.0000 0.1816 10.25000 0.05 0.27 Q8 1 0.1927 0.0000 0.2306 10.50000 0.05 0.26 Q9 1 -0.2319 -0.1251 0.1251 10.50000 0.05 0.25 Q10 1 0.0260 0.0260 0.1030 10.50000 0.05 0.25 Q11 1 -0.0639 -0.0381 0.0639 10.50000 0.05 0.24 Q12 1 -0.1655 -0.2003 0.1655 10.50000 0.05 0.24 Q13 1 -0.0312 0.0000 0.0964 10.50000 0.05 0.24 Q14 1 0.1100 0.0385 0.2143 11.00000 0.05 0.23 Q15 1 0.2775 0.0400 0.1308 11.00000 0.05 0.23 Q16 1 0.3800 0.0510 0.0510 10.50000 0.05 0.22 Q17 1 -0.1681 -0.1151 0.1681 10.50000 0.05 0.21 Q18 1 -0.0411 -0.0411 0.0411 10.16667 0.05 0.21 Q19 1 0.4142 0.0000 -0.0725 10.50000 0.05 0.20 Q20 1 0.1904 -0.0411 0.1904 10.50000 0.05 0.19 REM The information below was added by Olex2. REM REM R1 = 0.0233 for 701 Fo > 4sig(Fo) and 0.0244 for all 13152 data REM n/a parameters refined using n/a restraints REM Highest difference peak 0.40, deepest hole -0.37 REM Mean Shift 0, Max Shift 0.000. REM +++ Tabular Listing of Refinement Information +++ REM R1_all = 0.0244 REM R1_gt = 0.0233 REM wR_ref = 0.0714 REM GOOF = 1.113 REM Shift_max = 0.000 REM Shift_mean = 0 REM Reflections_all = 13152 REM Reflections_gt = 701 REM Parameters = n/a REM Hole = -0.37 REM Peak = 0.40 REM Flack = n/a ; #END Tags that were not found in dictionaries loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, z' '-x, y, -z' 'x, -y, -z' 'z, x, y' 'z, -x, -y' '-z, -x, y' '-z, x, -y' 'y, z, x' '-y, z, -x' 'y, -z, -x' '-y, -z, x' 'y, x, -z' '-y, -x, -z' 'y, -x, z' '-y, x, z' 'x, z, -y' '-x, z, y' '-x, -z, -y' 'x, -z, y' 'z, y, -x' 'z, -y, x' '-z, y, x' '-z, -y, -x' 'x, y+1/2, z+1/2' '-x, -y+1/2, z+1/2' '-x, y+1/2, -z+1/2' 'x, -y+1/2, -z+1/2' 'z, x+1/2, y+1/2' 'z, -x+1/2, -y+1/2' '-z, -x+1/2, y+1/2' '-z, x+1/2, -y+1/2' 'y, z+1/2, x+1/2' '-y, z+1/2, -x+1/2' 'y, -z+1/2, -x+1/2' '-y, -z+1/2, x+1/2' 'y, x+1/2, -z+1/2' '-y, -x+1/2, -z+1/2' 'y, -x+1/2, z+1/2' '-y, x+1/2, z+1/2' 'x, z+1/2, -y+1/2' '-x, z+1/2, y+1/2' '-x, -z+1/2, -y+1/2' 'x, -z+1/2, y+1/2' 'z, y+1/2, -x+1/2' 'z, -y+1/2, x+1/2' '-z, y+1/2, x+1/2' '-z, -y+1/2, -x+1/2' 'x+1/2, y, z+1/2' '-x+1/2, -y, z+1/2' '-x+1/2, y, -z+1/2' 'x+1/2, -y, -z+1/2' 'z+1/2, x, y+1/2' 'z+1/2, -x, -y+1/2' '-z+1/2, -x, y+1/2' '-z+1/2, x, -y+1/2' 'y+1/2, z, x+1/2' '-y+1/2, z, -x+1/2' 'y+1/2, -z, -x+1/2' '-y+1/2, -z, x+1/2' 'y+1/2, x, -z+1/2' '-y+1/2, -x, -z+1/2' 'y+1/2, -x, z+1/2' '-y+1/2, x, z+1/2' 'x+1/2, z, -y+1/2' '-x+1/2, z, y+1/2' '-x+1/2, -z, -y+1/2' 'x+1/2, -z, y+1/2' 'z+1/2, y, -x+1/2' 'z+1/2, -y, x+1/2' '-z+1/2, y, x+1/2' '-z+1/2, -y, -x+1/2' 'x+1/2, y+1/2, z' '-x+1/2, -y+1/2, z' '-x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, -z' 'z+1/2, x+1/2, y' 'z+1/2, -x+1/2, -y' '-z+1/2, -x+1/2, y' '-z+1/2, x+1/2, -y' 'y+1/2, z+1/2, x' '-y+1/2, z+1/2, -x' 'y+1/2, -z+1/2, -x' '-y+1/2, -z+1/2, x' 'y+1/2, x+1/2, -z' '-y+1/2, -x+1/2, -z' 'y+1/2, -x+1/2, z' '-y+1/2, x+1/2, z' 'x+1/2, z+1/2, -y' '-x+1/2, z+1/2, y' '-x+1/2, -z+1/2, -y' 'x+1/2, -z+1/2, y' 'z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, x' '-z+1/2, y+1/2, x' '-z+1/2, -y+1/2, -x' '-x, -y, -z' 'x, y, -z' 'x, -y, z' '-x, y, z' '-z, -x, -y' '-z, x, y' 'z, x, -y' 'z, -x, y' '-y, -z, -x' 'y, -z, x' '-y, z, x' 'y, z, -x' '-y, -x, z' 'y, x, z' '-y, x, -z' 'y, -x, -z' '-x, -z, y' 'x, -z, -y' 'x, z, y' '-x, z, -y' '-z, -y, x' '-z, y, -x' 'z, -y, -x' 'z, y, x' '-x, -y+1/2, -z+1/2' 'x, y+1/2, -z+1/2' 'x, -y+1/2, z+1/2' '-x, y+1/2, z+1/2' '-z, -x+1/2, -y+1/2' '-z, x+1/2, y+1/2' 'z, x+1/2, -y+1/2' 'z, -x+1/2, y+1/2' '-y, -z+1/2, -x+1/2' 'y, -z+1/2, x+1/2' '-y, z+1/2, x+1/2' 'y, z+1/2, -x+1/2' '-y, -x+1/2, z+1/2' 'y, x+1/2, z+1/2' '-y, x+1/2, -z+1/2' 'y, -x+1/2, -z+1/2' '-x, -z+1/2, y+1/2' 'x, -z+1/2, -y+1/2' 'x, z+1/2, y+1/2' '-x, z+1/2, -y+1/2' '-z, -y+1/2, x+1/2' '-z, y+1/2, -x+1/2' 'z, -y+1/2, -x+1/2' 'z, y+1/2, x+1/2' '-x+1/2, -y, -z+1/2' 'x+1/2, y, -z+1/2' 'x+1/2, -y, z+1/2' '-x+1/2, y, z+1/2' '-z+1/2, -x, -y+1/2' '-z+1/2, x, y+1/2' 'z+1/2, x, -y+1/2' 'z+1/2, -x, y+1/2' '-y+1/2, -z, -x+1/2' 'y+1/2, -z, x+1/2' '-y+1/2, z, x+1/2' 'y+1/2, z, -x+1/2' '-y+1/2, -x, z+1/2' 'y+1/2, x, z+1/2' '-y+1/2, x, -z+1/2' 'y+1/2, -x, -z+1/2' '-x+1/2, -z, y+1/2' 'x+1/2, -z, -y+1/2' 'x+1/2, z, y+1/2' '-x+1/2, z, -y+1/2' '-z+1/2, -y, x+1/2' '-z+1/2, y, -x+1/2' 'z+1/2, -y, -x+1/2' 'z+1/2, y, x+1/2' '-x+1/2, -y+1/2, -z' 'x+1/2, y+1/2, -z' 'x+1/2, -y+1/2, z' '-x+1/2, y+1/2, z' '-z+1/2, -x+1/2, -y' '-z+1/2, x+1/2, y' 'z+1/2, x+1/2, -y' 'z+1/2, -x+1/2, y' '-y+1/2, -z+1/2, -x' 'y+1/2, -z+1/2, x' '-y+1/2, z+1/2, x' 'y+1/2, z+1/2, -x' '-y+1/2, -x+1/2, z' 'y+1/2, x+1/2, z' '-y+1/2, x+1/2, -z' 'y+1/2, -x+1/2, -z' '-x+1/2, -z+1/2, y' 'x+1/2, -z+1/2, -y' 'x+1/2, z+1/2, y' '-x+1/2, z+1/2, -y' '-z+1/2, -y+1/2, x' '-z+1/2, y+1/2, -x' 'z+1/2, -y+1/2, -x' 'z+1/2, y+1/2, x' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_group Zr1 Zr 0.0000 0.0000 0.11975(2) 0.00837(13) Uani 1 8 d S T P . O1B O -0.0674(5) -0.0674(5) 0.0674(5) 0.015(2) Uani 0.54(4) 6 d S T P 2 O2A O 0.0940(2) 0.0000 0.17023(19) 0.0202(7) Uani 0.727(7) 2 d S T P 1 O3 O -0.1511(7) -0.1511(7) 0.1511(7) 0.26(2) Uani 0.56(4) 6 d S T P . O4 O -0.2108(7) -0.2108(7) 0.2108(7) 0.78(4) Uani 1 6 d S T P . O2B O 0.0825(8) 0.0000 0.1882(6) 0.035(3) Uani 0.273(7) 2 d S T P 2 C2 C 0.20279(12) 0.0000 0.20279(12) 0.0277(10) Uani 0.727(7) 4 d S T P 1 C3 C 0.26712(15) 0.0000 0.18534(15) 0.0541(14) Uani 0.727(7) 2 d S T P 1 H3 H 0.2789 0.0000 0.1411 0.065 Uiso 0.727(7) 2 calc RS T P 1 O1A O -0.0505(5) -0.0505(5) 0.0505(5) 0.006(2) Uani 0.46(4) 6 d S T P 1 C1 C 0.15179(11) 0.0000 0.15179(11) 0.0180(8) Uani 0.727(7) 4 d S T P 1 O6 O 0.396(3) 0.104(3) 0.104(3) 0.72(9) Uani 0.80(11) 6 d S T P . O5 O 0.373(2) 0.0000 0.0000 1.16(13) Uani 1.8(3) 8 d S T P . loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zr1 0.01006(14) 0.01006(14) 0.00498(16) 0.000 0.000 0.000 O1B 0.015(2) 0.015(2) 0.015(2) 0.002(2) 0.002(2) -0.002(2) O2A 0.0147(11) 0.0363(15) 0.0095(16) 0.000 -0.0052(11) 0.000 O3 0.26(2) 0.26(2) 0.26(2) 0.048(12) 0.048(12) -0.048(12) O4 0.78(4) 0.78(4) 0.78(4) 0.28(3) 0.28(3) -0.28(3) O2B 0.052(9) 0.023(4) 0.029(7) 0.000 -0.030(5) 0.000 C2 0.0143(11) 0.054(3) 0.0143(11) 0.000 -0.0109(13) 0.000 C3 0.0162(14) 0.131(4) 0.0151(14) 0.000 -0.0078(11) 0.000 O1A 0.006(2) 0.006(2) 0.006(2) 0.000(2) 0.000(2) 0.000(2) C1 0.0120(10) 0.0300(19) 0.0120(10) 0.000 -0.0080(11) 0.000 O6 0.72(9) 0.72(9) 0.72(9) 0.39(9) -0.39(9) -0.39(9) O5 0.58(9) 1.45(17) 1.45(17) 0.000 0.000 0.000 loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0040 0.0020 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0140 0.0070 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zr Zr -1.9670 0.6570 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O2A Zr1 O2A 123.50(17) 110 109 O2A Zr1 O2A 123.50(17) 2 . O2A Zr1 O2A 77.05(7) 109 . O2A Zr1 O2A 77.05(7) 109 2 O2A Zr1 O2A 77.05(7) 110 . O2A Zr1 O2A 77.05(7) 110 2 O2B Zr1 O2B 65.9(4) . 