#------------------------------------------------------------------------------ #$Date: 2017-12-05 15:01:10 +0200 (Tue, 05 Dec 2017) $ #$Revision: 203979 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/42/4514293.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4514293 loop_ _publ_author_name 'Lortie, John L.' 'Dudding, Travis' 'Gabidullin, Bulat M.' 'Nikonov, Georgii I.' _publ_section_title ; Zinc-Catalyzed Hydrosilylation and Hydroboration of N-Heterocycles ; _journal_issue 12 _journal_name_full 'ACS Catalysis' _journal_page_first 8454 _journal_paper_doi 10.1021/acscatal.7b02811 _journal_volume 7 _journal_year 2017 _chemical_formula_sum 'C46 H48 N4 Zn' _chemical_formula_weight 722.25 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _audit_creation_method SHELXL-2014/7 _cell_angle_alpha 66.838(2) _cell_angle_beta 73.267(2) _cell_angle_gamma 64.731(2) _cell_formula_units_Z 2 _cell_length_a 12.1191(18) _cell_length_b 13.987(2) _cell_length_c 14.338(2) _cell_measurement_reflns_used 9366 _cell_measurement_temperature 200(2) _cell_measurement_theta_max 26.41 _cell_measurement_theta_min 2.61 _cell_volume 1999.6(5) _computing_cell_refinement 'APEX II (Bruker, 2009)' _computing_data_collection 'APEX II (Bruker, 2009)' _computing_data_reduction 'SAINT (Bruker)' _computing_molecular_graphics 'Mercury (Macrae et al., 2008)' _computing_publication_material 'CIFTAB (Sheldrick, 1997)' _computing_structure_refinement 'SHELXL-2014/7 (Sheldrick, 2014)' _computing_structure_solution 'XT (Sheldrick, 2014)' _diffrn_ambient_temperature 200(2) _diffrn_measured_fraction_theta_full 0.998 _diffrn_measured_fraction_theta_max 0.958 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0229 _diffrn_reflns_av_unetI/netI 0.0330 _diffrn_reflns_Laue_measured_fraction_full 0.998 _diffrn_reflns_Laue_measured_fraction_max 0.958 _diffrn_reflns_limit_h_max 15 _diffrn_reflns_limit_h_min -15 _diffrn_reflns_limit_k_max 18 _diffrn_reflns_limit_k_min -18 _diffrn_reflns_limit_l_max 19 _diffrn_reflns_limit_l_min -18 _diffrn_reflns_number 24240 _diffrn_reflns_point_group_measured_fraction_full 0.998 _diffrn_reflns_point_group_measured_fraction_max 0.958 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 28.417 _diffrn_reflns_theta_min 1.878 _exptl_absorpt_coefficient_mu 0.650 _exptl_absorpt_correction_T_max 0.7457 _exptl_absorpt_correction_T_min 0.6817 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS, Bruker (2003)' _exptl_crystal_colour orange _exptl_crystal_density_diffrn 1.200 _exptl_crystal_description block _exptl_crystal_F_000 764 _exptl_crystal_size_max 0.526 _exptl_crystal_size_mid 0.353 _exptl_crystal_size_min 0.286 _refine_diff_density_max 0.501 _refine_diff_density_min -0.411 _refine_diff_density_rms 0.055 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.056 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 508 _refine_ls_number_reflns 9633 _refine_ls_number_restraints 274 _refine_ls_restrained_S_all 1.069 _refine_ls_R_factor_all 0.0751 _refine_ls_R_factor_gt 0.0457 _refine_ls_shift/su_max 0.007 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0794P)^2^+0.5077P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1240 _refine_ls_wR_factor_ref 0.1462 _reflns_Friedel_coverage 0.000 _reflns_number_gt 6920 _reflns_number_total 9633 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs7b02811_si_002.cif _cod_data_source_block shelx _cod_depositor_comments 'Adding full bibliography for 4514293.cif.' _cod_database_code 4514293 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_min 0.726 _shelx_estimated_absorpt_t_max 0.836 _shelx_res_file ; shelx.res created by SHELXL-2014/7 TITL gn219 in P-1 CELL 0.71073 12.1191 13.9870 14.3380 66.838 73.267 64.731 ZERR 2.00 0.0018 0.0020 0.0021 0.002 0.002 0.002 LATT 1 SFAC C H N ZN UNIT 92 96 8 2 MERG 2 OMIT -3.00 180.00 DFIX 1.52 0.02 C40 C41 C47 C48 SADI 0.04 C40 C42 C40 C46 C47 C49 C47 C53 RIGU C40 > C46 RIGU C47 > C53 SIMU C40 > C46 SIMU C47 > C53 ISOR 0.02 C40 > C46 ISOR 0.02 C47 > C53 FLAT C40 > C46 FLAT C47 > C53 DFIX -3.55 0.001 C23 C50 FMAP 2 PLAN 5 SIZE 0.286 0.353 0.526 ACTA BOND $H CONF L.S. 27 TEMP -73.10 WGHT 0.079400 0.507700 FVAR 0.59113 0.60067 ZN1 4 0.236359 0.263569 0.282814 11.00000 0.04126 0.04384 = 0.03868 -0.01034 -0.00821 -0.01625 C1 1 0.151049 0.268827 0.596309 11.00000 0.05476 0.05947 = 0.04573 -0.02070 -0.00701 -0.02147 AFIX 137 H1A 2 0.068400 0.326210 0.594056 11.00000 -1.50000 H1B 2 0.199606 0.283728 0.629509 11.00000 -1.50000 H1C 2 0.144446 0.195662 0.635332 11.00000 -1.50000 AFIX 0 C2 1 0.213889 0.270184 0.488259 11.00000 0.04339 0.03475 = 0.04184 -0.01129 -0.01042 -0.01021 C3 1 0.332593 0.275179 0.463055 11.00000 0.04630 0.04480 = 0.04543 -0.01154 -0.01233 -0.01760 AFIX 43 H3A 2 0.353603 0.298677 0.507247 11.00000 -1.20000 AFIX 0 C4 1 0.424286 0.250209 0.381564 11.00000 0.04120 0.04392 = 0.04639 -0.00371 -0.01228 -0.01792 C5 1 0.552738 0.236131 0.388980 11.00000 0.04890 0.08434 = 0.06532 -0.02411 -0.01207 -0.02731 AFIX 137 H5A 2 0.606272 0.157865 0.400205 11.00000 -1.50000 H5B 2 0.549324 0.259109 0.446416 11.00000 -1.50000 H5C 2 0.585793 0.282305 0.325122 11.00000 -1.50000 AFIX 0 C6 1 0.045018 0.240265 0.469082 11.00000 0.04118 0.04578 = 0.03649 -0.01515 -0.00297 -0.01757 C7 1 0.053596 0.129317 0.516950 11.00000 0.04813 0.04827 = 0.04099 -0.01277 -0.00697 -0.02042 C8 1 -0.054174 0.106078 0.557657 11.00000 0.05956 0.06157 = 0.05078 -0.01413 -0.00113 -0.03502 AFIX 43 H8A 2 -0.049606 0.031230 0.592093 11.00000 -1.20000 AFIX 0 C9 1 -0.167911 0.190569 0.548634 11.00000 0.05067 0.08217 = 0.06535 -0.03422 0.00702 -0.03660 AFIX 43 H9A 2 -0.241205 0.173800 0.575815 11.00000 -1.20000 AFIX 0 C10 1 -0.174737 0.299402 0.500016 11.00000 0.03872 0.07095 = 0.06293 -0.03521 -0.00169 -0.01450 AFIX 43 H10A 2 -0.253363 0.357015 0.493539 11.00000 -1.20000 AFIX 0 C11 1 -0.069669 0.326707 0.460403 11.00000 0.04543 0.05188 = 0.04988 -0.02223 -0.00628 -0.01448 C12 1 -0.078685 0.445549 0.410535 11.00000 0.05081 0.04663 = 0.08829 -0.02137 -0.01398 -0.00597 AFIX 137 H12A 2 -0.032972 0.462469 0.444612 11.00000 -1.50000 H12B 2 -0.165450 0.494389 0.416373 11.00000 -1.50000 H12C 2 -0.043534 0.457583 0.337976 11.00000 -1.50000 AFIX 0 C13 1 0.177768 0.036846 0.523125 11.00000 0.05383 0.04238 = 0.06904 -0.00824 -0.01321 -0.01796 AFIX 137 H13A 2 0.166645 -0.034745 0.560781 11.00000 -1.50000 H13B 2 0.226883 0.048075 0.558870 11.00000 -1.50000 H13C 2 0.220541 0.037065 0.453742 11.00000 -1.50000 AFIX 0 C14 1 0.509637 0.191907 0.232521 11.00000 0.03879 0.07491 = 0.04125 -0.01526 -0.00542 -0.02251 C15 1 0.548239 0.264499 0.142021 11.00000 0.05472 0.11509 = 0.04737 -0.00578 -0.00514 -0.04417 C16 1 0.642299 0.217019 0.072281 11.00000 0.06739 0.19930 = 0.04865 -0.02687 0.00877 -0.07203 AFIX 43 H16A 2 0.669395 0.264486 0.009640 11.00000 -1.20000 AFIX 0 C17 1 0.695595 0.105784 0.091449 11.00000 0.06799 0.21668 = 0.08221 -0.09422 0.01908 -0.05281 AFIX 43 H17A 2 0.758710 0.076265 0.042221 11.00000 -1.20000 AFIX 0 C18 1 0.659005 0.034742 0.182028 11.00000 0.05592 0.12715 = 0.10064 -0.07375 0.00126 -0.02002 AFIX 43 H18A 2 0.698123 -0.043448 0.195337 11.00000 -1.20000 AFIX 0 C19 1 0.565315 0.076652 0.254025 11.00000 0.04701 0.07868 = 0.06338 -0.03399 -0.00555 -0.01507 C20 1 0.520311 0.000056 0.350558 11.00000 0.07665 0.05310 = 0.08342 -0.01825 -0.01169 -0.00865 AFIX 137 H20A 2 0.570789 -0.077378 0.353823 11.00000 -1.50000 H20B 2 0.434068 0.013371 0.350637 11.00000 -1.50000 H20C 2 0.526730 0.014226 0.410163 11.00000 -1.50000 AFIX 0 C21 1 0.492343 0.388199 0.120321 11.00000 0.08891 0.11229 = 0.09234 0.03382 -0.01132 -0.06140 AFIX 137 H21A 2 0.556026 0.420917 0.083568 11.00000 -1.50000 H21B 2 0.457619 0.405319 0.185078 11.00000 -1.50000 H21C 2 0.426835 0.419241 0.078128 11.00000 -1.50000 AFIX 0 C22 1 0.318512 0.120437 0.153639 11.00000 0.05754 0.10306 = 0.09617 -0.06223 -0.00302 -0.02545 AFIX 43 H22A 2 0.389275 0.141127 0.131232 11.00000 -1.20000 AFIX 0 C23 1 0.320113 0.037243 0.126294 11.00000 0.07565 0.09362 = 0.09925 -0.06415 -0.00672 -0.01368 AFIX 43 H23A 2 0.393196 -0.000783 0.088973 11.00000 -1.20000 AFIX 0 C24 1 0.215653 0.005304 0.151846 11.00000 0.11511 0.07648 = 0.10318 -0.04953 -0.00608 -0.03883 AFIX 23 H24A 2 0.230353 -0.065853 0.208647 11.00000 -1.20000 H24B 2 0.206115 -0.007518 0.091913 11.00000 -1.20000 AFIX 0 C25 1 0.098692 0.089989 0.183089 11.00000 0.07683 0.05366 = 0.04981 -0.01174 -0.01288 -0.03339 C26 1 -0.017212 0.088119 0.186611 11.00000 0.10139 0.07579 = 0.05411 -0.00606 -0.02307 -0.05892 AFIX 43 H26A 2 -0.021430 0.034950 0.163447 11.00000 -1.20000 AFIX 0 C27 1 -0.124647 0.160380 0.222331 11.00000 0.07127 0.09913 = 0.05235 -0.00530 -0.01688 -0.05265 AFIX 43 H27A 2 -0.202141 0.157266 0.224419 11.00000 -1.20000 AFIX 0 C28 1 -0.117631 0.237067 0.254892 11.00000 0.05537 0.09226 = 0.04865 -0.01709 -0.00941 -0.03384 AFIX 43 H28A 2 -0.191112 0.286937 0.280970 11.00000 -1.20000 AFIX 0 C29 1 -0.005166 0.243102 0.250425 11.00000 0.05295 0.06459 = 0.04177 -0.01611 -0.00911 -0.02479 AFIX 43 H29A 2 -0.003523 0.298923 0.271435 11.00000 -1.20000 AFIX 0 C30 1 0.105732 0.169851 0.216071 11.00000 0.05737 0.04865 = 0.03668 -0.00626 -0.01272 -0.02672 C31 1 0.155403 0.433665 0.086215 11.00000 0.07179 0.06362 = 0.04729 -0.00507 -0.02147 -0.02847 AFIX 43 H31A 2 0.166369 0.365923 0.077853 11.00000 -1.20000 AFIX 0 C32 1 0.118015 0.532550 0.005296 11.00000 0.10004 0.08574 = 0.04774 0.00571 -0.03041 -0.04225 AFIX 43 H32A 2 0.108132 0.530800 -0.057313 11.00000 -1.20000 AFIX 0 C33 1 0.096215 0.630530 0.017706 11.00000 0.08334 0.06845 = 0.05862 0.01307 -0.02536 -0.02911 AFIX 43 H33A 2 0.066640 0.698550 -0.034895 11.00000 -1.20000 AFIX 0 C34 1 0.117471 0.631087 0.108414 11.00000 0.05163 0.04895 = 0.05752 0.00047 -0.00201 -0.01911 C35 1 0.100586 0.729629 0.126025 11.00000 0.07424 0.04572 = 0.07905 -0.00299 0.00515 -0.02284 AFIX 43 H35A 2 0.069447 0.799616 0.076061 11.00000 -1.20000 AFIX 0 C36 1 0.127847 0.725768 0.212127 11.00000 0.07973 0.04805 = 0.09065 -0.02392 0.01975 -0.03065 AFIX 43 H36A 2 0.115487 0.792796 0.222648 11.00000 -1.20000 AFIX 0 C37 1 0.174565 0.623053 0.286726 11.00000 0.07984 0.06337 = 0.06286 -0.02572 0.00874 -0.03614 AFIX 43 H37A 2 0.195688 0.621051 0.346512 11.00000 -1.20000 AFIX 0 C38 1 0.189954 0.525809 0.274122 11.00000 0.06207 0.04601 = 0.05113 -0.01140 -0.00436 -0.02290 AFIX 43 H38A 2 0.220252 0.456902 0.325576 11.00000 -1.20000 AFIX 0 C39 1 0.160889 0.527950 0.184949 11.00000 0.04258 0.04374 = 0.04509 -0.00656 -0.00225 -0.01671 N1 3 0.156640 0.263998 0.425713 11.00000 0.03846 0.03712 = 0.03845 -0.00947 -0.00755 -0.01413 N2 3 0.405932 0.236120 0.301771 11.00000 0.04159 0.04703 = 0.03900 -0.00689 -0.00593 -0.01869 N3 3 0.216880 0.177598 0.213689 11.00000 0.04452 0.05433 = 0.05111 -0.02132 -0.00749 -0.01750 N4 3 0.176177 0.429813 0.173507 11.00000 0.05108 0.04814 = 0.03951 -0.00414 -0.01240 -0.01954 PART 1 C40 1 0.229520 0.282377 0.856766 21.00000 0.15839 0.24133 = 0.16000 -0.08504 -0.05540 -0.06069 AFIX 137 H40A 2 0.234092 0.230845 0.926844 21.00000 -1.50000 H40B 2 0.218297 0.248634 0.813475 21.00000 -1.50000 H40C 2 0.159636 0.351835 0.857195 21.00000 -1.50000 AFIX 66 C41 1 0.346836 0.306623 0.815049 21.00000 0.21845 0.34441 = 0.26174 -0.10673 -0.05018 -0.11033 C42 1 0.417788 0.313574 0.871312 21.00000 0.21939 0.32661 = 0.23753 -0.10155 -0.04981 -0.12068 AFIX 43 H42 2 0.398173 0.294718 0.943824 21.00000 -1.20000 AFIX 65 C43 1 0.517439 0.348114 0.821480 21.00000 0.24775 0.36602 = 0.25712 -0.10198 -0.04474 -0.14985 AFIX 43 H43 2 0.565930 0.352864 0.859934 21.00000 -1.20000 AFIX 65 C44 1 0.546139 0.375703 0.715384 21.00000 0.32415 0.41241 = 0.30658 -0.10670 -0.04795 -0.17295 AFIX 43 H44 2 0.614246 0.399309 0.681326 21.00000 -1.20000 AFIX 65 C45 1 0.475189 0.368752 0.659120 21.00000 0.29118 0.38457 = 0.31262 -0.13414 -0.03685 -0.13658 AFIX 43 H45 2 0.494805 0.387608 0.586608 21.00000 -1.20000 AFIX 65 C46 1 0.375538 0.334213 0.708951 21.00000 0.28448 0.37244 = 0.26942 -0.12361 -0.03456 -0.13828 AFIX 43 H46 2 0.327046 0.329462 0.670497 21.00000 -1.20000 AFIX 0 PART 2 C47 1 0.494447 0.481936 0.642534 -21.00000 0.18053 0.19832 = 0.33462 -0.06564 -0.09814 -0.00428 AFIX 137 H47A 2 0.554938 0.489221 0.669780 -21.00000 -1.50000 H47B 2 0.430186 0.554940 0.619906 -21.00000 -1.50000 H47C 2 0.535654 0.453259 0.584275 -21.00000 -1.50000 AFIX 66 C48 1 0.439927 0.406774 0.720652 -21.00000 0.29387 0.26658 = 0.31615 -0.09738 -0.05775 -0.08393 C49 1 0.504787 0.293922 0.734644 -21.00000 0.30954 0.25309 = 0.30380 -0.08741 -0.04955 -0.07460 AFIX 43 H49 2 0.583669 0.269978 0.695846 -21.00000 -1.20000 AFIX 65 C50 1 0.454232 0.216104 0.805402 -21.00000 0.35302 0.28751 = 0.35470 -0.09264 -0.02056 -0.09716 AFIX 43 H50 2 0.498561 0.138975 0.814964 -21.00000 -1.20000 AFIX 65 C51 1 0.338816 0.251138 0.862168 -21.00000 0.33860 0.28485 = 0.34086 -0.10548 -0.03131 -0.10278 AFIX 43 H51 2 0.304264 0.197952 0.910528 -21.00000 -1.20000 AFIX 65 C52 1 0.273955 0.363990 0.848178 -21.00000 0.37287 0.29510 = 0.35896 -0.11151 -0.01630 -0.10392 AFIX 43 H52 2 0.195074 0.387933 0.886976 -21.00000 -1.20000 AFIX 65 C53 1 0.324509 0.441809 0.777420 -21.00000 0.32502 0.27114 = 0.34406 -0.11675 -0.02095 -0.08960 AFIX 43 H53 2 0.280179 0.518938 0.767858 -21.00000 -1.20000 AFIX 0 HKLF 4 REM gn219 in P-1 REM R1 = 0.0457 for 6920 Fo > 4sig(Fo) and 0.0751 for all 9633 data REM 508 parameters refined using 274 restraints END WGHT 0.0791 0.4859 REM Highest difference peak 0.501, deepest hole -0.411, 1-sigma level 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5.40 3.20 -3 -15 3 5.40 4.00 2 15 -3 30.10 4.10 2 15 -3 20.70 3.90 -2 -15 3 20.40 4.50 1 15 -3 -3.90 3.20 -1 -15 3 1.40 3.90 0 15 -3 -1.50 3.70 10 14 -3 -1.00 3.50 -10 -14 3 1.70 4.70 9 14 -3 -3.00 3.20 -9 -14 3 1.80 4.40 8 14 -3 11.60 3.50 -8 -14 3 13.30 4.40 7 14 -3 91.89 6.90 -7 -14 3 81.09 7.60 6 14 -3 9.30 3.30 -6 -14 3 4.80 3.80 5 14 -3 8.40 3.10 -5 -14 3 2.40 3.60 -4 -14 3 4.70 5.00 -4 -14 3 8.30 3.70 3 14 -3 6.60 3.00 -3 -14 3 5.50 4.90 -3 -14 3 10.50 3.70 2 14 -3 0.00 2.90 -2 -14 3 1.90 3.50 -2 -14 3 -4.40 4.50 1 14 -3 18.60 3.60 -1 -14 3 23.70 4.30 -1 -14 3 20.70 5.50 0 14 -3 -7.70 3.00 0 -14 3 -1.20 3.60 0 -14 3 -2.50 4.70 -1 14 -3 2.60 3.70 1 -14 3 3.60 5.00 1 -14 3 10.60 4.00 -2 14 -3 1.80 4.00 2 -14 3 11.40 4.20 2 -14 3 10.40 5.50 -11 -13 3 19.20 5.00 -10 -13 3 29.10 5.00 9 13 -3 -0.60 2.90 -9 -13 3 -2.80 3.90 8 13 -3 110.89 6.80 -8 -13 3 106.99 8.00 7 13 -3 9.80 3.10 -7 -13 3 1.70 3.50 6 13 -3 21.60 3.40 -6 -13 3 15.60 3.80 -5 -13 3 -1.00 3.20 -5 -13 3 -4.10 4.10 4 13 -3 38.10 4.30 -4 -13 3 51.79 5.80 -4 -13 3 48.90 6.00 3 13 -3 23.10 3.10 -3 -13 3 30.30 4.10 -3 -13 3 22.50 4.90 2 13 -3 20.30 3.20 -2 -13 3 21.10 4.90 -2 -13 3 26.50 4.00 1 13 -3 -1.00 2.60 -1 -13 3 -0.10 4.20 -1 -13 3 -1.20 3.00 0 13 -3 -4.80 2.70 0 -13 3 -0.80 4.30 0 -13 3 2.10 3.10 -1 13 -3 -3.00 3.10 1 -13 3 2.10 4.40 1 -13 3 5.50 3.50 -2 13 -3 0.80 3.40 2 -13 3 7.00 3.70 2 -13 3 1.00 4.50 -3 13 -3 -1.80 3.50 3 -13 3 -1.80 4.70 3 -13 3 5.50 3.90 4 -13 3 12.30 4.30 12 12 -3 10.40 4.10 11 12 -3 6.30 3.30 -10 -12 3 8.20 4.30 9 12 -3 61.59 5.90 -9 -12 3 43.90 4.80 8 12 -3 18.30 3.30 -8 -12 3 15.00 4.00 7 12 -3 172.48 7.10 -7 -12 3 163.48 7.70 -6 -12 3 8.10 4.30 -6 -12 3 9.90 3.40 5 12 -3 65.09 4.30 -5 -12 3 66.89 8.20 -5 -12 3 60.99 5.90 4 12 -3 34.00 3.80 -4 -12 3 33.00 4.90 -4 -12 3 36.00 3.90 3 12 -3 38.30 3.90 -3 -12 3 38.50 4.90 -3 -12 3 44.80 5.30 2 12 -3 3.60 2.40 -2 -12 3 1.70 3.90 -2 -12 3 4.20 2.90 1 12 -3 58.79 4.70 -1 -12 3 49.40 5.40 -1 -12 3 68.79 5.70 0 12 -3 8.90 2.80 0 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3 9.10 3.00 2 -10 3 10.30 3.70 -3 10 -3 26.40 3.60 3 -10 3 25.90 4.20 3 -10 3 21.70 3.50 -4 10 -3 10.20 3.20 4 -10 3 11.90 3.40 4 -10 3 9.00 3.70 -5 10 -3 40.10 4.20 5 -10 3 53.79 6.30 -6 10 -3 14.10 3.80 6 -10 3 17.50 4.10 -7 10 -3 -1.60 3.90 7 -10 3 -0.20 3.80 14 9 -3 -5.50 4.20 13 9 -3 24.00 4.70 -13 -9 3 18.10 4.60 12 9 -3 4.70 3.40 -12 -9 3 8.30 3.90 11 9 -3 21.50 3.80 -11 -9 3 30.30 4.20 10 9 -3 23.00 3.30 -10 -9 3 28.60 3.90 -9 -9 3 2.40 3.20 -9 -9 3 -0.50 2.80 8 9 -3 39.10 3.90 -8 -9 3 35.20 3.90 -8 -9 3 32.70 3.40 7 9 -3 86.09 3.70 -7 -9 3 87.99 5.70 -7 -9 3 87.99 4.70 -7 -9 3 86.59 6.70 6 9 -3 332.87 6.80 -6 -9 3 326.67 9.50 -6 -9 3 329.17 8.30 5 9 -3 0.50 1.40 -5 -9 3 1.10 2.50 -5 -9 3 2.30 3.10 4 9 -3 93.09 3.70 -4 -9 3 74.29 5.20 -4 -9 3 100.59 7.10 3 9 -3 102.59 3.90 -3 -9 3 97.89 6.70 -3 -9 3 101.79 5.10 2 9 -3 304.97 6.70 -2 -9 3 324.07 7.60 -2 -9 3 304.17 9.10 1 9 -3 21.80 2.40 -1 -9 3 21.50 2.90 -1 -9 3 27.80 3.80 0 9 -3 9.10 2.10 0 -9 3 6.20 3.20 0 -9 3 8.40 2.50 -1 9 -3 87.89 4.60 1 -9 3 82.69 6.50 1 -9 3 89.19 5.00 -2 9 -3 20.20 2.80 2 -9 3 18.50 3.50 2 -9 3 10.80 2.70 -3 9 -3 -2.90 2.30 3 -9 3 0.30 3.00 3 -9 3 -0.50 2.60 -4 9 -3 41.80 5.00 4 -9 3 51.29 5.50 4 -9 3 37.10 4.30 -5 9 -3 4.60 3.00 5 -9 3 11.10 3.40 -6 9 -3 6.80 3.30 6 -9 3 12.40 3.70 -7 9 -3 -3.10 3.40 7 -9 3 -0.10 3.60 -8 9 -3 8.50 4.00 8 -9 3 15.90 4.40 14 8 -3 8.10 4.50 13 8 -3 -4.30 3.70 -13 -8 3 3.80 4.00 12 8 -3 52.09 5.00 -12 -8 3 45.70 4.90 11 8 -3 14.70 3.50 -11 -8 3 12.90 3.70 10 8 -3 2.40 2.60 -10 -8 3 2.40 3.10 9 8 -3 116.29 5.60 -9 -8 3 104.89 5.80 8 8 -3 30.20 3.50 -8 -8 3 25.90 3.00 -8 -8 3 28.90 3.60 -8 -8 3 31.90 3.40 -7 -8 3 203.28 6.80 -7 -8 3 205.68 7.80 -7 -8 3 204.78 6.40 -7 -8 3 200.88 6.30 6 8 -3 22.10 2.50 -6 -8 3 19.90 2.70 -6 -8 3 19.60 3.00 -6 -8 3 18.90 3.40 5 8 -3 43.20 2.70 -5 -8 3 47.20 3.50 -5 -8 3 34.10 3.70 -5 -8 3 43.70 4.40 4 8 -3 28.60 2.50 -4 -8 3 30.50 3.80 -4 -8 3 25.00 3.40 3 8 -3 90.69 3.50 -3 -8 3 87.29 4.50 -3 -8 3 91.09 5.80 2 8 -3 10.40 1.70 -2 -8 3 13.20 2.30 -2 -8 3 11.70 2.90 1 8 -3 164.18 4.70 -1 -8 3 170.68 6.80 -1 -8 3 158.38 5.40 0 8 -3 6.20 1.80 0 -8 3 7.40 2.80 0 -8 3 13.60 2.40 -1 8 -3 4.90 2.00 1 -8 3 4.30 2.30 1 -8 3 -1.50 2.80 -2 8 -3 1.70 2.10 2 -8 3 -1.30 2.80 2 -8 3 0.10 2.40 -3 8 -3 163.88 5.70 3 -8 3 173.08 6.40 3 -8 3 161.88 7.20 -4 8 -3 45.00 4.60 4 -8 3 33.60 3.80 4 -8 3 42.40 4.90 -5 8 -3 59.49 4.90 5 -8 3 66.09 5.90 5 -8 3 56.39 5.90 -6 8 -3 0.10 3.00 6 -8 3 10.90 3.30 -7 8 -3 2.40 3.30 7 -8 3 15.80 3.70 -8 8 -3 -1.30 3.40 8 -8 3 6.00 3.70 -9 8 -3 11.10 4.30 9 -8 3 16.60 4.40 14 7 -3 -12.60 4.00 -14 -7 3 4.00 4.60 13 7 -3 23.80 4.60 -13 -7 3 26.30 4.80 12 7 -3 11.70 3.70 -12 -7 3 25.60 4.40 11 7 -3 18.30 3.50 -11 -7 3 14.80 3.80 10 7 -3 3.70 2.60 -10 -7 3 6.90 3.20 9 7 -3 13.80 2.60 -9 -7 3 10.40 2.40 -9 -7 3 14.50 3.20 8 7 -3 164.18 5.00 8 7 -3 168.78 5.80 -8 -7 3 164.48 5.50 -8 -7 3 165.38 6.20 -7 -7 3 86.49 5.00 -7 -7 3 85.39 5.80 -7 -7 3 92.99 4.70 -7 -7 3 91.29 5.40 -6 -7 3 193.88 6.10 -6 -7 3 194.98 5.80 -6 -7 3 192.38 6.80 -6 -7 3 188.08 5.60 5 7 -3 1.40 1.10 -5 -7 3 0.90 2.40 -5 -7 3 1.60 1.80 -5 -7 3 1.00 2.00 -5 -7 3 -0.40 2.00 4 7 -3 134.19 3.70 -4 -7 3 137.39 4.80 -4 -7 3 135.89 5.80 -4 -7 3 140.59 4.00 3 7 -3 20.80 1.70 3 7 -3 21.70 2.20 -3 -7 3 20.00 2.70 -3 -7 3 18.90 2.30 2 7 -3 155.78 4.10 -2 -7 3 148.99 5.90 -2 -7 3 147.19 4.60 1 7 -3 94.89 3.30 -1 -7 3 89.99 3.90 -1 -7 3 98.59 5.30 0 7 -3 23.80 2.50 0 -7 3 19.40 2.80 0 -7 3 22.10 2.30 -1 7 -3 18.20 2.10 1 -7 3 16.50 2.90 1 -7 3 19.50 2.40 -2 7 -3 8.00 1.80 2 -7 3 10.10 2.80 2 -7 3 5.90 2.20 -3 7 -3 37.70 3.70 3 -7 3 33.60 4.30 3 -7 3 32.20 3.60 -4 7 -3 274.17 7.00 4 -7 3 270.57 7.50 4 -7 3 274.17 8.20 -5 7 -3 8.20 2.50 5 -7 3 12.10 2.90 5 -7 3 8.40 2.70 -6 7 -3 74.39 5.40 6 -7 3 74.89 5.70 -7 7 -3 3.90 3.00 7 -7 3 5.40 3.20 -8 7 -3 26.20 4.00 8 -7 3 36.60 4.50 -9 7 -3 6.30 3.80 9 -7 3 20.10 4.10 -10 7 -3 5.60 4.00 10 -7 3 5.50 4.10 14 6 -3 0.80 4.30 -14 -6 3 25.00 5.30 13 6 -3 -5.40 3.50 -13 -6 3 -1.70 3.90 12 6 -3 47.20 4.70 -12 -6 3 55.99 6.60 11 6 -3 0.20 2.90 -11 -6 3 1.50 3.30 10 6 -3 0.00 2.30 -10 -6 3 3.30 2.20 -10 -6 3 1.10 3.00 9 6 -3 62.09 4.80 -9 -6 3 69.19 5.20 -9 -6 3 64.39 4.30 8 6 -3 60.79 4.30 -8 -6 3 59.89 4.80 -8 -6 3 61.09 4.20 -7 -6 3 234.88 6.90 -7 -6 3 230.98 6.50 -7 -6 3 221.98 6.80 -7 -6 3 221.88 6.00 -6 -6 3 50.39 4.20 -6 -6 3 37.10 4.60 -6 -6 3 45.00 3.60 -6 -6 3 45.20 3.80 -5 -6 3 67.99 4.60 -5 -6 3 71.29 3.80 -5 -6 3 70.49 3.60 -5 -6 3 69.49 3.90 -4 -6 3 13.60 1.80 -4 -6 3 14.10 2.10 -4 -6 3 14.50 2.30 -4 -6 3 13.40 2.00 3 6 -3 198.28 4.30 -3 -6 3 198.28 4.90 -3 -6 3 193.88 4.30 -3 -6 3 199.58 5.90 2 6 -3 182.78 3.30 2 6 -3 184.68 4.20 -2 -6 3 178.88 5.60 -2 -6 3 185.48 4.70 1 6 -3 207.78 4.50 -1 -6 3 195.78 5.70 -1 -6 3 199.98 4.80 0 6 -3 54.29 2.60 0 -6 3 53.99 3.10 0 -6 3 55.89 4.00 -1 6 -3 149.59 4.10 1 -6 3 151.78 5.50 1 -6 3 151.78 4.40 -2 6 -3 11.40 1.80 2 -6 3 8.20 1.90 2 -6 3 6.50 2.30 -3 6 -3 452.85 8.40 3 -6 3 443.76 8.60 3 -6 3 449.06 9.30 -4 6 -3 125.39 5.00 4 -6 3 118.59 5.40 4 -6 3 118.99 5.70 -5 6 -3 130.89 5.50 5 -6 3 144.39 6.00 5 -6 3 120.19 5.70 -6 6 -3 1.20 2.40 6 -6 3 -0.40 2.70 -7 6 -3 39.80 4.70 7 -6 3 33.20 3.90 -8 6 -3 11.60 3.20 8 -6 3 5.80 3.30 -9 6 -3 11.70 3.60 9 -6 3 20.50 4.00 -10 6 -3 0.00 3.60 10 -6 3 10.60 4.00 -11 6 -3 4.30 3.80 11 -6 3 5.50 4.30 14 5 -3 -11.70 4.00 -14 -5 3 1.50 4.50 13 5 -3 4.40 4.00 -13 -5 3 12.50 4.30 12 5 -3 4.10 3.40 -12 -5 3 14.80 4.00 11 5 -3 75.69 6.10 -11 -5 3 75.99 6.30 10 5 -3 3.00 2.50 -10 -5 3 4.90 2.20 -10 -5 3 11.40 3.20 9 5 -3 34.60 4.20 -9 -5 3 37.00 4.00 -9 -5 3 30.00 3.50 8 5 -3 157.38 5.70 -8 -5 3 156.58 5.30 -8 -5 3 157.58 6.00 7 5 -3 189.08 5.50 -7 -5 3 193.18 5.90 -7 -5 3 191.18 5.40 -7 -5 3 205.48 6.00 -6 -5 3 48.00 3.40 -6 -5 3 57.39 3.80 -6 -5 3 61.99 4.00 -6 -5 3 51.09 4.10 -5 -5 3 514.15 8.60 -5 -5 3 513.15 8.80 -5 -5 3 523.95 9.10 -5 -5 3 517.95 8.60 -4 -5 3 603.24 9.10 -4 -5 3 612.34 9.40 -4 -5 3 603.24 10.00 -4 -5 3 601.44 9.40 -3 -5 3 1.90 1.60 -3 -5 3 4.20 1.50 -3 -5 3 3.00 1.20 -3 -5 3 -0.30 1.20 2 5 -3 1559.54 19.40 2 5 -3 1576.74 18.50 -2 -5 3 1593.74 19.50 -2 -5 3 1544.75 20.50 1 5 -3 52.49 2.30 1 5 -3 53.29 1.60 -1 -5 3 56.09 2.60 -1 -5 3 53.99 3.40 0 5 -3 29.90 1.90 0 -5 3 30.10 2.40 0 -5 3 31.70 3.20 -1 5 -3 11.10 1.40 1 -5 3 9.20 1.90 1 -5 3 10.40 1.60 -2 5 -3 88.39 3.30 2 -5 3 89.79 3.60 2 -5 3 86.99 4.10 -3 5 -3 8.80 1.60 3 -5 3 8.80 2.00 3 -5 3 11.70 2.00 -4 5 -3 450.15 8.30 4 -5 3 452.05 8.80 4 -5 3 446.66 8.50 -5 5 -3 10.90 2.30 5 -5 3 12.10 2.50 5 -5 3 15.40 2.70 -6 5 -3 93.99 4.80 6 -5 3 84.59 5.00 6 -5 3 80.39 5.30 -7 5 -3 0.80 2.40 7 -5 3 0.00 2.60 -8 5 -3 95.79 5.60 8 -5 3 99.79 6.20 -9 5 -3 14.50 3.40 9 -5 3 16.80 3.70 -10 5 -3 8.20 3.50 10 -5 3 18.70 4.10 -11 5 -3 2.80 3.70 11 -5 3 6.30 4.00 -12 5 -3 -3.00 3.90 14 4 -3 0.40 4.30 -14 -4 3 3.60 4.50 13 4 -3 -8.40 3.40 -13 -4 3 -0.80 3.90 12 4 -3 18.80 4.10 -12 -4 3 21.60 4.30 11 4 -3 6.50 3.20 -11 -4 3 5.60 2.60 -11 -4 3 5.50 3.40 10 4 -3 -2.60 2.30 -10 -4 3 1.90 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3.60 -2 -14 4 24.80 4.30 -2 -14 4 14.80 5.50 1 14 -4 4.10 3.20 -1 -14 4 3.10 5.00 -1 -14 4 9.20 3.90 0 14 -4 20.20 4.00 0 -14 4 23.70 5.90 0 -14 4 30.10 4.60 -1 14 -4 13.00 4.00 1 -14 4 26.90 4.60 1 -14 4 18.70 6.00 9 13 -4 28.30 4.00 8 13 -4 4.10 3.10 7 13 -4 77.69 6.20 -6 -13 4 -1.70 4.40 -6 -13 4 -4.00 3.30 -5 -13 4 22.10 3.90 -5 -13 4 38.30 5.60 4 13 -4 6.40 2.60 -4 -13 4 7.60 3.50 -4 -13 4 5.90 4.50 3 13 -4 49.99 4.90 -3 -13 4 57.79 6.20 -3 -13 4 42.30 5.60 2 13 -4 -2.20 2.60 -2 -13 4 -3.10 3.00 -2 -13 4 -4.00 4.20 1 13 -4 2.70 2.90 -1 -13 4 -1.40 4.40 -1 -13 4 3.30 3.30 0 13 -4 0.80 3.00 0 -13 4 0.40 4.50 0 -13 4 3.50 3.40 -1 13 -4 6.50 3.50 1 -13 4 8.60 3.70 1 -13 4 5.40 4.80 -2 13 -4 -4.50 3.50 2 -13 4 2.40 3.60 2 -13 4 -5.00 4.50 3 -13 4 12.20 4.20 3 -13 4 10.30 5.10 9 12 -4 27.40 3.70 8 12 -4 153.98 7.10 -8 -12 4 134.09 7.60 -7 -12 4 -2.70 3.30 -7 -12 4 -0.80 4.10 -6 -12 4 48.30 4.70 -6 -12 4 38.50 5.20 5 12 -4 0.30 2.10 -5 -12 4 0.30 4.00 -5 -12 4 -0.10 3.00 4 12 -4 66.69 4.60 -4 -12 4 65.79 8.10 -4 -12 4 63.39 5.70 3 12 -4 1.30 2.30 -3 -12 4 1.10 3.00 -3 -12 4 4.60 4.10 2 12 -4 85.19 5.30 -2 -12 4 80.79 6.20 -2 -12 4 92.69 8.30 1 12 -4 5.50 2.70 -1 -12 4 3.60 3.00 -1 -12 4 2.00 4.10 0 12 -4 2.80 2.80 0 -12 4 6.40 4.30 0 -12 4 6.30 3.20 -1 12 -4 31.50 3.80 1 -12 4 37.40 4.10 1 -12 4 31.80 5.10 -2 12 -4 -1.40 3.00 2 -12 4 -0.50 3.10 2 -12 4 0.40 4.20 -3 12 -4 -3.50 3.20 3 -12 4 2.80 3.40 3 -12 4 -2.60 4.30 -4 12 -4 5.30 3.90 4 -12 4 20.30 4.30 5 -12 4 2.60 3.90 9 11 -4 42.70 5.00 -9 -11 4 25.70 4.30 8 11 -4 51.89 5.00 -8 -11 4 33.80 4.30 -7 -11 4 28.20 4.10 -7 -11 4 27.60 4.60 6 11 -4 12.20 2.30 -6 -11 4 18.50 3.50 -6 -11 4 13.10 4.10 5 11 -4 81.59 4.50 -5 -11 4 86.19 7.90 -5 -11 4 75.79 5.50 4 11 -4 -2.30 1.80 -4 -11 4 -1.60 2.70 -4 -11 4 -0.30 3.60 3 11 -4 116.59 5.20 -3 -11 4 135.89 8.40 -3 -11 4 120.69 6.20 2 11 -4 -0.40 2.10 -2 -11 4 5.50 2.90 -2 -11 4 0.20 3.60 1 11 -4 25.30 3.00 -1 -11 4 30.20 4.70 -1 -11 4 30.10 3.60 0 11 -4 6.40 2.60 0 -11 4 1.80 3.90 0 -11 4 2.60 2.80 -1 11 -4 13.40 3.10 1 -11 4 12.70 3.10 1 -11 4 9.60 4.20 -2 11 -4 3.40 2.90 2 -11 4 10.20 3.30 2 -11 4 4.60 3.90 -3 11 -4 26.00 3.80 3 -11 4 33.00 4.20 3 -11 4 29.70 4.80 -4 11 -4 -6.80 3.10 4 -11 4 -0.10 4.10 4 -11 4 3.50 3.40 -5 11 -4 3.30 3.70 5 -11 4 15.50 4.10 6 -11 4 5.50 4.10 -13 -10 4 11.60 4.50 -12 -10 4 1.60 4.00 11 10 -4 26.60 4.10 -11 -10 4 35.10 4.50 10 10 -4 60.49 5.70 -9 -10 4 -0.70 3.30 -8 -10 4 93.79 6.70 7 10 -4 7.80 2.00 -7 -10 4 10.30 3.30 -7 -10 4 4.80 3.60 6 10 -4 31.40 3.30 -6 -10 4 30.30 4.20 -6 -10 4 32.30 3.60 5 10 -4 5.70 1.90 -5 -10 4 8.10 2.80 -5 -10 4 6.70 3.50 4 10 -4 95.29 4.40 -4 -10 4 94.09 5.50 -4 -10 4 99.99 7.40 3 10 -4 2.90 1.90 -3 -10 4 5.90 3.40 -3 -10 4 3.90 2.60 2 10 -4 52.39 3.80 -2 -10 4 51.19 4.80 -2 -10 4 42.60 4.50 1 10 -4 6.00 2.10 -1 -10 4 5.40 3.50 -1 -10 4 7.80 2.60 0 10 -4 24.80 2.90 0 -10 4 31.80 4.30 0 -10 4 26.80 3.30 -1 10 -4 -1.40 2.30 1 -10 4 -1.00 3.40 1 -10 4 2.30 2.50 -2 10 -4 53.89 4.80 2 -10 4 62.19 5.30 2 -10 4 41.20 4.80 -3 10 -4 10.70 3.10 3 -10 4 13.80 4.10 3 -10 4 12.30 3.20 -4 10 -4 62.09 6.00 4 -10 4 60.49 7.30 4 -10 4 60.19 6.20 -5 10 -4 -4.50 3.10 5 -10 4 -2.80 3.20 -6 10 -4 4.40 3.70 6 -10 4 9.00 3.80 7 -10 4 13.70 4.40 -13 -9 4 1.00 4.30 12 9 -4 8.60 3.90 -12 -9 4 18.50 4.30 11 9 -4 0.90 3.20 -11 -9 4 5.60 3.50 10 9 -4 -0.60 2.60 -10 -9 4 -2.00 3.00 9 9 -4 81.19 5.10 -9 -9 4 75.59 5.80 -8 -9 4 56.09 5.20 -8 -9 4 59.59 5.80 -8 -9 4 57.29 6.70 -8 -9 4 54.69 4.90 7 9 -4 4.30 1.60 -7 -9 4 0.60 2.70 -7 -9 4 -3.10 3.00 6 9 -4 80.89 3.80 -6 -9 4 78.29 5.40 -6 -9 4 82.89 6.70 5 9 -4 162.78 5.00 -5 -9 4 181.68 7.90 -5 -9 4 171.08 6.30 4 9 -4 33.90 3.20 -4 -9 4 36.70 4.50 -4 -9 4 26.60 3.90 3 9 -4 200.18 5.60 -3 -9 4 206.88 6.50 -3 -9 4 206.98 8.10 2 9 -4 2.90 1.80 -2 -9 4 3.30 2.40 -2 -9 4 4.10 3.20 1 9 -4 63.99 3.80 -1 -9 4 63.89 4.70 -1 -9 4 61.89 6.30 0 9 -4 0.30 1.90 0 -9 4 0.50 2.30 0 -9 4 0.50 3.10 -1 9 -4 90.09 4.90 1 -9 4 86.49 6.80 1 -9 4 95.29 5.30 -2 9 -4 30.30 3.20 2 -9 4 28.00 4.10 2 -9 4 32.40 3.50 -3 9 -4 45.20 4.60 3 -9 4 52.99 5.10 3 -9 4 43.30 4.60 -4 9 -4 7.60 3.00 4 -9 4 7.40 3.70 4 -9 4 12.70 3.30 -5 9 -4 41.00 4.20 5 -9 4 43.30 4.40 5 -9 4 33.40 4.40 -6 9 -4 2.40 3.20 6 -9 4 4.50 3.40 -7 9 -4 0.60 3.50 7 -9 4 3.10 3.70 -8 9 -4 -6.10 4.00 8 -9 4 3.70 4.00 13 8 -4 13.30 4.30 -13 -8 4 23.60 4.90 12 8 -4 -6.80 3.30 -12 -8 4 3.30 3.80 11 8 -4 9.30 3.30 -11 -8 4 17.90 3.90 10 8 -4 9.00 2.90 -10 -8 4 10.10 3.40 9 8 -4 35.80 4.50 -9 -8 4 28.80 3.70 -8 -8 4 104.59 5.40 -8 -8 4 104.29 6.60 -8 -8 4 114.59 5.70 -8 -8 4 104.69 6.10 -7 -8 4 71.69 4.90 -7 -8 4 68.89 5.90 -7 -8 4 73.39 5.40 -7 -8 4 73.09 4.70 6 8 -4 141.59 4.60 -6 -8 4 136.29 5.30 -6 -8 4 147.79 6.00 -6 -8 4 147.19 7.10 5 8 -4 16.10 2.00 -5 -8 4 18.10 2.80 -5 -8 4 19.90 3.50 4 8 -4 54.49 3.10 -4 -8 4 57.79 6.00 -4 -8 4 58.59 4.50 3 8 -4 3.50 1.50 -3 -8 4 -0.30 2.10 -3 -8 4 -1.70 2.80 2 8 -4 179.48 5.10 -2 -8 4 176.18 7.30 -2 -8 4 169.58 5.60 1 8 -4 151.38 4.80 -1 -8 4 152.88 5.40 -1 -8 4 149.29 7.00 0 8 -4 50.39 3.50 0 -8 4 48.90 4.20 0 -8 4 50.69 5.80 -1 8 -4 107.99 4.70 1 -8 4 113.99 6.80 1 -8 4 118.69 5.40 -2 8 -4 43.10 3.80 2 -8 4 40.60 4.10 2 -8 4 48.30 4.70 -3 8 -4 20.50 2.80 3 -8 4 21.80 3.00 3 -8 4 17.20 3.40 -4 8 -4 146.29 6.00 4 -8 4 175.08 6.90 4 -8 4 159.28 7.60 -5 8 -4 9.20 2.90 5 -8 4 18.00 3.50 5 -8 4 7.30 3.40 -6 8 -4 35.50 3.90 6 -8 4 49.10 6.10 -7 8 -4 9.30 3.60 7 -8 4 12.00 3.70 -8 8 -4 -1.80 3.60 8 -8 4 7.20 3.90 -9 8 -4 -2.50 3.80 9 -8 4 6.90 4.10 14 7 -4 -9.40 4.10 13 7 -4 -9.20 3.60 -13 -7 4 4.40 4.30 12 7 -4 19.60 4.00 -12 -7 4 27.60 4.60 11 7 -4 0.30 2.90 -11 -7 4 1.90 3.40 10 7 -4 1.40 2.60 -10 -7 4 6.00 3.20 9 7 -4 46.70 4.70 -9 -7 4 53.49 5.20 -9 -7 4 49.99 4.80 8 7 -4 94.69 4.60 -8 -7 4 87.89 4.90 -8 -7 4 103.59 5.60 -7 -7 4 9.20 2.90 -7 -7 4 9.60 2.70 -7 -7 4 10.20 2.80 -7 -7 4 12.50 3.00 -6 -7 4 239.98 6.80 -6 -7 4 242.98 6.90 -6 -7 4 247.68 6.60 -6 -7 4 242.68 8.00 -5 -7 4 238.98 6.70 -5 -7 4 262.27 7.80 -5 -7 4 252.27 6.60 -5 -7 4 253.67 6.20 4 7 -4 10.60 1.60 4 7 -4 8.90 1.50 -4 -7 4 8.60 2.20 -4 -7 4 8.50 2.70 3 7 -4 107.29 3.70 -3 -7 4 108.19 4.40 -3 -7 4 101.29 5.70 2 7 -4 3.20 1.30 -2 -7 4 1.60 2.50 -2 -7 4 1.80 1.90 1 7 -4 174.48 4.70 -1 -7 4 175.98 5.20 -1 -7 4 179.28 6.60 0 7 -4 57.59 3.20 0 -7 4 58.19 3.80 0 -7 4 58.19 5.20 -1 7 -4 85.89 3.90 1 -7 4 87.79 4.40 1 -7 4 92.59 5.90 -2 7 -4 12.60 2.20 2 -7 4 16.80 3.30 2 -7 4 16.90 2.70 -3 7 -4 135.99 5.10 3 -7 4 138.29 5.80 3 -7 4 135.19 6.70 -4 7 -4 4.80 2.30 4 -7 4 4.40 2.50 4 -7 4 7.60 2.90 -5 7 -4 80.19 5.00 5 -7 4 89.59 6.10 5 -7 4 94.59 5.80 -6 7 -4 -3.00 2.60 6 -7 4 0.60 2.80 -7 7 -4 46.40 4.30 7 -7 4 58.49 5.90 -8 7 -4 -0.40 3.20 8 -7 4 7.80 3.60 -9 7 -4 10.00 3.80 9 -7 4 19.00 4.30 -10 7 -4 6.20 4.30 10 -7 4 13.30 4.50 14 6 -4 -12.80 4.10 13 6 -4 11.10 4.30 -13 -6 4 18.90 4.70 12 6 -4 -8.90 3.10 -12 -6 4 -1.50 3.60 11 6 -4 79.19 6.30 -11 -6 4 77.49 6.60 10 6 -4 2.50 2.60 -10 -6 4 7.40 3.30 -10 -6 4 6.80 2.60 9 6 -4 86.69 5.20 -9 -6 4 94.39 5.10 -9 -6 4 92.79 5.70 8 6 -4 178.38 6.00 -8 -6 4 186.48 6.10 -8 -6 4 189.68 6.70 7 6 -4 116.19 4.70 -7 -6 4 127.49 5.90 -7 -6 4 126.29 5.50 -7 -6 4 127.29 5.30 -6 -6 4 88.89 4.90 -6 -6 4 86.79 4.70 -6 -6 4 88.79 4.40 -6 -6 4 83.39 5.30 -5 -6 4 52.79 3.80 -5 -6 4 49.20 3.70 -5 -6 4 46.60 4.70 -5 -6 4 44.60 4.10 -4 -6 4 36.00 4.30 -4 -6 4 36.80 3.40 -4 -6 4 34.80 3.80 3 6 -4 44.20 2.20 3 6 -4 43.60 2.50 -3 -6 4 39.40 3.10 -3 -6 4 45.60 4.30 2 6 -4 168.98 3.40 2 6 -4 174.58 4.30 -2 -6 4 171.28 4.60 -2 -6 4 164.68 5.80 1 6 -4 123.19 3.70 -1 -6 4 117.89 5.20 -1 -6 4 124.39 4.00 0 6 -4 105.09 3.60 0 -6 4 106.49 5.10 0 -6 4 114.99 4.00 -1 6 -4 1.10 1.40 1 -6 4 1.70 2.20 1 -6 4 0.80 1.70 -2 6 -4 150.58 4.60 2 -6 4 157.18 5.00 2 -6 4 150.48 6.00 -3 6 -4 76.49 4.00 3 -6 4 73.69 4.30 3 -6 4 78.09 5.20 -4 6 -4 677.53 11.50 4 -6 4 661.03 11.50 4 -6 4 646.84 12.20 -5 6 -4 19.10 2.70 5 -6 4 18.60 3.00 5 -6 4 16.70 3.00 -6 6 -4 38.90 4.60 6 -6 4 45.70 5.10 6 -6 4 49.60 5.10 -7 6 -4 -0.40 2.70 7 -6 4 4.10 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139.09 6.40 -9 4 -4 42.90 5.00 9 -4 4 42.10 4.30 -10 4 -4 -4.10 3.10 10 -4 4 4.90 3.50 -11 4 -4 0.50 3.40 11 -4 4 6.80 3.80 -12 4 -4 -2.10 3.70 12 -4 4 8.20 4.20 14 3 -4 14.60 4.80 13 3 -4 -4.00 3.70 -13 -3 4 -1.10 4.20 12 3 -4 11.50 3.80 -12 -3 4 11.80 3.20 -12 -3 4 13.60 4.20 11 3 -4 0.10 3.00 -11 -3 4 1.80 2.50 -11 -3 4 0.60 3.30 10 3 -4 -0.50 2.50 -10 -3 4 6.90 3.30 -10 -3 4 3.10 2.40 9 3 -4 8.20 2.60 -9 -3 4 9.60 2.60 -9 -3 4 11.30 3.00 8 3 -4 697.83 12.10 -8 -3 4 698.43 12.50 -8 -3 4 678.73 11.70 7 3 -4 5.10 1.90 -7 -3 4 5.10 2.40 -7 -3 4 2.90 2.00 6 3 -4 330.67 6.60 -6 -3 4 328.67 6.30 -6 -3 4 322.87 6.70 -6 -3 4 323.67 7.20 5 3 -4 208.58 4.60 -5 -3 4 209.68 5.40 -5 -3 4 203.78 5.10 -5 -3 4 201.48 4.80 4 3 -4 93.09 2.80 -4 -3 4 96.49 3.60 -4 -3 4 97.49 3.50 -4 -3 4 106.09 3.50 3 3 -4 4.50 1.10 -3 -3 4 5.30 1.40 -3 -3 4 7.80 1.50 -3 -3 4 4.80 1.10 2 3 -4 56.49 2.00 -2 -3 4 55.09 2.30 -2 -3 4 57.89 2.90 -2 -3 4 59.49 2.80 1 3 -4 1014.00 12.60 -1 -3 4 1034.70 13.90 -1 -3 4 1038.50 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47.70 5.70 -4 10 -5 3.00 3.20 4 -10 5 3.30 3.10 4 -10 5 0.40 3.90 -5 10 -5 17.80 4.00 5 -10 5 21.00 4.00 -6 10 -5 -3.00 3.40 6 -10 5 5.00 3.70 7 -10 5 14.50 4.50 -12 -9 5 1.70 4.10 -11 -9 5 -1.70 3.70 -10 -9 5 5.90 3.60 -9 -9 5 26.30 3.80 -8 -9 5 13.70 3.70 -8 -9 5 20.40 3.50 7 9 -5 57.49 3.80 -7 -9 5 54.79 5.30 -7 -9 5 61.49 6.70 6 9 -5 1.80 1.60 -6 -9 5 1.50 3.20 -6 -9 5 -0.60 2.60 5 9 -5 68.89 4.00 -5 -9 5 68.79 4.90 -5 -9 5 81.49 7.00 4 9 -5 129.59 4.80 -4 -9 5 143.69 7.60 -4 -9 5 131.09 5.60 3 9 -5 2.20 1.80 -3 -9 5 1.40 2.30 -3 -9 5 1.80 3.20 2 9 -5 65.19 4.10 -2 -9 5 63.49 4.60 -2 -9 5 72.59 6.50 1 9 -5 36.30 3.80 -1 -9 5 38.70 4.40 -1 -9 5 28.20 4.00 0 9 -5 86.89 4.50 0 -9 5 83.99 4.90 0 -9 5 83.89 6.90 -1 9 -5 -1.50 2.10 1 -9 5 1.30 2.40 1 -9 5 3.60 3.50 -2 9 -5 94.69 5.20 2 -9 5 106.79 5.70 2 -9 5 93.49 7.40 -3 9 -5 0.10 2.60 3 -9 5 -0.40 3.50 3 -9 5 1.60 2.70 -4 9 -5 55.59 5.20 4 -9 5 59.69 5.80 4 -9 5 44.80 4.90 -5 9 -5 0.90 2.90 5 -9 5 1.50 3.60 5 -9 5 5.00 3.30 -6 9 -5 16.30 3.80 6 -9 5 20.30 3.90 -7 9 -5 1.30 3.70 7 -9 5 7.00 3.90 8 -9 5 13.60 4.40 -13 -8 5 -0.50 4.50 -12 -8 5 6.70 4.30 -11 -8 5 1.90 3.60 -10 -8 5 4.50 3.40 -9 -8 5 18.20 3.30 -9 -8 5 18.20 3.60 8 8 -5 138.09 5.40 -8 -8 5 136.79 6.20 -8 -8 5 133.19 6.30 -7 -8 5 2.50 2.70 -7 -8 5 1.30 2.60 -7 -8 5 1.40 2.60 -7 -8 5 2.50 2.90 6 8 -5 81.19 3.90 6 8 -5 77.99 4.00 -6 -8 5 86.39 6.50 -6 -8 5 72.19 5.10 5 8 -5 74.59 3.80 -5 -8 5 71.99 4.70 -5 -8 5 80.19 6.40 4 8 -5 84.29 3.80 -4 -8 5 89.99 6.60 -4 -8 5 79.19 4.70 3 8 -5 104.19 4.20 -3 -8 5 104.49 6.70 -3 -8 5 100.69 4.90 2 8 -5 4.10 1.80 -2 -8 5 0.90 2.30 -2 -8 5 5.70 3.20 1 8 -5 124.09 4.60 -1 -8 5 124.49 7.00 -1 -8 5 123.69 5.10 0 8 -5 43.60 3.60 0 -8 5 40.90 4.10 0 -8 5 41.40 4.10 -1 8 -5 120.29 4.90 1 -8 5 115.89 6.90 1 -8 5 112.79 5.20 -2 8 -5 -2.90 2.00 2 -8 5 0.10 3.00 2 -8 5 -2.30 2.20 -3 8 -5 103.29 5.20 3 -8 5 108.19 5.40 3 -8 5 107.19 7.10 -4 8 -5 3.70 2.70 4 -8 5 5.50 3.40 4 -8 5 6.90 2.80 -5 8 -5 67.99 5.30 5 -8 5 69.79 6.90 5 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2.70 1 -9 7 3.70 3.80 -2 9 -7 3.80 2.80 2 -9 7 3.70 3.90 -3 9 -7 5.40 2.90 3 -9 7 10.20 4.10 -4 9 -7 16.60 3.50 4 -9 7 16.20 4.30 -5 9 -7 -7.30 3.00 5 -9 7 