109 O2B Zr1 O2B 65.9(4) 110 2 O2B Zr1 O2B 100.6(8) 110 109 O2B Zr1 O2B 100.6(8) . 2 O2B Zr1 O2B 65.9(4) . 110 O2B Zr1 O2B 65.9(4) 109 2 O1A Zr1 O2A 83.3(4) . 2 O1A Zr1 O2A 83.3(4) 100 109 O1A Zr1 O2A 83.3(4) 2 110 O1A Zr1 O2A 140.95(9) 100 110 O1A Zr1 O2A 83.3(4) 2 . O1A Zr1 O2A 140.95(9) 100 2 O1A Zr1 O2A 140.95(9) . 110 O1A Zr1 O2A 140.95(9) 2 109 O1A Zr1 O2A 83.3(4) . 109 O1A Zr1 O2A 140.95(9) 99 109 O1A Zr1 O2A 83.3(4) 99 2 O1A Zr1 O2A 83.3(4) 99 110 O1A Zr1 O2A 140.95(9) 2 2 O1A Zr1 O2A 83.3(4) 100 . O1A Zr1 O2A 140.95(9) 99 . O1A Zr1 O2A 140.95(9) . . O1A Zr1 O1A 61.0(6) 100 . O1A Zr1 O1A 61.0(6) 99 2 O1A Zr1 O1A 91.7(10) 100 99 O1A Zr1 O1A 61.0(6) 99 . O1A Zr1 O1A 91.7(10) 2 . O1A Zr1 O1A 61.0(6) 100 2 Zr1 O1B Zr1 102.3(5) . 101 Zr1 O1B Zr1 102.3(5) . 105 Zr1 O1B Zr1 102.3(5) 105 101 C1 O2A Zr1 134.1(3) . . C3 C2 C3 120.3(3) . 22 C3 C2 C1 119.82(17) . . C3 C2 C1 119.83(17) 22 . C2 C3 C3 119.83(17) . 166 C2 C3 H3 120.1 . . C3 C3 H3 120.1 166 . Zr1 O1A Zr1 116.7(3) 105 101 Zr1 O1A Zr1 116.7(3) . 101 Zr1 O1A Zr1 116.7(3) . 105 O2A C1 O2A 125.4(5) . 22 O2A C1 C2 117.3(2) 22 . O2A C1 C2 117.3(2) . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Zr1 O2A 2.213(5) 110 Zr1 O2A 2.213(5) 2 Zr1 O2A 2.213(5) 109 Zr1 O2A 2.213(5) . Zr1 O2B 2.225(15) . Zr1 O2B 2.225(15) 109 Zr1 O2B 2.225(15) 110 Zr1 O2B 2.225(15) 2 Zr1 O1A 2.064(3) 100 Zr1 O1A 2.064(3) . Zr1 O1A 2.064(3) 99 Zr1 O1A 2.064(3) 2 O1B Zr1 2.256(8) 101 O1B Zr1 2.256(8) 105 O2A C1 1.259(4) . C2 C3 1.383(4) 22 C2 C3 1.383(4) . C2 C1 1.496(5) . C3 C3 1.395(6) 166 C3 H3 0.9500 . O1A Zr1 2.064(3) 105 O1A Zr1 2.064(3) 101 C1 O2A 1.260(4) 22 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 _geom_torsion_site_symmetry_4 Zr1 O2A C1 O2A 0.000(0) . 22 Zr1 O2A C1 C2 180.000(0) . . C3 C2 C3 C3 0.000(0) 22 166 C3 C2 C1 O2A 0.000(0) 22 . C3 C2 C1 O2A 0.000(0) . 22 C3 C2 C1 O2A 180.000(0) 22 22 C3 C2 C1 O2A 180.000(0) . . C1 C2 C3 C3 180.000(0) . 166 loop_ _refln_index_h _refln_index_k _refln_index_l _refln_F_squared_meas _refln_F_squared_sigma -2 -2 0 2177.38 105.19 0 -2 2 2395.06 105.19 0 2 -2 2192.98 105.19 2 0 -2 2512.55 105.29 -2 -2 2 1503.15 65.99 2 2 -2 1406.86 65.99 2 2 2 1447.46 65.89 -3 -1 -1 286.97 13.9 -3 1 1 313.87 14.1 -1 -3 -1 280.27 14 -1 -3 1 281.97 14.1 -1 1 -3 305.47 13.8 1 -1 -3 310.07 14 1 -1 3 283.17 13.8 1 1 -3 312.07 14 3 -1 -1 321.57 14.1 3 -1 1 321.17 14 3 1 -1 303.37 14.1 3 1 1 304.57 13.9 -3 -3 -1 794.72 36.1 -3 -3 1 769.82 36.2 -3 -1 -3 753.72 35.8 -3 -1 3 758.02 36.2 -3 1 3 903.91 36.3 -1 -3 3 737.83 36.2 -1 3 -3 782.62 36.1 1 -3 3 771.42 36.1 1 3 -3 743.13 36.1 3 -1 -3 795.62 36.3 3 1 -3 822.12 36.3 3 1 3 839.02 35.9 3 3 -1 764.42 36.2 3 3 1 824.22 36.2 -3 -3 -3 1068.99 49 -3 -3 3 1042.8 49.2 3 3 -3 1090.69 49.3 -4 0 -2 1253.17 57.39 -4 0 2 1236.28 57.59 -2 -4 0 1157.78 57.59 0 2 -4 1273.87 57.49 2 4 0 1235.48 57.59 4 0 -2 1317.87 57.69 4 0 2 1239.98 57.39 -4 -2 0 1297.17 57.59 -2 0 4 1280.17 57.59 0 -4 2 1264.67 57.59 0 4 -2 1233.18 57.59 2 0 -4 1234.88 57.59 4 2 0 1404.16 57.59 -4 -2 -2 573.74 24.4 -2 -4 -2 469.75 24.5 -2 -4 2 519.85 24.6 -2 -2 4 552.34 24.6 -2 2 -4 482.45 24.3 2 -2 -4 553.64 24.7 2 -2 4 521.55 24.3 2 2 -4 527.05 24.6 4 -2 -2 615.74 24.8 4 2 2 500.95 24.4 -4 -4 0 1455.55 68.69 -4 0 4 1496.65 68.79 0 -4 4 1447.76 68.69 0 4 -4 1590.04 68.69 4 0 -4 1592.24 68.89 4 4 0 1415.96 68.69 -4 -4 2 3719.73 193.48 -4 -2 4 4134.89 193.58 -2 -4 4 4179.78 193.48 2 -4 4 4308.27 193.38 2 4 -4 4220.28 193.48 4 -2 -4 4705.53 193.68 4 2 -4 4263.87 193.58 4 4 -2 4613.94 193.58 -5 -1 -1 1834.52 83.59 -5 -1 1 1744.73 83.69 -5 1 1 1893.41 83.79 -1 -5 -1 1782.92 83.69 -1 -5 1 1836.42 83.69 -1 -1 -5 1843.72 83.49 -1 -1 5 1718.53 83.59 -1 1 -5 2086.99 83.39 1 -1 -5 1830.72 83.59 1 -1 5 1853.21 83.39 1 1 -5 1893.81 83.59 1 5 -1 1762.22 83.69 5 -1 -1 1820.02 83.69 5 -1 1 1871.61 83.59 5 1 -1 1819.42 83.69 -5 -1 -3 977.2 43.7 5 1 -3 1008.7 44.1 -5 1 3 1030.3 44.2 -3 -5 -1 920.71 44 -5 -3 1 967.4 44 -3 -1 5 1024 44.1 5 3 1 973.5 43.9 1 -3 5 1006.4 43.8 1 3 -5 921.01 43.9 3 5 -1 897.11 44 3 -1 -5 984.9 44.1 5 -1 3 1030.8 43.7 -5 -1 3 1065.89 44.2 5 -1 -3 993.9 44.1 -5 -3 -1 825.82 43.9 -3 -5 1 957 44.1 -1 -3 5 933.21 43.9 -3 1 5 984.2 44.1 1 -5 3 961.2 44 5 1 3 1028.9 43.7 3 -1 5 781.02 43.5 3 1 -5 986.4 44.1 5 3 -1 1034.5 44.1 -1 3 -5 766.92 43.7 -5 -3 -3 1322.67 56.29 -5 -3 3 1261.77 56.59 -3 -5 -3 1205.08 56.49 -3 -5 3 1276.67 56.59 -3 -3 5 1294.47 56.59 3 -3 5 1156.08 56.19 3 3 -5 1201.48 56.49 3 5 -3 1239.78 56.59 5 -3 -3 1288.67 56.69 5 3 -3 1169.38 56.59 5 3 3 1181.68 56.29 -5 -5 -1 1652.23 76.49 -5 -5 1 1670.33 76.59 -5 -1 -5 1696.93 75.89 -5 -1 5 1707.93 76.59 -5 1 5 1697.83 76.59 -1 -5 5 1621.24 76.49 -1 5 -5 1623.64 76.39 1 -5 5 1711.13 76.39 1 5 -5 1666.23 76.49 5 -1 -5 1785.92 76.69 5 1 -5 1668.63 76.59 5 5 -1 1629.64 76.49 5 5 1 1658.93 76.49 -5 -5 3 4330.07 202.78 -5 -3 5 4496.45 202.78 -3 -5 -5 4499.55 202.48 -3 -5 5 4594.34 202.78 3 -5 5 4510.45 202.48 3 5 -5 4601.14 202.78 5 3 -5 4216.28 202.68 5 5 -3 4207.98 202.68 5 5 3 4754.32 202.68 -6 0 -2 49.1 3.1 -6 0 2 53.39 3.7 -2 -6 0 42.7 3.3 0 -2 -6 42.5 3 0 -2 6 45.5 3.1 0 2 -6 35.9 2.9 2 6 0 46.6 3.4 6 0 -2 46.4 3.5 6 0 2 44.8 3 6 -2 0 43.8 3.3 6 2 0 52.39 3.5 -2 0 6 42.3 3.2 0 -6 2 51.69 3.7 0 6 -2 53.89 3.6 -2 0 -6 45.1 2.5 -6 -2 0 46.7 3.3 2 -2 -6 122.99 6.9 -2 -2 6 125.69 6.9 2 2 -6 116.79 6.8 6 -2 2 121.79 6.7 6 2 -2 115.69 6.9 6 2 2 123.09 6.6 2 