1.40 4.10 -6 9 -7 1.50 3.70 11 8 -7 2.60 3.10 10 8 -7 10.20 3.10 9 8 -7 0.70 2.60 -9 -8 7 -2.30 3.20 -8 -8 7 17.00 3.70 -7 -8 7 2.00 3.40 -7 -8 7 -0.40 3.10 6 8 -7 3.20 2.00 -6 -8 7 2.70 3.40 5 8 -7 1.30 1.80 -5 -8 7 -1.50 3.30 4 8 -7 39.50 3.90 -4 -8 7 30.00 4.20 3 8 -7 -0.60 1.90 -3 -8 7 -2.10 3.10 2 8 -7 181.68 5.90 -2 -8 7 188.48 8.30 1 8 -7 37.60 3.80 -1 -8 7 25.70 4.10 0 8 -7 119.39 5.10 0 -8 7 120.39 7.30 -1 8 -7 51.69 4.30 1 -8 7 52.29 6.60 -2 8 -7 23.30 3.10 2 -8 7 20.50 4.10 -3 8 -7 66.39 5.20 3 -8 7 61.69 7.40 -4 8 -7 -3.80 2.70 4 -8 7 3.10 3.60 -5 8 -7 9.60 3.40 5 -8 7 16.80 4.10 -6 8 -7 -3.40 3.20 6 -8 7 -0.50 3.70 -7 8 -7 3.50 3.70 11 7 -7 9.30 3.30 10 7 -7 5.50 2.90 -10 -7 7 3.80 3.40 9 7 -7 49.80 5.10 -9 -7 7 54.49 6.10 8 7 -7 0.80 2.30 -8 -7 7 0.30 3.00 7 7 -7 75.99 4.60 -7 -7 7 76.69 6.20 -7 -7 7 74.69 6.80 6 7 -7 8.30 2.30 -6 -7 7 5.60 3.00 -6 -7 7 6.20 3.10 5 7 -7 5.80 2.00 -5 -7 7 7.20 3.30 -5 -7 7 8.70 3.20 4 7 -7 29.80 3.30 -4 -7 7 31.20 3.80 3 7 -7 78.59 4.10 -3 -7 7 88.19 6.50 2 7 -7 -1.30 1.60 -2 -7 7 -3.30 2.70 1 7 -7 69.99 4.20 -1 -7 7 76.99 6.20 0 7 -7 5.40 2.00 0 -7 7 4.00 2.90 -1 7 -7 171.08 5.70 1 -7 7 156.38 7.30 -2 7 -7 52.89 4.20 2 -7 7 50.49 6.10 -3 7 -7 121.99 5.50 3 -7 7 125.69 7.50 -4 7 -7 128.09 5.90 4 -7 7 119.39 5.70 4 -7 7 122.49 7.60 -5 7 -7 -0.40 2.80 5 -7 7 3.30 2.70 5 -7 7 0.40 3.30 -6 7 -7 39.00 4.10 6 -7 7 49.70 5.60 6 -7 7 58.19 6.80 -7 7 -7 5.40 3.50 7 -7 7 6.50 3.40 -8 7 -7 16.90 4.10 8 -7 7 20.70 4.30 9 -7 7 8.40 4.20 12 6 -7 21.10 3.90 11 6 -7 2.70 2.90 -11 -6 7 3.40 3.60 10 6 -7 2.50 2.70 -10 -6 7 6.50 3.20 9 6 -7 2.40 2.50 -9 -6 7 1.70 3.10 8 6 -7 20.20 3.00 -8 -6 7 18.50 3.50 7 6 -7 -0.90 2.00 -7 -6 7 1.40 2.80 6 6 -7 6.80 2.10 -6 -6 7 9.00 3.00 -6 -6 7 5.60 2.90 5 6 -7 1.00 1.90 -5 -6 7 5.60 2.70 -5 -6 7 -1.50 2.70 4 6 -7 248.68 5.90 -4 -6 7 246.88 8.00 -4 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7 2.00 2.60 -9 -11 -7 7.90 3.10 -9 -11 -7 2.70 2.20 9 11 7 2.90 2.90 -10 -11 -7 17.70 2.90 -10 -11 -7 13.70 3.60 10 11 7 14.70 3.30 -11 -11 -7 3.00 3.60 -11 -11 -7 5.70 2.90 11 11 7 -3.80 3.10 -12 -11 -7 1.60 3.00 12 11 7 -3.90 3.30 12 11 7 6.30 3.20 -13 -11 -7 32.20 4.20 13 11 7 33.20 4.40 -14 -11 -7 1.70 3.60 14 11 7 -2.20 3.80 -15 -11 -7 64.19 7.30 15 11 7 48.40 5.60 6 -12 -7 1.40 3.20 5 -12 -7 13.20 3.50 -5 12 7 10.90 3.40 4 -12 -7 3.50 2.90 -4 12 7 2.10 2.90 3 -12 -7 21.00 3.40 -3 12 7 19.00 3.20 2 -12 -7 1.30 2.40 -2 12 7 2.70 2.50 1 -12 -7 55.89 4.90 -1 12 7 57.19 4.50 0 -12 -7 3.70 2.30 0 12 7 0.20 1.90 0 12 7 0.50 1.80 -1 -12 -7 47.90 4.40 1 12 7 50.59 3.60 1 12 7 44.60 4.00 -2 -12 -7 47.50 4.40 2 12 7 48.30 4.10 -3 -12 -7 34.30 4.10 3 12 7 36.70 4.10 -4 -12 -7 116.99 5.50 4 12 7 108.89 5.30 -5 -12 -7 -0.30 2.20 -5 -12 -7 1.20 1.70 5 12 7 2.10 2.30 -6 -12 -7 78.39 4.00 -6 -12 -7 88.39 5.40 6 12 7 77.69 5.20 -7 -12 -7 2.10 1.90 -7 -12 -7 2.90 2.60 7 12 7 0.90 2.40 -8 -12 -7 27.50 2.90 -8 -12 -7 22.20 3.50 8 12 7 24.40 3.30 -9 -12 -7 195.88 8.10 -9 -12 -7 181.68 6.00 9 12 7 177.88 7.30 -10 -12 -7 132.89 5.80 -10 -12 -7 141.19 7.60 10 12 7 137.59 7.00 -11 -12 -7 4.00 3.70 -11 -12 -7 7.60 2.90 11 12 7 1.60 3.30 -12 -12 -7 37.50 4.10 12 12 7 31.70 4.10 12 12 7 20.40 4.00 -13 -12 -7 6.80 3.50 13 12 7 5.30 3.60 -14 -12 -7 7.70 3.80 14 12 7 5.00 4.10 -15 -12 -7 1.80 4.10 15 12 7 -7.20 4.00 5 -13 -7 9.70 3.70 -5 13 7 4.30 3.50 4 -13 -7 7.50 3.40 -4 13 7 5.00 3.20 3 -13 -7 1.00 2.80 -3 13 7 -1.60 2.70 2 -13 -7 7.70 3.00 -2 13 7 7.80 2.70 1 -13 -7 0.90 2.50 -1 13 7 -1.10 2.30 0 -13 -7 29.50 3.50 0 13 7 28.10 3.00 0 13 7 37.50 4.20 -1 -13 -7 46.50 4.80 1 13 7 35.80 4.20 -2 -13 -7 9.70 2.70 2 13 7 7.60 2.30 -3 -13 -7 1.70 2.30 3 13 7 -0.90 2.00 -4 -13 -7 22.90 3.10 4 13 7 22.10 2.90 -5 -13 -7 15.70 2.90 5 13 7 25.00 3.10 -6 -13 -7 20.90 3.30 6 13 7 21.00 3.10 -7 -13 -7 127.49 6.50 -7 -13 -7 114.39 4.60 7 13 7 118.59 6.20 -8 -13 -7 12.20 3.30 -8 -13 -7 6.40 2.30 8 13 7 8.10 3.00 -9 -13 -7 24.90 4.00 -9 -13 -7 23.50 3.00 9 13 7 25.30 3.70 -10 -13 -7 19.40 3.10 -10 -13 -7 14.60 4.00 10 13 7 11.60 3.60 -11 -13 -7 51.79 5.00 -11 -13 -7 46.30 5.10 11 13 7 33.90 4.30 -12 -13 -7 1.10 3.00 -12 -13 -7 1.20 4.10 12 13 7 -9.00 3.30 -13 -13 -7 38.30 4.40 13 13 7 52.79 6.60 -14 -13 -7 0.70 3.70 14 13 7 2.70 3.90 -15 -13 -7 18.60 4.50 -4 14 7 5.20 3.30 3 -14 -7 5.50 3.30 -3 14 7 8.70 3.20 2 -14 -7 1.70 2.90 -2 14 7 0.30 2.70 1 -14 -7 12.30 3.30 -1 14 7 14.50 2.90 0 -14 -7 8.80 2.90 0 14 7 6.90 2.50 -1 -14 -7 5.00 2.80 1 14 7 4.60 2.50 -2 -14 -7 20.10 3.40 2 14 7 18.10 3.00 -3 -14 -7 12.90 3.00 3 14 7 6.70 2.60 -4 -14 -7 2.20 2.70 4 14 7 3.30 2.50 -5 -14 -7 9.20 3.00 5 14 7 8.10 2.80 -6 -14 -7 -1.20 2.60 6 14 7 -1.40 2.50 -7 -14 -7 28.70 3.80 7 14 7 23.60 3.50 -8 -14 -7 27.00 3.90 8 14 7 22.50 3.60 -9 -14 -7 142.99 6.40 -9 -14 -7 138.69 7.70 9 14 7 133.19 7.60 -10 -14 -7 43.40 4.90 -10 -14 -7 42.00 5.00 10 14 7 41.50 4.40 -11 -14 -7 0.00 3.90 -11 -14 -7 0.10 2.80 11 14 7 -7.10 3.20 -12 -14 -7 55.59 5.90 -12 -14 -7 51.69 5.60 12 14 7 43.50 4.90 -13 -14 -7 -3.00 4.50 -13 -14 -7 5.50 3.60 13 14 7 7.60 3.50 13 14 7 -11.10 3.90 -14 -14 -7 66.59 7.10 14 14 7 70.19 7.60 -3 15 7 5.10 3.30 2 -15 -7 12.50 3.80 -2 15 7 11.40 3.40 1 -15 -7 6.50 3.30 0 -15 -7 1.40 3.00 -1 -15 -7 2.40 2.90 1 15 7 -1.90 2.40 -2 -15 -7 63.49 6.20 2 15 7 45.50 5.20 -3 -15 -7 13.20 3.20 3 15 7 7.20 2.80 -4 -15 -7 28.50 3.90 4 15 7 29.80 3.70 -5 -15 -7 59.99 6.10 5 15 7 53.69 5.70 -6 -15 -7 5.40 3.20 6 15 7 3.70 3.00 -7 -15 -7 24.20 3.90 7 15 7 22.60 3.70 -8 -15 -7 8.70 3.60 8 15 7 5.70 3.40 -9 -15 -7 12.90 4.00 9 15 7 8.60 3.60 -10 -15 -7 20.90 4.50 10 15 7 11.30 3.90 -11 -15 -7 12.60 4.60 11 15 7 2.40 3.80 -12 -15 -7 -0.40 3.20 -12 -15 -7 -0.10 4.50 12 15 7 -9.60 3.70 -13 -15 -7 18.70 4.00 -13 -15 -7 16.10 5.40 13 15 7 7.70 4.60 -14 -15 -7 5.10 4.00 0 -16 -7 0.40 3.30 -1 -16 -7 15.00 3.80 1 16 7 9.50 3.10 -2 -16 -7 22.50 3.90 2 16 7 18.60 3.40 -3 -16 -7 16.10 3.80 3 16 7 13.70 3.30 -4 -16 -7 7.40 3.40 4 16 7 6.50 3.00 -5 -16 -7 2.00 3.20 5 16 7 -3.00 2.80 -6 -16 -7 24.80 4.00 6 16 7 25.00 4.00 -7 -16 -7 7.30 3.60 7 16 7 1.20 3.30 -8 -16 -7 12.10 4.00 8 16 7 5.50 3.50 -9 -16 -7 17.70 4.30 9 16 7 10.60 3.90 -10 -16 -7 5.00 4.30 10 16 7 3.60 3.80 -11 -16 -7 -10.90 4.30 11 16 7 -9.80 3.70 -12 -16 -7 7.80 5.00 12 16 7 1.60 4.30 13 16 7 -7.20 4.40 -2 -17 -7 7.50 3.90 2 17 7 0.60 3.10 -3 -17 -7 3.70 3.70 3 17 7 1.10 3.20 -4 -17 -7 6.30 3.80 4 17 7 6.70 3.40 -5 -17 -7 3.10 3.60 5 17 7 1.90 3.30 -6 -17 -7 -0.40 3.40 6 17 7 -1.70 3.30 -7 -17 -7 7.90 4.00 7 17 7 9.30 4.00 -8 -17 -7 0.10 4.00 8 17 7 -1.40 3.60 -9 -17 -7 3.20 4.10 9 17 7 -2.20 3.80 -10 -17 -7 9.60 4.80 10 17 7 1.30 4.10 -11 -17 -7 3.60 5.00 11 17 7 -6.60 4.00 12 17 7 -10.60 4.20 3 18 7 -2.90 3.30 4 18 7 -6.20 3.30 -5 -18 -7 6.10 4.20 5 18 7 -5.40 3.40 -6 -18 -7 1.10 3.90 6 18 7 -4.50 3.50 -7 -18 -7 9.40 4.40 7 18 7 2.20 4.10 -8 -18 -7 6.70 4.60 8 18 7 2.60 4.30 6 12 -8 5.20 3.20 -6 -12 8 9.80 5.30 5 12 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4.70 8 9 -8 8.90 2.70 7 9 -8 1.10 2.20 -7 -9 8 0.80 3.90 6 9 -8 38.70 4.20 -6 -9 8 37.00 4.90 5 9 -8 0.70 2.30 -5 -9 8 0.20 3.80 4 9 -8 56.19 4.60 -4 -9 8 66.19 8.00 3 9 -8 20.70 3.10 -3 -9 8 21.60 4.50 2 9 -8 28.20 3.30 -2 -9 8 23.50 4.60 1 9 -8 12.80 2.90 -1 -9 8 14.40 4.30 0 9 -8 7.20 2.70 0 -9 8 9.80 4.10 -1 9 -8 0.10 2.60 1 -9 8 4.80 3.90 -2 9 -8 5.50 3.00 2 -9 8 11.30 4.20 -3 9 -8 20.20 3.60 3 -9 8 20.90 4.70 -4 9 -8 -2.00 3.20 4 -9 8 -1.70 4.10 -5 9 -8 1.50 3.50 5 -9 8 9.00 4.60 10 8 -8 1.10 3.10 -9 -8 8 17.70 4.10 -8 -8 8 3.50 3.70 -7 -8 8 15.20 3.90 6 8 -8 2.80 2.20 -6 -8 8 -1.70 3.50 5 8 -8 37.80 3.90 -5 -8 8 35.10 4.50 4 8 -8 7.70 2.40 -4 -8 8 9.30 3.80 3 8 -8 89.99 5.10 -3 -8 8 86.29 7.40 2 8 -8 -1.10 2.10 -2 -8 8 0.60 3.50 1 8 -8 122.99 5.70 -1 -8 8 123.79 7.80 0 8 -8 61.49 4.90 0 -8 8 63.39 7.20 -1 8 -8 13.10 2.90 1 -8 8 11.80 4.00 -2 8 -8 23.40 3.30 2 -8 8 19.20 4.10 -3 8 -8 7.10 3.00 3 -8 8 2.60 3.80 -4 8 -8 27.20 3.80 4 -8 8 25.40 4.60 -5 8 -8 -2.60 3.00 5 -8 8 -2.60 3.60 -6 8 -8 14.10 3.80 6 -8 8 16.30 4.60 -7 8 -8 -5.60 3.60 11 7 -8 7.50 3.50 10 7 -8 12.50 3.40 -10 -7 8 10.60 3.90 9 7 -8 6.40 3.00 -9 -7 8 6.50 3.60 8 7 -8 37.90 3.80 -8 -7 8 42.90 4.60 7 7 -8 -0.10 2.40 -7 -7 8 -1.90 3.20 -6 -7 8 141.69 7.80 -6 -7 8 133.69 7.00 5 7 -8 61.79 4.20 -5 -7 8 56.79 6.60 4 7 -8 23.60 2.70 -4 -7 8 23.00 3.80 3 7 -8 1.00 1.90 -3 -7 8 -4.30 3.00 2 7 -8 41.70 3.80 -2 -7 8 47.90 6.10 1 7 -8 -0.10 1.90 -1 -7 8 1.60 3.20 0 7 -8 122.09 5.20 0 -7 8 125.49 7.20 -1 7 -8 0.00 2.10 1 -7 8 3.40 3.20 -2 7 -8 