6 -2 115.79 7 6 -2 -2 120.59 7.1 -6 -2 -2 120.39 6.6 -6 -2 2 118.39 7 -2 -6 -2 119.79 6.9 -2 -6 2 117.59 7 2 -2 6 126.59 6.4 6 0 4 249.48 11.3 6 0 -4 249.58 11.9 4 6 0 235.88 11.9 -6 0 -4 231.98 11.3 -6 0 4 245.28 12.1 -4 -6 0 233.78 11.9 0 -4 6 237.68 11.7 0 4 -6 241.48 11.7 0 6 -4 251.27 11.9 4 0 -6 250.27 12 6 4 0 227.28 11.8 0 -6 4 245.18 11.9 -4 0 6 249.78 12 -6 -4 0 235.58 11.8 -4 -2 6 940.71 45.1 2 4 -6 979.5 45 4 6 -2 994.4 45.1 -6 -4 2 987.3 45.1 -2 -6 4 971.7 45.1 6 -2 4 959.8 44.6 6 2 -4 979 45.1 6 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45.3 12 -14 14 918.31 44.5 12 14 -14 946.91 44.9 14 -14 -12 944.91 45.2 14 -14 12 1005.3 44.8 14 -12 -14 936.41 45.2 14 -12 14 909.91 44 14 -12 14 918.81 44.3 14 12 -14 952.6 45 14 14 -12 936.81 44.9 -14 -14 -14 134.29 10.5 -14 -14 14 175.28 11.3 14 -14 -14 165.18 11.5 14 -14 14 149.19 10.3 14 14 -14 171.08 11.3 -15 -1 -1 1809.92 85.69 -15 -1 1 1805.82 85.79 -1 -15 -1 1772.12 85.79 -1 -15 1 1922.71 85.89 -1 -1 -15 1891.31 85.29 -1 -1 15 1850.11 85.59 -1 1 -15 1757.42 85.19 1 -15 -1 1775.42 85.79 1 -15 1 1920.51 85.89 1 -1 -15 2007.5 85.59 1 1 -15 1872.01 85.49 15 -1 -1 1931.21 85.89 15 -1 1 1872.31 85.69 15 1 -1 1902.01 85.79 15 1 1 1893.61 85.69 -15 -1 -3 9.1 3.1 15 3 1 3.7 2.9 -15 1 3 10.6 3.5 -3 -15 -1 5.8 3.1 -3 1 -15 7.6 1.9 -1 -3 -15 8.6 2.6 -1 -15 3 6.9 3 15 -3 -1 5.7 3.1 15 -1 3 7.2 2.7 1 -3 15 6.7 2.6 1 3 -15 6.4 2.6 1 -15 -3 10 3.3 3 -15 1 6.6 3.1 3 -1 -15 6.3 2.9 -3 -1 15 8.2 3.2 15 1 -3 7.3 3.3 -15 -3 1 7.1 3.2 -15 -3 -1 5.8 3 15 1 3 8.8 2.9 -3 -1 -15 8.2 1.9 1 -3 -15 6.6 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3.1 -5 -15 7 4.3 3.4 7 -15 5 5.9 3.3 -5 -7 -15 4.9 2.8 -15 -7 5 1.3 3.2 7 -5 -15 3.1 3.5 15 5 -7 3 3 -15 -5 -7 4.3 2.8 15 -5 7 3.6 2.7 -7 -15 -5 3.5 3.4 15 -7 -5 2.5 3.6 5 -7 15 3.3 2.4 5 7 -15 2.4 3.2 7 15 -5 4.6 3.3 -5 -7 15 3.7 3.5 -7 -5 -15 4.7 1.7 -15 -7 -5 4.5 3.2 -5 -15 -7 4.8 3.4 15 7 -5 6.5 3.7 -7 -5 -15 5 1.7 15 -5 -7 4.3 3.7 5 15 -7 7.9 3.4 -7 -15 5 4.8 2.7 5 -7 -15 7.5 3.7 5 -15 7 2.7 3.3 -15 -5 7 1.5 3.2 15 -7 5 3.8 3.3 15 5 7 3.3 2.8 7 5 -15 2.2 3.3 -7 -15 -7 868.81 39.8 15 7 -7 842.92 39.8 -15 -7 -7 775.72 39.3 -15 -7 7 877.01 40 7 7 -15 836.42 39.8 7 15 -7 889.21 39.9 15 -7 7 832.02 39.3 15 -7 -7 808.42 39.9 -7 -7 -15 859.01 38.9 -7 -7 15 875.21 40 7 -15 7 747.63 39.5 7 -7 -15 864.21 39.9 7 -7 15 873.21 38.6 -7 -15 7 866.11 39.8 15 7 7 796.82 39.3 -7 -7 -15 794.82 38.8 -9 -15 -1 848.62 39.9 15 -9 -1 776.12 39.9 15 9 1 783.52 39.7 9 15 -1 880.41 40 1 -9 15 804.82 39.5 -1 -15 9 859.01 39.9 15 -1 9 891.61 38.7 15 1 -9 868.01 39.9 9 -1 -15 834.72 39.8 -15 1 9 866.31 40.1 -9 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25.3 11 -15 -13 502.15 25.6 11 -13 15 520.65 24.6 11 13 -15 491.15 25.1 11 -13 -15 496.55 25.5 13 -15 -11 484.05 25.4 -13 -11 -15 439.66 24.3 15 -11 -13 477.85 25.3 -11 -15 -13 517.25 25.2 -13 -15 11 500.65 25.2 -15 -13 -11 465.15 25 11 -15 13 506.85 25 11 15 -13 506.65 25.1 -11 -13 15 522.35 25.4 13 -11 15 489.05 23.8 13 -11 15 508.15 24 13 11 -15 501.85 25.1 -15 -11 13 492.35 25.3 15 -13 11 471.75 24.8 15 13 -11 500.15 25.1 -15 -13 -13 628.14 30.6 -15 -13 13 622.84 30.8 -13 -15 -13 637.64 30.8 -13 -15 13 620.84 30.7 -13 -13 -15 556.64 30.2 -13 -13 15 635.64 30.9 13 -15 -13 642.34 30.9 13 -15 13 638.94 30.6 13 -13 -15 611.04 31 13 -13 15 597.74 29.9 13 13 -15 633.94 30.7 13 15 -13 650.13 30.7 15 -13 -13 607.04 31 15 -13 13 595.94 30.2 15 -13 13 637.44 30.6 15 13 -13 598.24 30.5 -15 -15 -1 916.51 42.9 -15 -15 1 905.01 42.8 -15 -1 15 897.81 43 -1 -15 15 872.11 42.7 1 -15 15 892.61 42.7 1 15 -15 852.21 42.7 15 -1 -15 893.81 42.8 15 1 -15 929.41 42.8 15 15 -1 909.11 42.9 15 15 1 896.91 42.8 -15 -15 -3 104.69 8.6 -15 -15 3 112.19 8.6 -15 -3 15 109.69 9.1 -3 -15 -15 117.79 8.8 -3 -15 15 105.29 8.6 3 -15 15 119.69 8.7 3 15 -15 122.49 8.8 15 -3 -15 114.29 8.9 15 3 -15 134.99 9.1 15 15 -3 129.19 9.1 15 15 3 101.49 8.6 -15 -15 -5 50.69 6.4 -15 -15 5 59.89 6.2 -15 -5 15 53.89 6.7 -5 -15 -15 45.6 6.3 -5 -15 15 47.7 6.3 5 -15 15 63.89 6.4 5 15 -15 59.99 6.4 15 -15 -5 49.3 6.6 15 -5 -15 57.99 6.6 15 5 -15 52.49 6.2 15 15 -5 53.19 6.1 -15 -15 -7 307.57 16.6 -15 -15 7 305.07 16.5 -15 -7 15 311.27 16.9 -7 -15 -15 275.97 16.7 -7 -15 15 319.57 16.8 7 -15 -15 293.37 17.1 7 -15 15 303.77 16.5 7 15 -15 309.67 16.9 15 -15 -7 286.67 17 15 -15 7 296.57 16.6 15 -7 -15 285.07 16.8 15 7 -15 307.67 16.6 15 15 -7 307.47 16.5 -15 -15 -9 819.52 38 -15 -15 9 784.52 37.9 -15 -9 -15 768.22 36.2 -15 -9 15 798.02 38 -9 -15 -15 758.12 37.7 -9 -15 15 791.72 38 9 -15 -15 798.22 38.4 9 -15 15 753.42 37.6 9 15 -15 785.82 37.9 15 -15 -9 757.22 38.1 15 -9 -15 758.62 38 15 9 -15 789.62 37.8 15 15 -9 812.72 37.9 -15 -15 -11 17.8 5.8 -15 -15 11 12.6 5.5 -15 -11 -15 13.4 4.9 -15 -11 15 18.2 5.6 -11 -15 -15 16.6 5.7 -11 -15 15 20.2 5.9 11 -15 -15 16.8 6.1 11 -15 15 20.8 5.6 11 15 -15 22.4 5.5 15 -15 -11 19.5 5.9 15 -15 11 22 5.8 15 -11 -15 27.9 6.1 15 -11 15 18.2 3.3 15 -11 15 16.6 3.5 15 11 -15 21.2 5.2 15 15 -11 18.5 5.4 -15 -15 -13 8 6.3 -15 -15 13 4.3 5.5 -15 -13 -15 3.6 5.7 -15 -13 15 6.3 5.4 -13 -15 -15 3.7 6.1 -13 -15 15 2.7 5.6 13 -15 -15 2.9 6.1 13 -15 15 4.6 5.5 13 15 -15 5.7 5.1 15 -15 -13 2.6 6 15 -15 13 1 5.9 15 -13 -15 7.6 5.8 15 -13 15 2.3 4.8 15 -13 15 5.7 5.6 15 13 -15 2.8 5.4 15 15 -13 4.5 5.3 -15 -15 15 675.43 33.7 15 -15 -15 662.13 33.9 15 -15 15 672.63 33.5 15 -15 15 681.73 34.4 15 15 -15 690.03 33.5 -16 0 0 5687.13 261.27 0 -16 0 5639.94 261.17 0 0 -16 5802.62 260.77 16 0 0 5850.61 261.17 -16 0 2 1543.05 71.29 -2 -16 0 1575.54 71.19 0 -2 -16 1537.75 70.79 0 -2 16 1507.85 70.79 0 2 -16 1554.74 70.69 2 -16 0 1488.85 71.09 16 0 -2 1484.45 71.09 16 0 2 1520.35 70.99 16 2 0 1546.55 71.09 16 -2 0 1559.74 71.19 -16 -2 0 1514.35 71.09 -2 0 -16 1655.83 70.49 0 -16 -2 1447.36 71.09 0 -16 2 1586.44 71.19 2 0 -16 1548.55 70.89 -2 -2 -16 806.32 37.4 -2 -16 2 847.52 38.2 16 -2 2 803.82 38 16 2 -2 804.12 38.1 16 2 2 793.92 37.9 -2 2 -16 791.02 37.4 2 -16 -2 812.02 38.1 2 -16 2 785.12 38.1 2 -2 -16 834.22 37.9 2 2 -16 819.42 37.8 16 -2 -2 793.92 38.1 -16 -2 -2 791.82 38 -16 -2 2 821.22 38.3 -2 -16 -2 809.12 38.2 -2 -2 16 765.42 37.9 0 -4 16 325.57 16.1 0 4 -16 313.87 16 0 -4 -16 342.47 16.2 16 0 -4 311.47 16.5 -16 -4 0 312.57 16.4 -4 0 -16 348.77 15.2 0 -16 -4 309.57 16.4 0 -16 4 286.27 16.3 4 0 -16 310.87 16.3 16 -4 0 302.97 16.5 16 4 0 310.47 16.3 4 -16 0 310.97 16.4 -16 0 4 356.76 16.8 -4 -16 0 326.97 16.5 16 0 4 303.97 16.1 -4 2 -16 82.99 4.7 -2 -4 -16 77.49 5.5 -2 -16 4 84.49 6.6 2 -16 -4 81.39 6.3 2 -4 16 70.49 5.3 -16 -4 2 78.89 6.4 16 2 -4 77.79 6.3 2 4 -16 77.29 5.9 4 -16 2 86.59 6.4 -4 -16 -2 84.09 6.5 -16 -2 -4 76.49 6 16 -2 4 72.99 5.8 -4 -2 16 74.09 6.3 4 -2 -16 84.59 6.2 16 4 2 85.09 6.3 16 -4 -2 71.69 6.3 -16 -4 -2 66.09 6 -4 -16 2 80.09 6.5 -2 -16 -4 76.09 6.2 -2 -4 16 76.09 6.1 16 -2 -4 67.09 6.3 2 -4 -16 88.09 6.2 -4 -2 -16 82.79 4.9 -16 -2 4 87.19 6.7 16 -4 2 73.89 6.1 16 4 -2 76.19 6.2 4 2 -16 85.69 6.2 16 2 4 68.39 5.6 -2 4 -16 92.49 5.6 2 -16 4 83.29 6.6 -16 -4 4 33 4.8 -4 -4 -16 38.1 3.4 -4 -4 16 29.3 4.5 -4 4 -16 41.8 3.3 4 -16 4 37.6 4.5 4 -4 -16 33.5 4.4 4 -4 16 42.3 3.3 4 4 -16 39.1 4.4 16 -4 -4 28.3 4.5 16 -4 4 36 4.2 -16 -4 -4 35.8 4.4 16 4 4 32.7 4.2 16 4 -4 39 4.7 -4 -16 4 37.5 4.7 -4 -16 -4 41.2 4.7 0 -6 16 279.57 17.9 16 0 6 402.96 17.9 16 -6 0 352.66 18.5 0 -6 -16 356.76 18.2 -16 0 6 366.76 18.7 16 6 0 369.36 18.5 6 0 -16 350.56 18.3 0 6 -16 368.66 18.1 16 0 -6 339.07 18.5 0 -16 6 404.66 18.7 -6 -16 0 367.06 18.4 -16 -6 0 374.26 18.6 0 -16 -6 388.16 18.5 -16 -2 -6 68.79 5.3 6 -16 2 75.59 5.9 16 -6 -2 59.49 5.8 2 6 -16 65.39 5.4 16 6 2 55.09 5.5 -16 -6 2 62.79 5.9 -6 -2 16 66.29 6 16 2 -6 62.09 5.8 2 -6 16 62.49 5 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85.79 6.6 -16 -6 -6 80.29 6.3 -6 -6 16 80.69 6.8 -6 -6 -16 79.79 5.1 -6 -16 -6 75.79 6.5 -6 -16 6 91.99 6.9 -6 -6 -16 74.89 4.9 16 6 -6 83.99 6.7 16 6 6 69.89 5.9 -16 -6 6 80.89 6.9 6 -6 -16 66.89 6.4 6 -6 16 79.29 5 6 6 -16 71.79 6.2 16 0 8 2039.5 92.39 0 -8 16 1978.5 92.99 0 -8 -16 1883.01 92.99 -16 0 8 2137.09 93.49 -8 -16 0 2101.99 93.29 -16 -8 0 2155.28 93.39 0 -16 -8 2095.19 93.29 16 0 -8 2147.99 93.39 16 -8 0 1968.9 93.39 0 8 -16 1938.61 92.89 0 -16 8 2048.4 93.29 8 0 -16 2030.5 93.29 16 8 0 1801.72 93.09 -8 -16 -2 1552.54 68.79 8 -2 -16 1481.45 68.79 16 -2 8 1541.75 67.89 16 -8 -2 1461.95 68.89 2 -8 16 1416.16 68.29 -8 -2 16 1494.25 68.89 8 16 -2 1491.75 68.79 -2 -8 -16 1493.55 68.49 2 8 -16 1425.46 68.49 16 2 -8 1559.24 68.89 -16 -8 2 1444.56 68.79 16 8 2 1351.26 68.59 -2 -16 8 1481.45 68.69 2 -16 8 1541.65 68.79 -2 -8 16 1272.87 68.39 8 2 -16 1487.75 68.79 -8 -16 2 1543.15 68.79 -16 -2 8 1569.24 68.99 16 -2 -8 1483.55 68.79 16 -8 2 1355.16 68.69 16 2 8 1666.53 67.99 -16 -8 -2 1469.35 68.69 2 -8 -16 1371.26 68.69 -2 -16 -8 1526.15 68.79 16 8 -2 1493.45 68.79 -2 8 -16 1523.25 68.39 -8 -16 -4 652.63 30.1 -4 -16 8 655.03 30.1 -16 -8 4 636.14 30.1 -8 -4 16 633.74 30.2 16 -4 8 677.53 29.2 16 8 4 517.05 29.6 8 -4 -16 623.74 30.1 -16 -4 -8 622.14 29.3 8 16 -4 641.54 30.1 16 -8 -4 633.84 30.2 4 8 -16 585.84 29.8 4 -8 16 661.13 29.4 16 4 -8 603.64 30 8 -16 4 617.94 29.9 -4 -8 -16 598.64 29.5 -16 -4 8 658.53 30.2 16 -8 4 569.94 29.9 -16 -8 -4 561.04 29.8 16 -4 -8 604.74 30.1 4 -8 -16 581.04 30 4 16 -8 660.23 30.1 -4 -16 -8 607.24 29.9 16 4 8 649.43 29.3 8 4 -16 606.54 29.9 -8 -16 4 652.43 30 4 -16 8 630.74 30 -4 -8 16 558.94 29.9 16 8 -4 611.24 30 16 8 6 1082.19 51.39 -6 -8 -16 1116.49 50.99 -16 -6 -8 1063.59 51.19 6 -8 16 1159.68 50.89 8 16 -6 1170.78 51.79 6 8 -16 1069.59 51.59 16 -6 8 1114.99 51.09 -8 -16 -6 1063.19 51.59 16 6 -8 1101.29 51.69 -16 -8 6 1082.59 51.69 8 -16 6 956.2 51.39 8 -6 -16 1116.19 51.89 -6 -8 -16 1151.68 51.09 16 -8 -6 1089.19 51.89 -6 -16 8 1115.89 51.69 -8 -6 16 1106.19 51.89 6 16 -8 1141.39 51.79 -8 -16 6 1145.89 51.79 8 6 -16 1064.59 51.59 -6 -8 16 1113.89 51.89 -16 -6 8 1148.69 51.99 6 -16 8 1068.89 51.59 16 -6 -8 1147.39 51.89 -8 -6 -16 1097.09 50.29 -16 -8 -6 917.31 51.19 16 6 8 1215.88 51.19 -8 -6 -16 1131.99 50.29 16 8 -6 1113.59 51.69 -6 -16 -8 1099.29 51.69 6 -8 -16 1079.89 51.89 16 -8 6 1081.59 51.49 -8 -8 -16 3977.3 177.48 8 8 -16 3864.01 178.28 8 -8 16 4023.3 177.18 16 -8 8 3935.61 177.88 -16 -8 -8 3756.62 177.88 -16 -8 8 3912.31 178.48 -8 -16 -8 3682.63 178.18 -8 -16 8 4010.7 178.38 8 -8 -16 3946.61 178.48 -8 -8 -16 4010.3 177.48 -8 -8 16 3914.31 178.48 8 16 -8 3920.41 178.38 16 8 8 4017.6 177.98 16 8 -8 3969.1 178.28 16 -8 -8 4102.19 178.58 8 -16 8 3429.16 178.08 -16 0 10 1519.35 65.79 10 0 -16 1452.05 65.49 10 16 0 1518.55 65.59 16 10 0 1439.36 65.49 -10 -16 0 1496.05 65.49 16 -10 0 1386.76 65.59 16 0 10 1309.17 63.99 0 -16 10 1513.75 65.59 0 -10 16 1166.68 64.99 0 10 -16 1253.67 64.99 -16 -10 0 1461.65 65.49 16 0 -10 1504.65 65.59 0 -10 -16 1284.07 65.39 16 10 2 407.46 24.9 -2 -16 10 528.05 25.3 16 -10 -2 524.45 25.5 10 -2 -16 546.85 25.5 -10 -16 -2 536.75 25.3 -10 -2 16 532.65 25.5 2 10 -16 458.15 24.9 10 16 -2 534.85 25.3 -16 -10 2 528.25 25.3 16 -2 10 556.24 23.7 2 -10 16 444.96 24.7 16 2 -10 541.25 25.3 -2 -10 16 422.46 24.9 16 -2 -10 549.25 25.4 16 10 -2 529.55 25.4 -10 -16 2 513.05 25.2 10 2 -16 538.35 25.3 -16 -10 -2 524.45 25.2 16 -10 2 437.36 25.1 -2 10 -16 536.15 24.9 -16 -2 10 541.15 25.5 16 2 10 508.45 23.7 2 -16 10 521.25 25.2 -2 -16 -10 511.85 25.2 2 -10 -16 474.15 25.4 16 -10 -4 136.99 9.5 10 -4 -16 147.69 9.6 16 4 -10 148.69 9.4 -4 -16 10 150.78 9.4 16 10 4 128.09 9.2 4 10 -16 140.99 9.3 10 -16 4 132.69 9.2 10 16 -4 158.58 9.8 -16 -10 4 126.19 9.2 16 -4 10 124.99 7.4 -10 -16 -4 144.49 9.4 -10 -4 16 157.78 10 4 -10 16 136.99 8.8 -16 -4 10 139.99 9.5 4 16 -10 142.89 9.2 16 10 -4 141.99 9.4 4 -16 10 118.89 9 -4 -16 -10 137.79 9.2 16 -10 4 114.29 9.2 -16 -10 -4 134.39 9.3 -10 -16 4 143.09 9.1 4 -10 -16 121.79 9.4 10 4 -16 147.69 9.5 16 -4 -10 147.59 9.6 -4 -10 16 132.79 9.3 6 10 -16 274.77 15.4 -10 -6 16 277.57 15.7 -10 -16 -6 259.27 15.4 10 -6 -16 285.27 15.9 16 6 -10 304.27 15.6 16 -10 -6 296.47 15.9 -16 -6 -10 327.17 14.7 10 -16 6 253.17 15.4 16 10 6 268.57 15.4 -6 -10 -16 235.98 14.8 -6 -16 10 288.77 15.6 -16 -10 6 290.17 15.6 16 -6 10 320.47 14.4 6 -10 16 296.37 14.9 10 16 -6 289.37 15.5 16 10 -6 283.77 15.5 16 -6 -10 302.97 15.8 -16 -6 10 288.27 15.7 -6 -10 16 299.97 15.9 6 -10 -16 294.47 15.9 6 -16 10 262.07 15.3 6 16 -10 302.27 15.7 -6 -16 -10 295.07 15.7 -16 -10 -6 265.97 15.4 10 6 -16 304.47 15.7 -10 -16 6 294.97 15.5 16 -10 6 281.57 15.7 10 -8 -16 1875.11 85.49 -10 -16 -8 1812.22 85.19 -8 -10 -16 1802.12 84.59 -8 -16 10 1973.2 85.49 -16 -10 8 1794.42 85.29 16 -8 10 1889.11 84.59 8 -10 16 1833.62 84.39 8 10 -16 1813.62 85.29 -16 -8 -10 1717.83 84.59 10 -16 8 1609.84 84.99 16 -8 10 1841.62 84.49 -10 -8 16 1915.51 85.59 16 8 -10 1851.31 85.29 16 -10 -8 1895.21 85.49 10 16 -8 1908.11 85.29 16 10 -8 1842.72 85.29 8 16 -10 1858.81 85.29 -16 -8 10 1866.81 85.39 10 8 -16 1876.21 85.29 8 -16 10 1759.42 85.09 16 -10 8 1844.42 85.09 -10 -16 8 1890.11 85.29 -8 -10 16 1908.11 85.49 -16 -10 -8 1658.03 84.89 -8 -16 -10 1750.32 85.19 -10 -8 -16 1927.41 84.09 16 -8 -10 1925.11 85.49 -10 -8 -16 1994.7 84.19 8 -10 -16 1809.52 85.49 -16 -10 10 1065.79 51.49 -16 -10 -10 1063.29 51.09 -10 -10 16 1126.59 51.79 10 -16 10 1106.79 51.39 10 -10 -16 1109.89 51.79 10 16 -10 1110.79 51.59 16 -10 -10 1059.59 51.59 16 -10 10 1125.49 50.89 16 10 -10 1087.49 51.49 -10 -16 -10 1093.09 51.49 -10 -16 10 1072.19 51.49 -10 -10 -16 1095.39 50.69 10 -10 16 1071.19 50.29 16 -10 10 1085.49 51.09 10 10 -16 1102.59 51.49 12 16 0 246.58 13.5 16 0 -12 246.28 13.4 0 -16 12 235.58 13.3 0 12 -16 222.08 13.1 0 -12 16 222.68 13.2 -12 -16 0 238.38 13.3 -16 -12 0 217.38 13.2 12 0 -16 236.18 13.4 16 -12 0 225.68 14 16 12 0 254.77 13.7 -16 0 12 217.18 13.5 -16 -12 2 4.9 4.1 12 16 -2 2.7 4.1 16 12 2 4.1 4.2 16 -12 -2 1.2 4.6 2 -12 16 1.4 3.6 2 12 -16 -0.6 3.7 -12 -2 16 0.3 4.1 16 2 -12 2.8 4.1 -12 -16 -2 1.9 3.8 12 -2 -16 0.4 3.8 -2 -16 12 -0.2 3.9 2 16 -12 -1 4 12 16 2 6 4.2 12 2 -16 1 3.9 16 12 -2 0.4 3.9 2 -12 -16 -1.5 4.5 -16 -12 -2 3 4 -2 -12 16 0.8 3.9 -16 -2 12 3.4 4.4 16 -12 2 4.9 4.6 -2 -16 -12 1.1 3.9 16 -2 -12 4.9 4 2 -16 12 0.2 4 -12 -16 2 6 3.8 -4 -16 12 478.95 22.8 4 12 -16 431.16 22.5 12 -4 -16 455.95 22.8 -12 -16 -4 475.35 22.7 12 16 -4 465.85 22.7 16 12 4 390.76 22.5 -4 -12 -16 429.86 22.4 -12 -4 16 455.25 23 16 -12 -4 460.55 23.1 -16 -12 4 481.95 22.9 16 4 -12 478.35 22.7 4 -12 16 427.86 22.3 4 -12 -16 460.55 23.1 -4 -12 16 448.76 22.8 4 16 -12 473.85 22.8 -12 -16 4 441.06 22.6 16 -12 4 390.16 22.7 4 -16 12 431.76 22.5 12 4 -16 474.85 22.7 -16 -12 -4 410.26 22.6 16 -4 -12 464.45 22.8 -4 -16 -12 433.96 22.7 16 12 -4 453.15 22.7 -16 -4 12 446.36 22.8 -6 -16 12 173.38 10.6 -16 -6 -12 135.49 8.4 16 6 -12 165.78 10.3 16 -12 -6 149.49 10.7 -6 -12 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11.4 -12 -8 -16 181.68 8.8 16 -12 8 179.78 12 8 16 -12 185.48 11.4 16 -10 12 18.8 4.2 16 -12 -10 18.3 5.4 10 -12 16 11.1 4 10 12 -16 20.6 5.1 12 16 -10 14.6 5 12 -16 10 18.2 5.2 16 10 -12 13.6 4.5 -10 -12 -16 21.7 4.7 -16 -10 -12 14.4 4.5 12 -10 -16 22.5 5.5 10 -16 -12 19.1 5.3 -12 -10 16 19.6 5.6 -16 -12 10 18.5 5.1 -10 -16 12 20.8 5 16 -10 12 22.6 4 -12 -16 -10 17.2 5.4 16 -10 -12 20.2 5.3 -16 -12 -10 19.5 5 16 12 -10 20.4 5.2 -12 -10 -16 13.3 3.7 16 -12 10 21.1 5.4 -10 -16 -12 26.2 5.5 10 -12 -16 17.8 5.6 16 -12 10 14.2 4.6 12 10 -16 20.9 5.2 10 16 -12 24.5 5.3 12 -10 16 18.1 2.4 12 -16 -10 14.8 5.6 12 -10 16 19.6 2.5 -12 -16 10 19.1 5.1 -16 -10 12 24 5.6 10 -16 12 21.7 5.4 -10 -12 16 19.9 5.2 16 -12 12 219.98 12.6 12 -12 16 202.48 11.8 12 -12 -16 222.48 13.6 -12 -12 -16 212.98 12.6 12 16 -12 204.58 12.9 -12 -12 16 205.38 13.3 -16 -12 -12 209.68 13 -16 -12 12 213.98 13 16 -12 -12 214.38 13.3 -12 -16 -12 199.88 13.2 12 -16 12 203.88 13.2 16 -12 12 209.38 13.1 16 12 -12 197.78 12.7 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4.9 -14 -16 4 13.8 4.7 4 -16 14 9.3 4.6 -16 -14 -4 13.4 4.7 4 16 -14 12.2 4.7 16 14 -4 13.6 4.6 -16 -4 14 8.2 5 14 4 -16 9.5 4.6 4 -14 -16 14 5.5 -4 -16 -14 7.9 4.7 -4 -14 16 9.7 4.9 -6 -14 -16 -0.3 4.6 6 14 -16 2.9 4.6 -6 -16 14 5.4 4.8 14 16 -6 -1.3 4.5 16 6 -14 2.2 4.1 14 -6 -16 1.8 4.8 14 -16 6 3.2 4.9 16 -14 -6 1.4 5 -14 -6 16 3.3 4.8 -16 -14 6 2.5 4.6 -14 -16 -6 2 4.7 6 -14 16 -2 4.3 6 -16 14 2 4.5 -16 -6 14 7.2 4.7 -6 -16 -14 3.9 4.7 14 6 -16 -0.7 4.1 16 14 -6 1 4.6 -16 -14 -6 0.5 4.8 -6 -14 16 4.6 4.9 6 -14 -16 4.6 5.2 16 -6 -14 -0.2 4.6 6 16 -14 3.9 4.5 -14 -16 6 1.6 4.1 8 -16 -14 521.55 26 14 16 -8 509.85 25.3 -16 -8 -14 485.45 23.6 14 -8 -16 506.85 25.7 -14 -16 -8 511.95 25.5 -8 -16 14 519.25 25.5 -8 -14 -16 494.05 25.3 16 -14 -8 522.05 25.7 -16 -14 8 489.35 25.4 8 -14 16 549.74 25.2 8 14 -16 512.35 25.4 14 -16 8 500.55 25.4 16 8 -14 492.35 25.2 -14 -8 16 497.65 25.6 8 -16 14 493.15 25.3 8 -14 -16 507.35 25.9 -14 -16 8 484.45 25.4 -16 -14 -8 502.65 25.5 14 -16 -8 478.15 25.7 8 16 -14 494.05 25.3 -16 -8 14 501.85 25.6 14 8 -16 496.85 25.3 16 14 -8 498.35 25.3 -8 -14 16 538.25 25.8 16 -14 8 490.65 26 16 -8 -14 481.65 25.5 16 -14 8 505.35 25.4 -8 -16 -14 495.65 25.4 16 10 -14 179.58 11.7 -14 -10 16 198.58 12.5 -16 -14 10 180.88 12 16 -10 14 173.38 9.4 14 16 -10 184.18 11.8 -16 -10 -14 175.18 10.9 16 -10 14 175.68 9.6 -14 -16 -10 197.28 12.3 14 -10 -16 186.48 12.2 -10 -14 -16 155.78 11.2 16 -14 -10 168.58 12.1 10 -16 -14 167.68 12.2 10 -14 16 177.38 11.3 10 14 -16 184.48 12 -10 -16 14 197.38 12.2 14 -16 10 192.18 12.1 -16 -14 -10 166.58 11.6 14 -16 -10 198.28 12.5 -14 -10 -16 179.78 10.2 -16 -10 14 172.18 11.9 -10 -16 -14 170.68 11.6 16 -10 -14 189.08 12 10 -14 -16 188.18 12.4 10 -16 14 163.88 11.4 10 16 -14 161.48 11.6 -14 -16 10 173.58 11.8 14 10 -16 178.18 11.8 -10 -14 16 178.88 12 16 -14 10 177.28 12.2 16 14 -10 175.48 11.6 16 -14 10 199.08 12.2 -14 -16 -12 70.39 7.9 -12 -14 -16 73.29 7.6 14 -12 -16 76.99 7.9 -16 -12 -14 73.59 7.5 12 -14 16 57.59 6.9 12 14 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1765.92 79.99 16 -8 -16 1720.53 80.09 16 8 -16 1666.43 79.79 16 16 -8 1704.03 79.89 -16 -16 -10 792.12 49.1 -16 -16 10 1046.6 49.4 -16 -10 16 1051.29 49.5 -10 -16 -16 1061.99 49.4 -10 -16 16 1099.89 49.6 10 -16 -16 1059.09 49.8 10 -16 16 1083.69 49.3 10 16 -16 1089.09 49.5 16 -16 -10 1027.1 49.6 16 -16 10 1003.1 49.2 16 -10 -16 1026.4 49.5 16 10 -16 1084.89 49.3 16 16 -10 1025.7 49.2 -16 -16 -12 78.69 9.1 -16 -16 12 105.29 9 -16 -12 -16 86.39 8.1 -16 -12 16 101.49 9.1 -12 -16 -16 88.59 9.1 -12 -16 16 96.39 9.2 12 -16 -16 86.09 9.3 12 -16 16 89.69 8.9 12 16 -16 98.69 8.8 16 -16 -12 76.49 8.9 16 -16 12 79.29 8.8 16 -12 -16 90.29 9.1 16 12 -16 95.19 8.7 16 16 -12 89.29 8.4 -16 -16 -14 497.65 27.1 -16 -16 14 494.05 26.4 -16 -14 16 485.05 26.5 -14 -16 16 505.85 26.4 14 -16 -16 507.05 26.9 14 16 -16 492.95 26.3 16 -16 -14 486.65 26.6 16 -16 14 515.15 27 16 -16 14 449.76 27.8 16 -14 -16 512.45 26.5 16 -14 16 604.14 25.9 16 -14 16 518.45 25.9 16 14 -16 473.75 26.1 16 16 -14 498.25 26.1 -16 -16 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976.4 48.2 20 12 2 969.3 48.5 -12 -20 -2 998.3 48.3 20 -12 -2 1184.98 49.1 20 2 -12 974.3 48.2 -2 -20 12 1044.5 48.5 -20 -12 2 1014.1 48.6 12 -2 -20 959.7 48.4 2 12 -20 1075.59 48.4 2 -20 -12 989.6 48.3 12 -20 2 1013.2 48.3 -12 -20 2 1030.1 48.4 20 -12 2 1022.9 48.8 -20 -2 12 955.6 48.5 -2 -12 20 1036.7 48.6 12 2 -20 1026.5 48.4 -2 -20 -12 1004.3 48.3 20 12 -2 1017.1 48.5 -20 -12 -2 1033.1 48.6 20 -2 -12 990.1 48.3 2 -20 12 996.1 48.3 2 -12 -20 1035.7 48.7 20 -12 -4 2110.99 97.59 12 20 -4 2115.99 97.29 4 -12 20 2126.59 97.09 20 4 -12 2050.49 97.19 12 -20 4 2075.39 97.29 20 12 4 2053.79 97.29 4 12 -20 2146.49 97.39 12 -4 -20 2074.69 97.49 -4 -12 -20 2160.78 97.19 -20 -12 4 2009.2 97.29 -12 -4 20 2273.17 97.79 -12 -20 -4 2136.39 97.39 -4 -20 12 2159.18 97.39 4 -20 12 2129.49 97.39 -20 -4 12 2030.7 97.29 20 -4 -12 2026.5 97.19 -4 -20 -12 2132.69 97.39 20 -12 4 2127.29 97.49 -20 -12 -4 2106.19 97.49 -4 -12 20 2059.79 97.39 12 4 -20 1995.5 97.19 20 12 -4 2078.79 97.29 -12 -20 4 2100.79 97.29 4 -12 -20 2184.68 97.79 6 -12 20 538.35 28.7 12 20 -6 583.24 29.1 -6 -20 12 583.34 29.2 20 12 6 571.74 29.3 6 12 -20 598.94 29.3 12 -20 6 592.84 29.3 -12 -20 -6 594.14 29.5 -12 -6 20 566.34 29.6 -20 -12 6 600.94 29.4 -6 -12 -20 586.24 29.1 20 -12 -6 586.14 29.7 20 6 -12 561.14 29 12 -6 -20 584.14 29.5 -20 -12 -6 601.34 29.5 20 -12 6 597.14 29.8 12 6 -20 588.44 29.3 -12 -20 6 567.94 29 -6 -20 -12 595.94 29.4 -6 -12 20 592.04 29.8 20 12 -6 569.54 29.1 -20 -6 12 552.34 29.3 6 -20 12 620.44 29.4 20 -6 -12 557.44 29.3 6 -12 -20 604.04 29.9 -8 -20 12 117.89 9.7 8 -12 20 104.69 8.3 -12 -8 20 106.49 10 -20 -8 -12 102.09 8.5 12 -20 8 138.99 10.3 20 -8 12 110.59 7.3 12 -8 -20 118.89 10.1 -20 -12 8 123.19 10 20 8 -12 123.19 9.6 12 20 -8 130.29 9.6 20 -12 -8 129.19 10.1 8 12 -20 87.69 9.2 20 -8 12 117.59 7.5 -8 -12 -20 90.29 8.6 -12 -20 -8 129.29 10.2 12 8 -20 110.49 9.6 20 -12 8 119.49 10.2 20 -8 -12 117.79 9.6 -12 -20 8 113.69 9.5 8 -12 -20 123.79 10.3 -8 -20 -12 145.99 10.5 8 20 -12 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1063.69 48.1 12 12 -20 1024.9 49.9 -12 -12 20 1043.7 50.09 14 0 -20 14.7 5.9 0 -20 14 12.2 6.1 0 -20 -14 12.8 5.9 20 -14 0 11.4 6.7 -14 -20 0 13.4 5.5 0 -14 20 12.7 6.3 20 14 0 12.3 6.2 0 -14 -20 11.4 6.6 20 0 -14 13.3 5.6 -20 -14 0 10.3 6.1 14 -2 -20 419.76 22.5 2 14 -20 416.86 22.5 -2 -20 14 408.86 22.4 20 -14 -2 425.36 23.3 -20 -14 2 419.56 22.7 20 2 -14 392.76 22.1 20 14 2 453.15 22.9 14 20 -2 443.76 22.4 -14 -20 -2 416.06 22.4 2 -14 20 404.76 22.6 20 -14 2 431.66 23.4 -2 -14 20 427.96 22.8 2 -14 -20 428.46 23.5 2 -20 14 433.66 22.9 -20 -14 -2 405.66 22.6 20 -2 -14 377.96 22 -20 -2 14 418.56 22.6 20 14 -2 457.15 22.8 -2 -20 -14 415.06 22.7 14 2 -20 417.46 22.4 -14 -20 2 465.95 22.5 -4 -14 -20 943.91 43.9 -20 -14 4 906.91 43.9 14 -20 4 963.4 44 20 -14 -4 937.01 44.3 4 -14 20 887.81 43.8 -14 -4 20 893.21 44.2 20 4 -14 914.21 43.7 20 14 4 961.8 44 14 -4 -20 943.01 44 14 20 -4 953.6 43.8 4 14 -20 973.1 44.1 -14 -20 -4 913.91 43.9 -4 -20 14 712.33 43.4 -4 -20 -14 913.01 44 20 14 -4 834.92 43.7 4 -14 -20 955.6 44.5 14 4 -20 883.41 43.7 -20 -14 -4 914.31 44.2 -14 -20 4 871.11 43.6 4 -20 14 905.71 43.9 -20 -4 14 885.21 43.9 20 -4 -14 891.71 43.7 20 -14 4 929.91 44.5 -4 -14 20 939.61 44.1 -6 -14 -20 114.59 10.2 -20 -14 6 124.29 10.2 6 -14 20 98.19 9.7 6 14 -20 120.19 10.2 -14 -20 -6 131.09 10.6 -6 -20 14 141.29 10.5 -14 -6 20 119.79 10.7 20 6 -14 121.89 9.7 14 -6 -20 139.09 10.6 14 20 -6 129.99 9.9 20 -14 -6 106.99 10.4 20 14 6 126.79 10.6 14 6 -20 126.19 10 -14 -20 6 115.39 9.8 -20 -14 -6 121.19 10.4 -6 -14 20 146.49 11.1 6 20 -14 140.79 10.3 6 -14 -20 116.99 10.5 6 -20 14 125.19 10.2 20 -14 6 117.69 11 -6 -20 -14 129.29 10.5 -20 -6 14 120.39 10.3 20 -6 -14 118.89 9.8 20 14 -6 162.08 10.6 8 -14 20 0.6 6.5 -14 -8 20 1.4 6.7 -8 -14 -20 2.8 6.6 20 8 -14 4.2 5.4 8 14 -20 3.6 6.1 -14 -20 -8 2.8 6.6 20 -14 -8 -1 6.5 14 20 -8 0.7 5.8 -20 -14 8 1.3 6.1 -8 -20 14 1.5 6.2 14 -20 8 4.1 6.8 14 -8 -20 3 6.6 14 8 -20 2.8 5.9 8 -20 14 6.1 6.7 8 20 -14 3.5 5.6 -8 -20 -14 -3.6 6.6 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-21 3 427.96 20.8 1 3 -21 399.96 20.4 -3 1 -21 437.76 19.6 3 -21 1 417.36 20.8 21 3 1 386.46 20.8 21 -1 3 327.97 20.4 21 1 -3 414.26 20.9 -21 -3 1 391.26 21 21 -3 -1 391.76 21.1 21 -1 -3 383.46 20.9 21 -3 1 393.16 20.8 21 3 -1 403.76 20.8 -21 -3 -1 393.26 21.2 21 1 3 536.65 21.3 -3 -1 -21 412.36 19.6 3 -21 -1 389.96 20.5 -1 -21 -3 385.56 20.6 1 -3 -21 409.26 20.5 -21 -1 3 396.66 21.2 1 -21 3 401.76 20.7 -3 -21 1 399.36 20.6 3 1 -21 381.76 20.6 -3 -3 -21 1447.26 65.09 -3 3 -21 1504.75 64.99 3 -21 -3 1404.06 65.79 -3 -21 3 1562.94 65.99 -21 -3 -3 1394.16 66.09 -21 -3 3 1442.66 66.19 -3 -21 -3 1437.86 65.89 3 -3 -21 1365.16 65.69 3 3 -21 1360.56 65.69 21 -3 -3 1449.26 66.19 21 -3 3 1345.97 65.79 21 3 -3 1395.26 65.99 21 3 3 1175.48 65.49 3 -21 3 1476.15 65.99 21 -5 -1 253.17 15.3 5 -1 -21 248.68 15.1 21 -1 5 275.87 15 21 1 -5 262.77 15.3 5 -21 1 271.07 14.9 -1 -21 5 296.77 15.2 -5 -21 -1 290.37 15.1 1 5 -21 261.17 14.8 21 5 1 249.78 15 -21 -5 1 272.17 15.8 1 -21 -5 270.57 14.9 -21 -1 5 263.17 15.6 -5 -21 1 271.67 14.9 1 -21 5 283.97 15.1 21 -1 -5 268.97 15.3 5 1 -21 247.78 15 5 -21 -1 275.27 14.9 21 -5 1 277.17 15.6 21 5 -1 281.67 15.6 -21 -5 -1 271.27 15.6 21 1 5 259.27 15 1 -5 -21 275.57 15 -1 -21 -5 265.37 15 -1 -5 21 260.67 15.3 5 -21 3 1542.45 70.09 -21 -5 3 1493.55 70.19 21 3 -5 1462.15 69.99 -5 -21 -3 1543.45 