46.10 4.30 2 -7 8 40.60 4.50 -3 7 -8 107.39 5.50 3 -7 8 93.49 7.60 -4 7 -8 -2.00 2.60 4 -7 8 5.10 3.60 -5 7 -8 33.80 3.90 5 -7 8 35.00 4.60 -6 7 -8 -2.70 3.10 6 -7 8 -2.70 3.50 -7 7 -8 -1.60 3.40 -8 7 -8 6.00 3.90 11 6 -8 9.80 3.50 -11 -6 8 10.60 4.10 10 6 -8 -0.20 2.90 -10 -6 8 1.10 3.70 9 6 -8 23.00 3.50 -9 -6 8 20.20 3.80 8 6 -8 7.00 2.70 -8 -6 8 7.90 3.30 7 6 -8 84.39 5.20 -7 -6 8 80.59 6.50 6 6 -8 1.80 2.20 -6 -6 8 5.60 3.00 -6 -6 8 6.10 3.30 5 6 -8 1.70 2.10 -5 -6 8 2.40 3.10 -5 -6 8 3.40 2.90 4 6 -8 0.40 2.00 -4 -6 8 3.10 3.00 -4 -6 8 -0.30 2.70 3 6 -8 170.68 5.50 -3 -6 8 190.98 7.50 2 6 -8 -1.90 1.60 -2 -6 8 -1.30 2.70 1 6 -8 54.99 3.70 -1 -6 8 56.69 6.00 0 6 -8 13.60 2.30 0 -6 8 16.50 3.20 -1 6 -8 91.39 4.50 1 -6 8 95.29 6.40 -2 6 -8 -0.60 1.90 2 -6 8 -4.80 2.90 -3 6 -8 149.19 5.70 3 -6 8 150.38 7.50 -4 6 -8 133.69 5.80 4 -6 8 125.69 7.50 -5 6 -8 0.40 2.70 5 -6 8 8.30 3.50 -6 6 -8 57.09 5.70 6 -6 8 59.89 6.90 -7 6 -8 3.30 3.20 7 -6 8 9.40 3.70 -8 6 -8 2.60 3.50 -9 6 -8 -0.50 3.60 11 5 -8 6.80 3.40 -11 -5 8 6.00 3.90 10 5 -8 7.40 3.10 -10 -5 8 7.80 3.50 9 5 -8 18.80 3.30 -9 -5 8 15.00 3.60 8 5 -8 98.49 5.70 -8 -5 8 90.79 6.20 7 5 -8 -1.30 2.30 -7 -5 8 -4.20 2.70 6 5 -8 147.89 5.50 -6 -5 8 149.19 6.80 -6 -5 8 139.99 6.40 5 5 -8 23.10 2.70 -5 -5 8 19.20 3.00 -5 -5 8 22.00 3.40 4 5 -8 59.49 3.80 -4 -5 8 64.59 5.40 -4 -5 8 56.59 5.10 3 5 -8 -2.30 1.70 -3 -5 8 2.10 2.80 -3 -5 8 -4.50 2.50 2 5 -8 28.10 3.00 2 5 -8 26.00 3.00 -2 -5 8 23.30 3.40 1 5 -8 0.40 1.60 -1 -5 8 1.80 2.70 0 5 -8 284.97 6.70 0 -5 8 286.57 8.40 -1 5 -8 17.10 2.40 1 -5 8 20.70 3.30 -2 5 -8 6.80 2.10 2 -5 8 7.60 2.90 -3 5 -8 154.08 5.50 3 -5 8 141.49 6.90 -4 5 -8 85.89 5.00 4 -5 8 82.29 6.40 -5 5 -8 7.30 2.60 5 -5 8 9.40 3.20 -6 5 -8 25.90 3.50 6 -5 8 22.50 3.70 -7 5 -8 37.30 4.00 7 -5 8 33.80 4.10 -8 5 -8 6.10 3.40 -9 5 -8 8.90 3.70 -10 5 -8 -5.30 3.70 -12 -4 8 2.50 4.10 11 4 -8 5.80 3.20 -11 -4 8 5.10 3.90 10 4 -8 4.30 2.90 -10 -4 8 8.60 3.60 9 4 -8 91.39 5.80 -9 -4 8 74.49 6.20 8 4 -8 7.30 2.70 -8 -4 8 2.30 3.20 7 4 -8 106.29 5.30 -7 -4 8 96.19 5.90 6 4 -8 5.80 2.20 -6 -4 8 1.30 2.70 5 4 -8 73.39 4.10 -5 -4 8 74.89 5.50 -5 -4 8 63.69 5.10 4 4 -8 10.40 2.20 -4 -4 8 5.20 2.60 -4 -4 8 11.10 3.10 3 4 -8 353.86 7.10 -3 -4 8 346.37 8.70 -3 -4 8 361.96 8.70 2 4 -8 -0.50 1.70 -2 -4 8 4.10 2.70 -2 -4 8 2.00 2.40 1 4 -8 194.48 4.70 1 4 -8 195.38 5.30 -1 -4 8 192.08 6.80 0 4 -8 140.39 3.90 0 4 -8 135.99 4.50 0 -4 8 140.19 6.10 -1 4 -8 28.00 2.90 1 -4 8 22.40 3.10 -2 4 -8 2.10 1.70 2 -4 8 1.70 2.50 -3 4 -8 55.89 3.60 3 -4 8 47.60 5.40 -4 4 -8 196.88 5.80 4 -4 8 187.68 7.20 -5 4 -8 16.50 2.70 5 -4 8 17.30 3.20 -6 4 -8 21.00 3.00 6 -4 8 22.20 3.00 6 -4 8 21.10 3.40 -7 4 -8 60.09 5.40 7 -4 8 72.19 6.10 7 -4 8 79.39 5.50 -8 4 -8 28.70 3.70 8 -4 8 27.40 3.60 -9 4 -8 -6.50 3.00 9 -4 8 2.40 3.20 -10 4 -8 -0.50 3.40 10 -4 8 3.30 3.60 -11 4 -8 -2.40 3.80 11 -4 8 10.90 4.30 -12 -3 8 -0.50 4.00 11 3 -8 5.10 3.20 -11 -3 8 4.70 3.60 10 3 -8 5.80 2.90 -10 -3 8 4.00 3.50 9 3 -8 59.59 5.30 -9 -3 8 64.69 6.40 8 3 -8 109.99 5.60 -8 -3 8 105.49 6.60 7 3 -8 16.90 2.70 -7 -3 8 16.90 3.30 6 3 -8 178.28 5.90 -6 -3 8 175.08 6.60 5 3 -8 -0.80 1.90 -5 -3 8 -0.20 2.40 -5 -3 8 -1.90 2.10 4 3 -8 249.28 6.10 -4 -3 8 246.88 7.20 -4 -3 8 245.18 6.90 3 3 -8 1.50 1.70 -3 -3 8 0.50 2.10 -3 -3 8 -0.80 2.30 2 3 -8 239.18 5.40 -2 -3 8 231.88 6.70 -2 -3 8 231.38 6.60 1 3 -8 33.70 2.70 -1 -3 8 37.50 4.20 -1 -3 8 40.90 4.10 0 3 -8 63.39 3.20 0 3 -8 68.99 3.10 0 -3 8 63.39 4.70 -1 3 -8 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1 4 -10 180.08 5.80 -1 -4 10 199.28 7.70 0 4 -10 18.10 2.50 0 -4 10 17.00 3.20 -1 4 -10 30.30 3.50 1 -4 10 24.60 3.60 -2 4 -10 10.40 2.30 2 -4 10 12.10 3.10 -3 4 -10 43.20 4.20 3 -4 10 38.00 4.10 -4 4 -10 1.10 2.30 4 -4 10 1.60 3.20 -5 4 -10 349.07 8.60 5 -4 10 346.97 10.20 -6 4 -10 18.30 3.30 6 -4 10 17.70 3.80 -7 4 -10 1.90 2.90 7 -4 10 7.60 3.50 -8 4 -10 29.40 3.90 8 -4 10 38.30 4.60 -9 4 -10 -6.50 3.20 -10 4 -10 -6.30 3.70 10 3 -10 -0.30 3.30 -10 -3 10 6.50 4.00 9 3 -10 9.00 3.40 -9 -3 10 14.00 4.10 8 3 -10 12.00 3.30 -8 -3 10 14.00 3.90 7 3 -10 40.10 3.90 -7 -3 10 31.40 4.20 6 3 -10 34.00 3.60 -6 -3 10 39.30 4.30 5 3 -10 2.70 2.40 -5 -3 10 5.90 3.20 4 3 -10 11.20 2.50 -4 -3 10 12.00 2.70 -4 -3 10 13.20 3.20 3 3 -10 3.50 2.10 -3 -3 10 0.30 2.50 -3 -3 10 6.20 2.90 2 3 -10 28.40 2.80 -2 -3 10 28.10 3.40 -2 -3 10 28.60 3.30 1 3 -10 50.99 3.60 1 3 -10 46.10 3.60 -1 -3 10 36.10 3.70 -1 -3 10 54.79 5.30 0 3 -10 116.69 4.30 0 3 -10 119.79 4.70 0 -3 10 119.69 6.20 -1 3 -10 78.39 3.70 -1 3 -10 67.99 3.90 1 -3 10 80.59 5.70 -2 3 -10 274.27 6.70 2 -3 10 252.67 8.00 -3 3 -10 -3.50 1.90 3 -3 10 3.50 2.80 -4 3 -10 199.68 6.00 4 -3 10 207.58 7.60 -5 3 -10 32.80 3.90 5 -3 10 31.70 3.80 -6 3 -10 21.10 3.00 6 -3 10 27.10 3.80 -7 3 -10 -0.60 2.60 7 -3 10 9.60 3.30 -8 3 -10 2.10 2.90 8 -3 10 8.20 3.50 -9 3 -10 13.70 3.60 -10 3 -10 0.20 3.60 -11 3 -10 10.40 4.10 10 2 -10 24.30 4.20 -10 -2 10 25.30 4.60 9 2 -10 2.80 3.10 -9 -2 10 3.20 3.80 8 2 -10 11.40 3.20 -8 -2 10 13.30 3.70 7 2 -10 3.80 2.70 -7 -2 10 2.50 3.20 6 2 -10 56.19 4.80 -6 -2 10 56.19 6.10 5 2 -10 39.00 4.20 -5 -2 10 31.60 3.80 4 2 -10 22.20 2.80 -4 -2 10 21.40 3.40 -4 -2 10 23.20 2.90 3 2 -10 162.18 5.40 -3 -2 10 172.88 6.90 -3 -2 10 170.98 6.30 2 2 -10 17.70 2.50 -2 -2 10 19.70 3.30 -2 -2 10 16.80 2.90 1 2 -10 158.78 5.00 -1 -2 10 163.08 6.40 0 2 -10 0.60 1.50 0 2 -10 -0.50 1.90 0 -2 10 -3.60 2.60 0 -2 10 3.50 2.60 -1 2 -10 7.60 1.80 -1 2 -10 9.00 2.10 1 -2 10 5.80 2.60 -2 2 -10 169.98 4.80 -2 2 -10 173.98 5.20 2 -2 10 182.68 6.80 -3 2 -10 224.48 6.00 -3 2 -10 225.58 5.40 3 -2 10 230.18 7.50 -4 2 -10 39.40 3.80 4 -2 10 30.00 3.60 -5 2 -10 385.16 8.20 5 -2 10 385.36 9.80 -6 2 -10 -4.00 2.20 6 -2 10 -1.70 2.60 -7 2 -10 21.30 3.20 7 -2 10 21.80 3.60 -8 2 -10 6.30 2.90 8 -2 10 13.80 3.40 -9 2 -10 21.80 3.50 9 -2 10 30.40 4.00 -10 2 -10 17.90 3.80 10 1 -10 4.10 3.40 -10 -1 10 4.40 3.90 9 1 -10 34.50 4.20 -9 -1 10 35.70 4.60 8 1 -10 -2.50 2.60 -8 -1 10 -2.50 3.20 7 1 -10 111.69 5.90 -7 -1 10 109.29 7.00 6 1 -10 43.90 4.60 -6 -1 10 50.49 5.40 5 1 -10 128.69 5.40 -5 -1 10 122.29 6.10 4 1 -10 10.60 2.40 -4 -1 10 6.80 2.70 -4 -1 10 11.00 2.30 3 1 -10 2.10 2.00 -3 -1 10 -0.30 2.50 -3 -1 10 0.90 2.10 2 1 -10 93.09 4.30 -2 -1 10 95.99 5.30 -2 -1 10 89.29 5.60 1 1 -10 27.90 3.20 -1 -1 10 20.00 3.10 -1 -1 10 20.90 2.80 0 1 -10 466.35 8.30 0 -1 10 458.35 9.60 0 -1 10 441.76 9.40 -1 1 -10 0.90 1.50 -1 1 -10 0.50 1.80 1 -1 10 -1.60 2.20 -2 1 -10 127.99 4.30 -2 1 -10 125.59 4.30 2 -1 10 124.59 5.70 -3 1 -10 18.10 2.10 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529.85 10.40 -4 0 -10 149.09 4.70 -4 0 -10 149.88 4.60 4 0 10 144.39 6.20 -5 0 -10 164.98 5.00 -5 0 -10 168.98 4.90 5 0 10 166.08 6.80 -6 0 -10 3.00 2.00 -6 0 -10 0.70 1.80 6 0 10 2.70 2.70 -7 0 -10 19.20 2.50 -7 0 -10 20.30 2.50 7 0 10 20.30 3.30 -8 0 -10 2.90 2.10 -8 0 -10 -2.00 2.10 8 0 10 -3.40 2.70 -9 0 -10 38.90 4.50 9 0 10 52.99 6.00 10 -1 -10 -2.50 3.10 -10 1 10 2.00 3.90 9 -1 -10 24.90 3.80 -9 1 10 30.40 4.30 8 -1 -10 0.00 2.60 -8 1 10 0.70 3.00 7 -1 -10 17.00 3.10 -7 1 10 17.60 3.40 6 -1 -10 3.20 2.40 -6 1 10 5.00 2.80 5 -1 -10 67.09 4.40 -5 1 10 59.59 4.80 4 -1 -10 -3.00 1.80 -4 1 10 -1.70 2.20 3 -1 -10 24.30 2.60 -3 1 10 23.10 2.90 -3 1 10 20.50 2.40 2 -1 -10 28.60 3.20 -2 1 10 25.40 3.00 -2 1 10 23.90 2.60 1 -1 -10 394.66 7.60 -1 1 10 379.66 8.10 -1 1 10 389.56 8.40 0 -1 -10 93.59 4.00 0 1 10 92.69 4.60 0 1 10 94.09 4.70 -1 -1 -10 274.67 6.00 1 1 10 270.17 6.90 1 1 10 267.57 6.70 -2 -1 -10 296.07 6.30 2 1 10 293.37 7.00 2 1 10 295.37 7.40 -3 -1 -10 223.08 5.40 -3 -1 -10 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4.40 3.40 -9 -5 -13 2.50 2.80 9 5 13 2.80 3.60 -10 -5 -13 26.40 3.80 10 5 13 25.30 4.20 -11 -5 -13 1.30 3.10 11 5 13 2.70 3.60 -12 -5 -13 31.50 4.40 12 5 13 25.60 4.40 -13 -5 -13 9.40 4.00 6 -6 -13 1.00 2.90 -6 6 13 -4.20 3.50 5 -6 -13 10.70 3.10 -5 6 13 13.50 3.60 4 -6 -13 2.40 2.50 -4 6 13 7.80 3.10 3 -6 -13 14.80 2.90 -3 6 13 10.90 3.00 2 -6 -13 -0.80 2.20 -2 6 13 -0.90 2.50 1 -6 -13 92.49 5.10 -1 6 13 91.29 5.40 -1 6 13 89.49 5.10 0 -6 -13 -0.90 2.10 0 6 13 2.90 2.20 0 6 13 0.10 2.30 -1 -6 -13 2.40 2.20 1 6 13 1.80 2.20 1 6 13 5.50 2.40 -2 -6 -13 13.00 2.50 2 6 13 9.00 2.30 2 6 13 7.80 2.70 -3 -6 -13 7.80 2.30 3 6 13 10.20 2.30 3 6 13 6.10 2.80 -4 -6 -13 2.40 2.20 4 6 13 3.50 2.70 4 6 13 1.20 2.00 -5 -6 -13 190.58 6.10 5 6 13 196.98 7.50 -6 -6 -13 7.70 2.50 6 6 13 4.50 2.90 -7 -6 -13 83.09 5.10 7 6 13 91.59 6.60 -8 -6 -13 14.70 3.00 