69.99 5 -3 -21 1414.06 69.79 3 5 -21 1451.05 69.79 21 -3 5 1503.15 69.79 -3 -21 5 1519.35 69.89 3 -21 -5 1448.85 69.79 21 5 3 1470.15 69.89 21 -5 -3 1522.55 70.19 -3 -5 21 1521.95 70.09 5 3 -21 1353.36 69.69 -3 -21 -5 1542.35 69.99 3 -5 -21 1447.46 69.89 21 -5 3 1485.65 69.99 21 5 -3 1469.55 69.99 21 3 5 1435.16 69.69 21 -3 -5 1536.65 70.19 -21 -3 5 1555.24 70.29 3 -21 5 1528.15 69.99 -5 -21 3 1534.75 69.99 -5 -3 -21 1602.94 68.39 -3 5 -21 1538.35 69.19 -5 -3 -21 1505.05 68.39 5 -21 -3 1523.05 69.89 -21 -5 -3 1554.24 70.19 -5 -5 -21 2026 85.99 -5 -21 -5 1866.01 87.09 -5 -21 5 1864.71 86.99 -21 -5 -5 1830.62 87.09 -21 -5 5 1848.12 87.29 5 -21 5 1968.3 87.19 5 -5 -21 1745.53 86.99 5 5 -21 1857.91 86.99 21 -5 5 1805.82 86.89 -5 -5 -21 1965.7 85.99 -5 -5 21 1885.11 87.29 5 -21 -5 1865.11 86.99 21 5 5 1857.61 86.99 21 5 -5 1876.31 87.19 21 -5 -5 1925.31 87.39 1 -7 21 35.3 5.7 -7 -21 -1 45.8 6 7 -21 1 58.69 6.2 21 -7 -1 44 6.4 1 7 -21 46.1 6.3 7 -1 -21 42.1 6 21 1 -7 44.5 6.3 21 -1 7 45.5 5.5 1 -21 -7 43.2 5.5 21 7 1 49.9 6.4 -21 -7 1 45 6.4 -1 -21 7 52.39 6.3 21 -7 1 47.6 6.7 1 -7 -21 45.8 6.2 -1 -7 21 43 6 21 1 7 48.8 5.7 -7 -21 1 48.6 6 7 1 -21 41.7 6.1 -21 -1 7 46.7 6.6 1 -21 7 52.79 6.2 21 -1 -7 48 6.4 -21 -7 -1 45.3 6.5 7 -21 -1 54.99 6.1 -1 -21 -7 42.9 6 21 7 -1 45.6 6.3 3 -21 -7 260.77 14.9 -7 -3 21 288.47 16.1 21 7 3 262.97 15.6 7 -21 3 263.77 15.1 3 7 -21 277.47 15.4 21 -3 7 268.27 14.9 21 3 -7 270.07 15.3 -7 -21 -3 279.47 15.3 3 -7 21 272.77 14.8 -21 -7 3 266.17 15.6 7 -3 -21 245.58 15.5 21 -7 -3 262.37 15.8 -3 -21 7 269.57 15.1 -21 -3 7 264.47 15.6 7 3 -21 242.58 15.2 -3 -21 -7 287.87 15.4 21 -7 3 283.07 15.8 21 7 -3 273.17 15.4 7 -21 -3 272.87 14.9 -21 -7 -3 251.27 15.6 21 -3 -7 258.77 15.4 -7 -21 3 282.57 15.2 -3 -7 21 250.97 15.5 3 -7 -21 261.67 15.6 21 3 7 266.77 14.9 3 -21 7 284.97 15.3 21 7 5 431.66 21.3 21 -7 -5 403.76 21.5 -5 -7 -21 411.16 20.2 -5 -21 7 415.06 21.2 -5 -7 -21 414.26 20.2 5 7 -21 390.86 21.2 7 -21 5 442.76 21.5 7 -5 -21 377.66 21.2 -7 -5 21 408.96 21.7 21 5 -7 412.66 21.3 -21 -7 5 407.96 21.6 -21 -5 -7 381.26 21.3 21 -5 7 393.86 20.9 -7 -21 -5 400.26 21.1 5 -21 7 410.66 21.4 -21 -5 7 394.36 21.4 7 5 -21 396.36 21.3 -5 -21 -7 425.26 21.3 -21 -7 -5 408.66 21.5 -7 -21 5 411.26 21 21 7 -5 401.86 21.3 -5 -7 21 398.86 21.6 5 -7 -21 404.36 21.6 21 -5 -7 420.46 21.4 21 -7 5 375.96 21.2 21 5 7 395.66 20.9 -7 -7 -21 36 3.4 21 -7 7 33.8 6.2 21 7 -7 35.9 6.1 -7 -21 -7 35.2 6.1 -7 -7 21 39.3 6.8 -21 -7 -7 29.8 6.4 7 -21 7 34.5 6.1 7 -7 -21 38.8 6.6 7 7 -21 32.9 6.1 -7 -21 7 38.2 5.7 21 -7 -7 42.8 6.5 -21 -7 7 38.7 6.5 21 7 7 41.1 6.3 9 -21 1 3.4 4.6 9 -1 -21 0.6 4.9 21 -9 -1 -2.9 5.6 21 9 1 -1.9 5 -1 -21 9 -1.7 4.7 1 -21 -9 -2.5 4.4 -21 -9 1 -1.4 5.3 1 -9 21 0.5 4.9 -9 -21 -1 1.8 4.7 21 1 -9 -0.3 5 21 -1 9 -0.7 3.9 21 -9 1 -0.7 5.5 9 -21 -1 2.1 4.4 -1 -9 21 1.7 5 21 -1 -9 3 4.9 -1 -21 -9 1.5 4.5 -21 -9 -1 0.4 5.4 21 9 -1 6.6 5.2 -9 -21 1 0.3 4.7 21 1 9 -1.3 3.9 1 -9 -21 0.4 4.9 9 1 -21 0.7 4.8 1 -21 9 -0.7 4.9 3 -9 21 396.66 21.1 21 -9 -3 413.26 22.1 3 -21 -9 401.16 21.1 -9 -3 21 426.06 22.3 3 9 -21 423.76 21.5 9 -21 3 432.86 21.5 21 3 -9 405.56 21.4 -9 -21 -3 421.56 21.4 21 9 3 421.26 21.7 -3 -21 9 401.66 21.4 9 -3 -21 401.06 21.5 -21 -9 3 422.26 22 21 -3 9 418.36 20.6 -21 -3 9 386.06 21.6 -9 -21 3 407.26 21.3 3 -9 -21 365.86 21.5 -21 -9 -3 425.26 21.9 21 9 -3 371.76 21.3 21 3 9 420.36 20.7 -3 -21 -9 425.66 21.6 -3 -9 21 413.56 21.9 21 -9 3 421.26 21.9 3 -21 9 410.76 21.5 21 -3 -9 388.56 21.5 9 3 -21 389.06 21.3 -5 -9 -21 362.06 16.3 9 -5 -21 306.27 17.3 -9 -5 21 308.47 17.3 21 -9 -5 327.37 17.4 21 5 -9 302.87 16.7 -5 -21 9 302.17 16.7 21 9 5 299.57 17 9 -21 5 295.97 16.7 5 -9 21 277.47 15.9 5 9 -21 319.77 17 -9 -21 -5 300.17 16.7 21 -5 9 281.37 16 -21 -9 5 300.27 17 21 -5 -9 298.37 16.9 -21 -9 -5 270.47 17.1 9 5 -21 278.67 16.6 21 9 -5 296.67 16.8 21 5 9 299.97 16.3 -5 -9 21 315.57 17.4 5 -21 9 281.77 16.7 -5 -21 -9 290.17 16.7 -9 -21 5 288.67 16.3 -21 -5 9 265.67 16.9 21 -9 5 265.77 16.9 5 -9 -21 285.57 17.3 7 9 -21 9.9 5.7 -9 -7 21 2.1 5.9 -7 -9 -21 9.9 4.3 -7 -21 9 4.9 5.4 -9 -21 -7 5.5 5.3 -21 -7 -9 6.7 5.7 21 7 -9 4.9 5.4 9 -7 -21 6.8 5.8 9 -21 7 6.5 5.6 21 -9 -7 7.2 5.7 21 9 7 4.6 5.6 -21 -9 7 10.2 5.6 21 -7 9 10.2 5.2 9 7 -21 8.5 5.5 -9 -21 7 8 5.3 -7 -21 -9 7.5 5.6 -21 -7 9 8.2 5.5 7 -9 -21 7.3 6 21 9 -7 11.2 5.6 21 -9 7 5.7 5.9 21 7 9 10.3 5.3 -7 -9 21 6.1 6 7 -21 9 11.3 5.7 21 -7 -9 12.5 5.7 -21 -9 -7 11.7 6 -9 -21 -9 10.2 6 9 -21 9 5.5 6 -9 -21 9 5.7 5.2 -9 -9 21 12.6 6.7 -21 -9 -9 3.4 6.4 21 -9 9 5.4 5.9 21 9 -9 3.1 5.2 -21 -9 9 2.3 5.6 9 21 -9 5.6 5.5 21 -9 -9 4.6 5.8 9 -9 -21 0.9 6.1 9 9 -21 8.9 5.8 -21 -11 1 175.08 12.4 11 -1 -21 178.58 12.3 -11 -21 -1 207.48 12.4 1 -21 -11 185.48 12.1 21 11 1 173.48 12.1 21 -11 -1 174.58 12.6 21 1 -11 186.18 12.1 -1 -21 11 207.68 12.6 11 -21 1 188.38 12.2 1 -11 21 201.68 12.5 21 -1 11 186.08 9.5 21 -11 1 194.28 13 -1 -21 -11 172.58 12 21 -1 -11 189.18 12.3 -1 -11 21 213.48 12.8 11 1 -21 186.98 12.3 -21 -11 -1 201.08 12.9 1 -21 11 139.89 11.7 -11 -21 1 179.08 12.1 21 11 -1 176.68 12.3 21 11 3 1372.06 64.39 -11 -3 21 1322.87 64.49 3 -11 21 1308.97 63.89 11 -21 3 1329.17 64.09 -11 -21 -3 1416.96 64.39 -21 -11 3 1354.26 64.39 21 -3 11 1494.55 62.49 11 -3 -21 1331.67 64.29 -3 -21 11 1419.16 64.39 3 11 -21 1486.35 64.49 21 3 -11 1324.37 64.09 21 -11 -3 1325.67 64.49 3 -21 -11 1345.27 64.09 21 -3 -11 1377.06 64.29 -3 -11 21 1371.56 64.39 3 -11 -21 1369.06 64.49 -11 -21 3 1342.47 64.09 3 -21 11 1373.56 64.29 -3 -21 -11 1354.76 64.29 11 3 -21 1357.36 64.29 -21 -3 11 1291.07 64.29 -21 -11 -3 1375.46 64.49 21 11 -3 1376.36 64.29 21 -11 3 1369.46 64.59 21 -11 -5 1050.29 51.69 11 -5 -21 1075.69 51.59 21 5 -11 1030.1 51.29 -11 -21 -5 1059.49 51.49 -5 -21 11 1134.19 51.59 -5 -11 -21 1075.19 51.19 5 11 -21 1166.98 51.79 21 -5 11 1103.29 49.99 11 -21 5 1088.89 51.49 21 11 5 1085.39 51.59 -21 -11 5 1088.19 51.69 -11 -5 21 1069.69 51.89 5 -11 21 1028.2 50.89 21 -11 5 1106.29 51.89 21 11 -5 1072.69 51.49 -5 -11 21 1099.49 51.79 11 5 -21 1063.79 51.39 -11 -21 5 1107.99 51.29 5 -21 11 1088.59 51.59 21 -5 -11 1055.49 51.49 -21 -11 -5 1043.7 51.69 -21 -5 11 1041.6 51.59 5 -11 -21 1129.69 51.99 -5 -21 -11 1112.99 51.59 21 7 -11 145.99 10.8 -21 -11 7 151.28 11.3 21 11 7 163.18 11.4 7 -11 21 147.39 9.7 21 -7 11 142.39 9.3 -7 -21 11 162.98 11.1 11 21 -7 163.08 10.9 -7 -11 -21 111.99 9.7 21 -11 -7 163.98 11.7 21 -7 11 146.29 9.4 -11 -7 21 156.58 11.8 -11 -21 -7 156.38 11.3 11 -21 7 161.18 11.6 7 11 -21 151.28 11.1 11 -7 -21 140.09 11.2 21 11 -7 139.09 10.8 7 -11 -21 166.48 11.7 21 -7 -11 140.79 11.1 -11 -21 7 149.69 10.7 11 7 -21 151.68 11 -21 -7 11 158.58 11.3 7 -21 11 150.88 11.2 -21 -11 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391.76 21.7 1 -21 -13 376.56 20.8 -13 -21 -1 383.66 20.9 1 -13 21 377.06 21.3 21 13 1 435.76 21.7 21 -13 1 411.06 22 -1 -13 21 371.56 21.2 -21 -13 -1 367.46 21.1 21 13 -1 399.06 21.3 1 -21 13 391.06 21.3 21 -1 -13 372.16 20.7 -13 -21 1 387.16 20.8 -1 -21 -13 401.86 21 13 1 -21 387.76 20.9 21 13 3 1663.53 76.69 21 3 -13 1595.64 76.39 21 -13 -3 1637.74 76.99 -3 -21 13 1661.73 76.69 13 -21 3 1632.24 76.59 13 -3 -21 1626.44 76.69 -3 -13 -21 1609.64 76.59 -21 -13 3 1632.44 76.69 3 -13 -21 1740.13 77.29 13 3 -21 1637.04 76.69 21 -3 -13 1568.64 76.49 -21 -13 -3 1648.83 76.89 21 13 -3 1553.84 76.59 -21 -3 13 1568.94 76.69 3 -21 13 1665.23 76.79 -13 -21 3 1611.94 76.49 21 -13 3 1690.03 77.29 -3 -13 21 1688.53 76.89 -3 -21 -13 1743.33 76.89 -5 -21 13 1204.48 58.19 21 5 -13 1172.68 57.89 21 -13 -5 1230.28 58.49 -13 -21 -5 1240.38 58.39 -21 -13 5 1200.18 58.29 -13 -5 21 1285.87 58.69 13 -21 5 1280.37 58.39 13 21 -5 1253.67 58.19 21 13 5 1215.08 58.29 -5 -13 -21 1153.48 57.99 5 -13 21 1177.38 57.89 5 13 -21 1328.87 58.69 13 -5 -21 1173.28 58.29 13 5 -21 1185.88 58.09 21 -5 -13 1229.48 58.19 21 -13 5 1281.47 58.79 5 -21 13 1298.77 58.49 -21 -5 13 1139.29 58.09 -21 -13 -5 1231.98 58.49 -5 -21 -13 1223.58 58.39 21 13 -5 1220.08 58.19 -13 -21 5 1238.18 58.09 5 -13 -21 1288.47 58.69 -5 -13 21 1248.18 58.69 21 -13 -7 187.78 12.7 -13 -21 -7 188.88 12.6 -7 -21 13 163.58 12 13 -21 7 173.98 12.3 13 -7 -21 158.88 12.2 -21 -13 7 151.48 11.9 21 7 -13 176.98 11.9 -13 -7 21 142.69 12.3 7 -13 21 172.18 11.7 13 21 -7 177.68 11.8 7 13 -21 172.18 12.3 -7 -21 -13 194.98 12.8 7 -21 13 179.38 12.6 21 -13 7 161.08 12.6 13 7 -21 155.58 11.8 -21 -7 13 146.89 11.9 7 -13 -21 144.39 12.2 -13 -21 7 169.98 11.8 21 -7 -13 142.99 11.7 -7 -13 21 169.48 12.8 -21 -13 -7 150.58 12.5 21 13 -7 175.38 11.9 21 -13 -9 218.78 14.6 9 13 -21 240.58 14.7 -9 -13 -21 212.58 13.8 13 -9 -21 243.98 15.1 -13 -9 21 231.28 15.2 13 21 -9 221.18 14.2 9 -13 21 220.68 13.6 -13 -21 -9 209.58 14.4 -9 -21 13 224.48 14.5 -21 -13 9 237.28 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33.4 11.7 27 -9 3 33.8 11.2 27 9 5 -2.3 10.8 -27 -9 5 2.2 10.7 27 -9 -5 -1.9 10.3 27 -9 5 1.6 11.6 -27 -9 -5 -3.7 12.3 27 9 -5 1.8 9.5 -7 -9 27 249.97 19.1 -9 -9 27 280.37 21.3 1 11 -27 15.7 11.9 27 11 1 15.5 10.7 -27 -11 1 12.5 11.6 11 -1 -27 18.6 10.3 27 -11 -1 17.5 11.6 -27 -11 -1 22.2 12 27 -11 1 21 11.8 27 11 -1 21.9 10.6 1 -11 -27 20.3 12 11 1 -27 29.9 10.8 27 11 3 118.79 13.8 11 -3 -27 89.29 12.2 27 -11 -3 97.49 13.3 -27 -11 -3 96.69 15.1 -3 -11 27 93.39 14.9 27 11 -3 109.99 12.7 11 3 -27 83.09 11.8 27 -11 3 121.79 15.2 27 11 5 187.28 17.1 11 -5 -27 236.88 17 -5 -11 27 200.78 18.1 11 5 -27 208.88 16.1 27 -11 5 166.88 18.6 11 -7 -27 -6.3 11.6 -7 -11 27 0.2 13.1 11 7 -27 7.2 11.4 27 13 1 2.7 11.4 27 -13 -1 14.3 13.6 27 -13 1 -2.6 13.3 27 13 -1 0.8 11.3 -27 -13 -1 3.5 13.2 27 13 3 190.38 16.9 27 -13 3 150.48 17.3 -27 -13 -3 166.88 18.1 0 0 -28 148.29 14 28 0 0 185.58 14.6 0 -2 -28 1.8 10.2 0 2 -28 4.5 10 28 0 -2 6.1 8.8 28 0 2 2.4 9.7 28 2 0 6.2 9.7 2 0 -28 1.7 9.9 28 -2 0 1.5 9.1 -2 0 -28 6.4 7.7 28 -2 -2 16.2 9.4 -2 2 -28 21.4 8 2 -2 -28 13.7 10.1 28 -2 2 10.5 9.7 2 2 -28 16.3 10.3 28 2 -2 18.4 9.8 28 2 2 14.3 9.5 -2 -2 -28 17.9 9 28 4 0 188.78 14.4 0 4 -28 122.29 13.7 28 0 -4 170.28 13.6 0 -4 -28 160.88 14.3 28 0 4 138.49 13.7 28 -4 0 147.09 13.6 28 2 -4 313.87 19.5 28 -2 4 280.47 18.5 2 4 -28 250.67 18.7 28 4 2 306.17 18.9 28 -4 2 269.27 18.4 28 4 -2 277.57 18.3 28 -2 -4 317.47 19.7 2 -4 -28 219.88 18 28 2 4 285.97 18.5 28 4 -4 908.51 45.4 28 -4 -4 925.21 45.8 28 -4 4 878.31 45.9 28 4 4 912.81 45.9 28 6 0 21.4 10.4 28 -6 0 23.9 10.7 0 -6 -28 8.6 11.6 0 6 -28 16.8 11.2 28 0 -6 9.3 9.1 28 0 6 17 11.3 28 6 2 109.89 12.8 28 -6 -2 95.79 12.4 28 2 -6 107.49 11.8 28 -2 6 81.79 13 2 -6 -28 100.59 13.1 28 -2 -6 103.39 11.8 28 6 -2 88.19 11.8 28 2 6 94.39 13.1 28 -6 2 117.19 13.3 28 4 -6 587.94 31.7 -28 -6 4 511.75 31.7 28 6 4 587.84 32.4 28 -4 6 550.94 33 28 -6 -4 605.84 32.4 28 6 -4 585.14 31.6 28 -4 -6 577.34 31.4 28 -6 -6 333.77 21.3 28 8 0 166.58 14.8 28 -8 0 188.88 15.9 -28 -8 0 173.78 16.9 -28 -8 2 41.1 12.3 2 8 -28 60.19 13 28 -8 -2 67.29 12.8 28 8 2 79.09 12.5 -28 -8 -2 56.29 13.5 28 -8 2 62.59 12.9 28 8 -2 68.89 11.9 2 -8 -28 45.7 12.7 28 -8 -4 24.8 11.6 28 8 4 18.7 11.6 28 8 -4 15 10.6 28 -8 4 31 13.5 -28 -10 0 30.6 13.1 28 -10 0 38.4 13.3 28 10 0 36.8 11.8 28 10 2 7 11.5 28 -10 -2 7.5 12.6 28 -10 2 10 13.4 28 10 -2 1.6 11.1 -28 -10 -2 -1.4 13 28 10 4 185.88 17.1 -28 -10 -4 148.29 17.8 28 -12 0 26.6 15.5 29 -1 -1 20.7 10.6 29 -1 1 29.2 11.2 29 1 -1 25.7 11.1 29 1 1 31 11.4 3 -1 -29 147.59 16 29 -1 3 179.68 16 29 1 -3 187.38 15.4 29 -3 -1 196.08 15.7 29 3 1 203.38 16.2 29 3 -1 199.98 16.2 29 -1 -3 173.98 15.1 29 1 3 158.78 15.5 29 -3 1 164.18 15.7 29 -3 3 661.03 37.9 29 3 3 689.43 37.9 3 -3 -29 681.53 38.3 29 -3 -3 720.03 37.6 29 3 -3 729.63 36.9 29 1 -5 172.48 15.4 29 5 1 206.18 16.6 29 -5 -1 201.18 16.4 29 -1 -5 224.68 16.4 29 5 -1 168.58 15.5 29 -5 1 186.38 16.3 29 -5 -3 862.41 42.8 29 3 -5 753.02 43 29 5 3 839.22 43.1 29 -5 3 793.12 43 29 5 -3 834.42 42.6 29 -3 -5 827.42 42.4 29 -7 -1 2 12.3 29 7 1 3.6 11.6 29 7 -1 3.6 12.1 29 -7 1 4.9 13.7 29 -7 -3 263.97 19.6 29 7 3 227.88 19 29 9 1 72.39 14.6 29 -9 -1 63.29 15.2 29 -9 1 64.59 15.8 -29 -9 -1 59.79 16.6 30 0 0 278.47 20.8 30 0 -2 -3.2 12.3 30 0 2 1 13 30 -2 0 9.4 12.6 30 2 0 0.3 12.6 30 -2 -2 90.29 14 30 2 -2 121.19 15.2 30 -4 0 135.59 16.5 30 4 0 139.89 15.5 30 -4 -2 481.65 31 30 4 -2 491.95 30.5