8 6 13 10.60 3.60 -9 -6 -13 36.40 3.90 9 6 13 30.70 4.30 -10 -6 -13 10.80 3.30 10 6 13 8.60 3.80 -11 -6 -13 14.80 3.70 11 6 13 21.90 4.30 -12 -6 -13 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8.00 3.10 -1 -8 -16 52.39 5.50 1 8 16 54.49 5.60 1 8 16 59.89 6.50 -2 -8 -16 24.20 3.60 2 8 16 25.60 3.90 -3 -8 -16 22.00 3.60 3 8 16 31.30 4.10 -4 -8 -16 73.09 5.70 4 8 16 87.99 7.30 -5 -8 -16 -2.00 2.70 5 8 16 -0.90 3.40 -6 -8 -16 5.60 3.00 6 8 16 9.60 3.70 -7 -8 -16 0.90 3.00 7 8 16 6.00 3.70 -8 -8 -16 21.20 3.70 8 8 16 21.50 4.30 -9 -8 -16 2.90 3.20 9 8 16 4.40 4.00 -10 -8 -16 20.80 4.20 10 8 16 19.00 4.50 -11 -8 -16 3.30 3.80 11 8 16 -1.90 4.30 12 8 16 24.90 5.10 2 -9 -16 7.80 3.50 -2 9 16 13.10 3.50 1 -9 -16 0.20 3.10 -1 9 16 0.30 3.00 0 -9 -16 14.10 3.50 0 9 16 6.20 3.10 -1 -9 -16 14.00 3.40 -2 -9 -16 18.70 3.50 2 9 16 26.80 3.90 -3 -9 -16 9.50 3.10 3 9 16 7.50 3.30 -4 -9 -16 18.20 3.40 4 9 16 22.70 4.00 -5 -9 -16 25.10 3.70 5 9 16 31.10 4.40 -6 -9 -16 15.20 3.40 6 9 16 20.60 4.10 -7 -9 -16 34.40 4.00 7 9 16 31.50 4.40 -8 -9 -16 3.90 3.10 8 9 16 8.20 3.70 -9 -9 -16 69.39 6.40 9 9 16 73.69 7.70 -10 -9 -16 1.40 3.50 10 9 16 -0.70 4.10 -11 -9 -16 14.70 4.10 11 9 16 9.60 4.60 12 9 16 9.20 4.70 -2 10 16 0.00 3.20 1 -10 -16 14.50 3.60 -1 10 16 20.30 3.80 0 -10 -16 -1.40 2.80 -1 -10 -16 10.70 3.20 -2 -10 -16 6.50 3.10 2 10 16 6.90 3.40 -3 -10 -16 4.80 3.00 3 10 16 6.70 3.40 -4 -10 -16 22.00 3.50 4 10 16 19.40 3.90 -5 -10 -16 5.10 3.00 5 10 16 5.90 3.50 -6 -10 -16 21.60 3.60 6 10 16 24.10 4.20 -7 -10 -16 3.70 3.10 7 10 16 -0.50 3.40 -8 -10 -16 20.60 3.70 8 10 16 17.70 4.20 -9 -10 -16 6.30 3.50 9 10 16 2.20 3.90 -10 -10 -16 28.60 4.40 10 10 16 29.40 4.90 -11 -10 -16 2.40 3.70 11 10 16 7.20 4.30 12 10 16 21.70 5.20 1 -11 -16 0.30 3.10 0 -11 -16 16.50 3.70 -1 -11 -16 0.40 3.00 -2 -11 -16 42.10 4.30 2 11 16 35.00 4.40 -3 -11 -16 9.10 3.10 3 11 16 13.00 3.70 -4 -11 -16 3.50 2.90 4 11 16 4.30 3.50 -5 -11 -16 30.50 3.70 5 11 16 24.50 4.30 -6 -11 -16 -2.00 2.90 6 11 16 1.60 3.50 -7 -11 -16 20.40 3.60 7 11 16 13.30 4.10 -8 -11 -16 4.10 3.20 8 11 16 4.20 3.90 -9 -11 -16 21.60 3.90 9 11 16 21.90 4.60 -10 -11 -16 -0.90 3.60 10 11 16 2.30 4.10 -11 -11 -16 10.40 4.10 11 11 16 11.60 4.60 0 -12 -16 -1.80 3.00 -1 -12 -16 19.20 3.70 -2 -12 -16 6.00 3.10 -3 -12 -16 6.50 3.10 3 12 16 6.00 3.70 -4 -12 -16 3.60 3.00 4 12 16 1.80 3.60 -5 -12 -16 9.10 3.10 5 12 16 8.00 3.80 -6 -12 -16 36.30 4.10 6 12 16 30.20 4.70 -7 -12 -16 -1.90 3.00 7 12 16 1.30 3.80 -8 -12 -16 20.50 3.90 8 12 16 15.30 4.50 -9 -12 -16 0.70 3.30 9 12 16 -0.20 3.90 -10 -12 -16 13.40 4.10 10 12 16 14.90 4.50 -11 -12 -16 1.30 4.00 11 12 16 4.10 4.50 -1 -13 -16 0.70 3.10 -2 -13 -16 5.40 3.20 -3 -13 -16 -0.70 2.90 3 13 16 -0.40 3.70 -4 -13 -16 9.60 3.20 4 13 16 1.00 3.80 -5 -13 -16 13.10 3.40 5 13 16 12.80 4.20 -6 -13 -16 -1.10 3.00 6 13 16 -4.50 3.70 -7 -13 -16 0.70 3.00 7 13 16 -3.10 3.90 -8 -13 -16 12.00 3.60 8 13 16 9.90 4.40 -9 -13 -16 20.50 4.10 9 13 16 14.90 4.80 -10 -13 -16 3.20 3.80 10 13 16 0.60 4.40 -2 -14 -16 3.60 3.20 -3 -14 -16 15.60 3.50 3 14 16 4.30 4.10 -4 -14 -16 -2.00 2.80 4 14 16 0.00 3.90 -5 -14 -16 5.60 3.10 5 14 16 -3.50 3.90 -6 -14 -16 10.00 3.40 6 14 16 0.80 4.20 -7 -14 -16 5.30 3.30 7 14 16 -1.70 4.20 -8 -14 -16 4.30 3.40 8 14 16 -3.20 4.30 -9 -14 -16 4.10 3.60 -10 -14 -16 0.00 3.90 4 15 16 3.70 4.20 -5 -15 -16 -0.10 3.10 5 15 16 -4.10 4.10 -6 -15 -16 -1.40 3.10 6 15 16 -4.30 4.20 -7 -15 -16 6.30 3.40 -8 -15 -16 7.40 3.50 -9 -15 -16 4.30 3.70 0 -1 17 15.00 4.50 -3 1 -17 -2.60 3.30 1 0 -17 1.40 3.40 -1 0 17 13.10 4.20 0 0 -17 5.50 3.50 0 0 -17 3.90 3.40 0 0 17 7.70 4.10 -1 0 -17 21.00 3.80 -1 0 -17 18.50 4.20 1 0 17 27.50 4.80 -2 0 -17 -1.10 3.20 2 0 17 6.00 4.20 -3 0 -17 13.00 3.50 3 0 17 21.20 4.70 -4 0 -17 -0.80 3.10 -5 0 -17 9.70 3.50 2 -1 -17 0.20 3.50 1 -1 -17 0.60 3.40 -1 1 17 3.30 4.00 -1 1 17 4.80 4.00 0 -1 -17 -2.50 3.20 0 1 17 0.50 4.20 0 1 17 4.60 3.90 -1 -1 -17 1.80 3.10 -1 -1 -17 4.90 3.40 1 1 17 6.80 4.10 -2 -1 -17 3.00 3.40 -2 -1 -17 5.80 3.20 2 1 17 13.40 4.30 -3 -1 -17 1.80 3.10 -3 -1 -17 1.50 3.20 3 1 17 9.10 4.20 -4 -1 -17 22.30 3.70 4 1 17 28.50 4.90 -5 -1 -17 -0.50 2.90 5 1 17 4.30 4.20 2 -2 -17 -0.90 3.50 1 -2 -17 5.40 3.50 -1 2 17 6.70 4.00 0 -2 -17 -2.50 3.10 0 2 17 5.50 3.80 0 2 17 3.50 3.70 -1 -2 -17 10.00 3.40 1 2 17 10.90 3.90 1 2 17 4.00 3.90 -2 -2 -17 2.10 3.00 -2 -2 -17 -4.40 3.10 2 2 17 0.30 3.60 -3 -2 -17 -3.00 3.10 -3 -2 -17 0.20 2.70 3 2 17 1.70 3.80 -4 -2 -17 9.10 3.20 -4 -2 -17 17.80 3.70 4 2 17 12.50 4.30 -5 -2 -17 13.90 3.30 -5 -2 -17 21.00 3.80 5 2 17 24.80 4.70 6 2 17 6.20 4.30 2 -3 -17 3.20 3.60 -2 3 17 3.20 3.90 1 -3 -17 -1.10 3.20 -1 3 17 0.50 3.80 0 -3 -17 -3.50 3.00 0 3 17 -2.60 3.50 0 3 17 1.90 3.50 -1 -3 -17 11.20 3.50 1 3 17 14.80 4.00 1 3 17 14.60 4.00 -2 -3 -17 6.40 3.30 2 3 17 10.20 3.90 2 3 17 -2.00 3.80 -3 -3 -17 0.40 3.10 -3 -3 -17 0.60 2.70 3 3 17 4.00 3.80 -4 -3 -17 34.00 3.70 -4 -3 -17 34.60 4.10 4 3 17 43.30 5.00 -5 -3 -17 2.20 3.20 5 3 17 1.30 3.90 -6 -3 -17 11.40 3.50 6 3 17 15.10 4.30 -7 -3 -17 1.80 3.20 7 3 17 8.40 4.30 -8 -3 -17 2.50 3.50 8 3 17 10.10 4.80 2 -4 -17 2.00 3.70 -2 4 17 -0.10 3.90 1 -4 -17 1.70 3.20 -1 4 17 0.70 3.50 0 -4 -17 3.10 3.20 0 4 17 9.30 3.60 0 4 17 5.10 3.80 -1 -4 -17 1.20 3.00 1 4 17 5.40 3.60 1 4 17 -0.90 3.50 -2 -4 -17 21.90 3.80 2 4 17 21.60 4.20 2 4 17 23.50 4.10 -3 -4 -17 9.50 2.80 -3 -4 -17 1.10 3.10 3 4 17 8.80 3.80 3 4 17 3.80 3.80 -4 -4 -17 8.80 3.40 4 4 17 8.30 3.90 -5 -4 -17 22.90 3.80 5 4 17 23.30 4.40 -6 -4 -17 1.40 3.20 6 4 17 3.80 4.00 -7 -4 -17 47.60 5.80 7 4 17 36.20 5.00 -8 -4 -17 4.70 3.40 8 4 17 2.90 4.30 -9 -4 -17 -1.20 3.50 -2 5 17 12.10 4.10 1 -5 -17 -3.30 3.10 -1 5 17 -5.60 3.50 0 -5 -17 -2.60 2.90 0 5 17 -1.40 3.40 -1 -5 -17 29.90 4.00 1 5 17 36.80 4.50 1 5 17 28.60 4.30 -2 -5 -17 8.10 3.30 2 5 17 0.90 3.20 2 5 17 9.70 3.70 -3 -5 -17 1.10 3.10 3 5 17 9.20 3.70 3 5 17 2.30 3.40 -4 -5 -17 36.90 4.20 4 5 17 39.00 4.70 -5 -5 -17 10.60 3.40 5 5 17 16.80 4.10 -6 -5 -17 12.50 3.50 6 5 17 12.50 4.20 -7 -5 -17 4.60 3.30 7 5 17 1.70 3.90 -8 -5 -17 8.00 3.50 8 5 17 9.80 4.30 -9 -5 -17 3.70 3.60 9 5 17 7.50 4.40 -10 -5 -17 15.30 4.10 -2 6 17 0.00 3.70 1 -6 -17 -4.40 3.10 -1 6 17 -1.30 3.60 0 -6 -17 15.70 3.60 0 6 17 14.90 3.90 -1 -6 -17 4.30 3.20 1 6 17 5.50 3.40 1 6 17 11.00 3.60 -2 -6 -17 22.80 3.80 2 6 17 14.50 3.60 2 6 17 24.90 4.20 -3 -6 -17 1.70 3.10 3 6 17 6.40 3.60 -4 -6 -17 6.80 3.30 4 6 17 11.00 3.90 -5 -6 -17 34.20 4.10 5 6 17 36.90 4.80 -6 -6 -17 1.90 3.10 6 6 17 8.50 4.00 -7 -6 -17 40.20 4.30 7 6 17 63.19 7.80 -8 -6 -17 3.50 3.40 8 6 17 11.40 4.30 -9 -6 -17 24.70 4.20 9 6 17 22.60 4.80 -10 -6 -17 1.80 3.60 10 6 17 -1.50 4.50 -2 7 17 1.90 3.70 1 -7 -17 2.90 3.30 -1 7 17 4.80 3.70 0 -7 -17 0.00 3.10 0 7 17 0.80 3.30 -1 -7 -17 33.20 4.10 1 7 17 30.30 4.30 1 7 17 56.29 7.20 -2 -7 -17 13.50 3.50 2 7 17 23.70 4.20 -3 -7 -17 4.70 3.20 3 7 17 10.60 3.80 -4 -7 -17 0.80 3.10 4 7 17 2.10 3.60 -5 -7 -17 26.60 3.80 5 7 17 27.70 4.50 -6 -7 -17 18.50 3.70 6 7 17 17.10 4.30 -7 -7 -17 2.10 3.20 7 7 17 7.50 4.10 -8 -7 -17 27.60 4.10 8 7 17 27.20 4.80 -9 -7 -17 -2.80 3.30 9 7 17 4.10 4.20 -10 -7 -17 19.30 4.30 10 7 17 20.10 4.90 1 -8 -17 4.70 3.70 -1 8 17 -0.50 3.50 0 -8 -17 12.30 3.50 0 8 17 8.90 3.60 -1 -8 -17 2.60 3.20 -2 -8 -17 9.60 3.40 2 8 17 14.30 3.90 -3 -8 -17 3.30 3.10 3 8 17 5.60 3.60 -4 -8 -17 30.30 4.00 4 8 17 29.70 4.50 -5 -8 -17 60.09 6.00 5 8 17 81.49 7.80 -6 -8 -17 -0.40 3.10 6 8 17 7.40 4.10 -7 -8 -17 31.70 4.10 7 8 17 25.90 4.60 -8 -8 -17 -3.10 3.20 8 8 17 8.60 4.20 -9 -8 -17 21.30 4.10 9 8 17 19.20 4.60 -10 -8 -17 -1.10 3.70 10 8 17 4.00 4.40 -1 9 17 7.90 3.70 0 -9 -17 -2.40 3.10 -1 -9 -17 8.30 3.30 -2 -9 -17 0.60 3.00 2 9 17 3.70 3.50 -3 -9 -17 2.40 3.10 3 9 17 9.30 3.70 -4 -9 -17 6.80 3.20 4 9 17 14.70 4.00 -5 -9 -17 21.80 3.80 5 9 17 25.00 4.30 -6 -9 -17 67.49 6.10 6 9 17 73.69 7.90 -7 -9 -17 4.10 3.30 7 9 17 5.80 3.90 -8 -9 -17 19.30 3.80 8 9 17 16.70 4.40 -9 -9 -17 5.50 3.70 9 9 17 4.40 4.10 -10 -9 -17 15.10 4.20 10 9 17 19.50 4.90 0 -10 -17 9.10 3.50 -1 -10 -17 -4.20 3.00 -2 -10 -17 14.10 3.60 2 10 17 20.90 4.10 -3 -10 -17 -1.60 2.90 3 10 17 1.60 3.50 -4 -10 -17 8.70 3.20 4 10 17 11.80 3.90 -5 -10 -17 20.70 3.70 5 10 17 14.40 4.10 -6 -10 -17 3.00 3.20 6 10 17 2.50 3.80 -7 -10 -17 34.30 4.20 7 10 17 25.50 4.50 -8 -10 -17 4.60 3.50 8 10 17 5.80 4.10 -9 -10 -17 11.60 3.80 9 10 17 16.20 4.50 -10 -10 -17 4.90 3.90 10 10 17 6.70 4.50 -1 -11 -17 3.80 3.40 -2 -11 -17 1.10 3.20 -3 -11 -17 8.40 3.40 3 11 17 16.20 4.10 -4 -11 -17 10.50 3.40 4 11 17 13.40 4.10 -5 -11 -17 11.20 3.40 5 11 17 12.60 4.10 -6 -11 -17 24.00 4.00 6 11 17 27.20 4.60 -7 -11 -17 0.90 3.20 7 11 17 3.80 4.00 -8 -11 -17 5.50 3.40 8 11 17 5.20 4.20 -9 -11 -17 3.90 3.60 9 11 17 2.50 4.20 -2 -12 -17 6.20 3.40 -3 -12 -17 -0.80 3.10 3 12 17 0.50 3.60 -4 -12 -17 1.40 3.10 4 12 17 11.30 4.10 -5 -12 -17 17.20 3.70 5 12 17 14.60 4.30 -6 -12 -17 2.00 3.30 6 12 17 11.70 4.30 -7 -12 -17 22.00 4.00 7 12 17 16.00 4.50 -8 -12 -17 2.30 3.40 8 12 17 11.30 4.50 -9 -12 -17 8.00 3.90 9 12 17 16.40 5.00 -3 -13 -17 -0.30 3.10 3 13 17 -0.30 3.80 -4 -13 -17 0.10 3.10 4 13 17 -4.40 3.70 -5 -13 -17 12.90 3.50 5 13 17 16.70 4.40 -6 -13 -17 15.90 3.70 6 13 17 19.70 4.70 -7 -13 -17 6.50 3.60 7 13 17 2.80 4.30 -8 -13 -17 8.10 3.70 -5 -14 -17 4.20 3.30 5 14 17 -4.40 4.00 -6 -14 -17 5.80 3.50 -7 -14 -17 10.70 3.80 -2 -1 -18 -0.30 3.50 -3 -1 -18 2.30 3.30 0 2 18 3.40 4.00 -1 -2 -18 5.80 3.40 -1 -2 -18 -1.60 3.30 1 2 18 -0.20 3.90 1 2 18 -2.00 4.10 -2 -2 -18 1.70 3.50 -2 -2 -18 3.40 3.30 2 2 18 4.50 4.20 -3 -2 -18 1.60 3.10 -3 -2 -18 -0.20 3.30 -4 -2 -18 1.60 3.20 -4 -2 -18 -2.00 3.40 0 3 18 0.70 4.00 0 3 18 4.20 4.10 -1 -3 -18 -1.70 3.30 1 3 18 -0.70 4.00 1 3 18 7.80 4.10 -2 -3 -18 -4.10 3.20 -2 -3 -18 2.50 3.20 2 3 18 0.10 3.90 -3 -3 -18 -3.30 2.90 -3 -3 -18 -0.90 3.40 3 3 18 -0.10 4.00 -4 -3 -18 3.80 3.60 4 3 18 1.10 4.20 -5 -3 -18 15.50 3.90 -6 -3 -18 4.30 3.60 0 4 18 0.80 4.00 -1 -4 -18 14.20 3.90 1 4 18 18.40 4.40 1 4 18 13.90 4.30 -2 -4 -18 1.50 3.50 2 4 18 0.50 3.80 2 4 18 4.40 4.00 -3 -4 -18 2.00 3.40 -3 -4 -18 0.50 2.90 3 4 18 8.00 4.00 -4 -4 -18 11.40 3.70 4 4 18 16.60 4.60 -5 -4 -18 1.50 3.40 5 4 18 6.50 4.30 -6 -4 -18 6.90 3.60 -7 -4 -18 1.10 3.30 0 5 18 4.80 3.90 -1 -5 -18 1.00 3.30 1 5 18 6.80 3.80 1 5 18 0.50 3.70 -2 -5 -18 5.00 3.50 2 5 18 11.30 4.10 2 5 18 6.20 3.90 -3 -5 -18 -0.70 3.30 3 5 18 5.00 3.90 -4 -5 -18 7.30 3.50 4 5 18 8.40 4.20 -5 -5 -18 16.20 3.80 5 5 18 15.90 4.60 -6 -5 -18 7.60 3.60 6 5 18 9.00 4.50 -7 -5 -18 17.40 3.90 -8 -5 -18 8.00 3.70 0 6 18 1.10 3.60 -1 -6 -18 31.40 4.40 1 6 18 36.80 4.80 1 6 18 24.40 4.40 -2 -6 -18 4.00 3.50 2 6 18 17.10 4.20 -3 -6 -18 6.00 3.50 3 6 18 6.70 4.00 -4 -6 -18 7.20 3.50 4 6 18 15.10 4.40 -5 -6 -18 24.10 4.10 5 6 18 26.80 4.80 -6 -6 -18 4.10 3.50 6 6 18 16.60 4.60 -7 -6 -18 4.30 3.50 7 6 18 6.30 4.40 -8 -6 -18 16.30 4.10 0 7 18 5.30 3.90 -1 -7 -18 12.50 4.10 -2 -7 -18 2.10 3.40 2 7 18 11.40 4.00 -3 -7 -18 5.40 3.50 3 7 18 11.30 4.10 -4 -7 -18 2.50 3.30 4 7 18 7.80 4.10 -5 -7 -18 7.80 3.50 5 7 18 15.80 4.50 -6 -7 -18 41.40 4.70 6 7 18 36.90 5.20 -7 -7 -18 20.40 4.00 7 7 18 21.20 4.90 -8 -7 -18 13.10 3.90 -2 -8 -18 3.20 3.50 2 8 18 10.70 4.10 -3 -8 -18 -1.60 3.20 3 8 18 3.70 3.90 -4 -8 -18 2.00 3.30 4 8 18 6.50 4.10 -5 -8 -18 33.60 4.40 5 8 18 32.10 5.10 -6 -8 -18 49.00 4.90 6 8 18 72.09 8.40 -7 -8 -18 9.30 3.80 7 8 18 14.00 4.60 -8 -8 -18 18.60 4.10 8 8 18 25.50 5.40 2 9 18 7.90 4.00 -3 -9 -18 -2.10 3.30 3 9 18 2.20 3.90 -4 -9 -18 2.00 3.30 4 9 18 7.30 4.10 -5 -9 -18 2.20 3.40 5 9 18 -2.40 4.00 -6 -9 -18 26.50 4.10 6 9 18 18.50 4.70 -7 -9 -18 22.10 4.10 7 9 18 20.40 4.80 -8 -9 -18 4.40 3.70 8 9 18 7.70 4.90 -3 -10 -18 2.80 3.50 3 10 18 6.50 4.00 -4 -10 -18 -3.20 3.20 4 10 18 5.20 4.00 -5 -10 -18 34.50 4.30 5 10 18 31.90 4.90 -6 -10 -18 28.40 4.30 6 10 18 20.80 4.70 -7 -10 -18 -0.40 3.50 7 10 18 3.00 4.30 3 11 18 7.50 4.00 4 11 18 1.80 3.80 -5 -11 -18 6.00 3.50 5 11 18 7.20 4.20 -6 -11 -18 5.50 3.60 6 11 18 3.20 4.20 7 11 18 3.50 4.40 4 12 18 -0.10 3.90 5 12 18 17.80 4.70 3 6 19 13.70 4.70 3 7 19 8.20 4.40 4 8 19 6.50 4.60 _computing_structure_solution 'SHELXT 2014/4 (Sheldrick, 2014)' ; _shelx_hkl_checksum 78586 loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn _atom_site_refinement_flags_adp _atom_site_refinement_flags_occupancy _atom_site_disorder_assembly _atom_site_disorder_group Zn1 Zn 0.23636(2) 0.26357(2) 0.28281(2) 0.04113(10) Uani 1 1 d . . . . . C1 C 0.1510(2) 0.2688(2) 0.59631(19) 0.0515(6) Uani 1 1 d . . . . . H1A H 0.0684 0.3262 0.5941 0.077 Uiso 1 1 calc R U . . . H1B H 0.1996 0.2837 0.6295 0.077 Uiso 1 1 calc R U . . . H1C H 0.1444 0.1957 0.6353 0.077 Uiso 1 1 calc R U . . . C2 C 0.2139(2) 0.27018(18) 0.48826(17) 0.0406(5) Uani 1 1 d . . . . . C3 C 0.3326(2) 0.27518(19) 0.46306(18) 0.0445(5) Uani 1 1 d . . . . . H3A H 0.3536 0.2987 0.5072 0.053 Uiso 1 1 calc R U . . . C4 C 0.4243(2) 0.2502(2) 0.38156(19) 0.0449(5) Uani 1 1 d . . . . . C5 C 0.5527(3) 0.2361(3) 0.3890(2) 0.0637(7) Uani 1 1 d . . . . . H5A H 0.6063 0.1579 0.4002 0.096 Uiso 1 1 calc R U . . . H5B H 0.5493 0.2591 0.4464 0.096 Uiso 1 1 calc R U . . . H5C H 0.5858 0.2823 0.3251 0.096 Uiso 1 1 calc R U . . . C6 C 0.0450(2) 0.24027(19) 0.46908(17) 0.0402(5) Uani 1 1 d . . . . . C7 C 0.0536(2) 0.1293(2) 0.51695(18) 0.0449(5) Uani 1 1 d . . . . . C8 C -0.0542(3) 0.1061(2) 0.5577(2) 0.0551(6) Uani 1 1 d . . . . . H8A H -0.0496 0.0312 0.5921 0.066 Uiso 1 1 calc R U . . . C9 C -0.1679(3) 0.1906(3) 0.5486(2) 0.0611(7) Uani 1 1 d . . . . . H9A H -0.2412 0.1738 0.5758 0.073 Uiso 1 1 calc R U . . . C10 C -0.1747(2) 0.2994(3) 0.5000(2) 0.0559(7) Uani 1 1 d . . . . . H10A H -0.2534 0.3570 0.4935 0.067 Uiso 1 1 calc R U . . . C11 C -0.0697(2) 0.3267(2) 0.46040(19) 0.0481(6) Uani 1 1 d . . . . . C12 C -0.0787(3) 0.4455(2) 0.4105(3) 0.0651(8) Uani 1 1 d . . . . . H12A H -0.0330 0.4625 0.4446 0.098 Uiso 1 1 calc R U . . . H12B H -0.1654 0.4944 0.4164 0.098 Uiso 1 1 calc R U . . . H12C H -0.0435 0.4576 0.3380 0.098 Uiso 1 1 calc R U . . . C13 C 0.1778(2) 0.0368(2) 0.5231(2) 0.0568(7) Uani 1 1 d . . . . . H13A H 0.1666 -0.0347 0.5608 0.085 Uiso 1 1 calc R U . . . H13B H 0.2269 0.0481 0.5589 0.085 Uiso 1 1 calc R U . . . H13C H 0.2205 0.0371 0.4537 0.085 Uiso 1 1 calc R U . . . C14 C 0.5096(2) 0.1919(2) 0.23252(19) 0.0519(6) Uani 1 1 d . . . . . C15 C 0.5482(3) 0.2645(3) 0.1420(2) 0.0743(9) Uani 1 1 d . . . . . C16 C 0.6423(4) 0.2170(5) 0.0723(3) 0.1040(16) Uani 1 1 d . . . . . H16A H 0.6694 0.2645 0.0096 0.125 Uiso 1 1 calc R U . . . C17 C 0.6956(4) 0.1058(6) 0.0914(4) 0.1126(18) Uani 1 1 d . . . . . H17A H 0.7587 0.0763 0.0422 0.135 Uiso 1 1 calc R U . . . C18 C 0.6590(3) 0.0347(4) 0.1820(3) 0.0894(12) Uani 1 1 d . . . . . H18A H 0.6981 -0.0434 0.1953 0.107 Uiso 1 1 calc R U . . . C19 C 0.5653(3) 0.0767(3) 0.2540(2) 0.0623(7) Uani 1 1 d . . . . . C20 C 0.5203(3) 0.0001(3) 0.3506(3) 0.0774(9) Uani 1 1 d . . . . . H20A H 0.5708 -0.0774 0.3538 0.116 Uiso 1 1 calc R U . . . H20B H 0.4341 0.0134 0.3506 0.116 Uiso 1 1 calc R U . . . H20C H 0.5267 0.0142 0.4102 0.116 Uiso 1 1 calc R U . . . C21 C 0.4923(4) 0.3882(4) 0.1203(3) 0.1109(16) Uani 1 1 d . . . . . H21A H 0.5560 0.4209 0.0836 0.166 Uiso 1 1 calc R U . . . H21B H 0.4576 0.4053 0.1851 0.166 Uiso 1 1 calc R U . . . H21C H 0.4268 0.4192 0.0781 0.166 Uiso 1 1 calc R U . . . C22 C 0.3185(3) 0.1204(3) 0.1536(3) 0.0782(10) Uani 1 1 d . . . . . H22A H 0.3893 0.1411 0.1312 0.094 Uiso 1 1 calc R U . . . C23 C 0.3201(4) 0.0372(3) 0.1263(3) 0.0856(11) Uani 1 1 d D . . . . H23A H 0.3932 -0.0008 0.0890 0.103 Uiso 1 1 calc R U . . . C24 C 0.2157(4) 0.0053(3) 0.1518(3) 0.0916(12) Uani 1 1 d . . . . . H24A H 0.2304 -0.0659 0.2086 0.110 Uiso 1 1 calc R U . . . H24B H 0.2061 -0.0075 0.0919 0.110 Uiso 1 1 calc R U . . . C25 C 0.0987(3) 0.0900(2) 0.1831(2) 0.0569(7) Uani 1 1 d . . . . . C26 C -0.0172(4) 0.0881(3) 0.1866(2) 0.0689(9) Uani 1 1 d . . . . . H26A H -0.0214 0.0350 0.1634 0.083 Uiso 1 1 calc R U . . . C27 C -0.1246(3) 0.1604(3) 0.2223(2) 0.0703(9) Uani 1 1 d . . . . . H27A H -0.2021 0.1573 0.2244 0.084 Uiso 1 1 calc R U . . . C28 C -0.1176(3) 0.2371(3) 0.2549(2) 0.0638(8) Uani 1 1 d . . . . . H28A H -0.1911 0.2869 0.2810 0.077 Uiso 1 1 calc R U . . . C29 C -0.0052(2) 0.2431(2) 0.25043(19) 0.0513(6) Uani 1 1 d . . . . . H29A H -0.0035 0.2989 0.2714 0.062 Uiso 1 1 calc R U . . . C30 C 0.1057(2) 0.1699(2) 0.21607(17) 0.0456(5) Uani 1 1 d . . . . . C31 C 0.1554(3) 0.4337(3) 0.0862(2) 0.0604(7) Uani 1 1 d . . . . . H31A H 0.1664 0.3659 0.0779 0.072 Uiso 1 1 calc R U . . . C32 C 0.1180(4) 0.5326(3) 0.0053(2) 0.0787(10) Uani 1 1 d . . . . . H32A H 0.1081 0.5308 -0.0573 0.094 Uiso 1 1 calc R U . . . C33 C 0.0962(3) 0.6305(3) 0.0177(2) 0.0768(9) Uani 1 1 d . . . . . H33A H 0.0666 0.6986 -0.0349 0.092 Uiso 1 1 calc R U . . . C34 C 0.1175(3) 0.6311(2) 0.1084(2) 0.0594(7) Uani 1 1 d . . . . . C35 C 0.1006(3) 0.7296(2) 0.1260(3) 0.0751(9) Uani 1 1 d . . . . . H35A H 0.0694 0.7996 0.0761 0.090 Uiso 1 1 calc R U . . . C36 C 0.1278(3) 0.7258(3) 0.2121(3) 0.0767(10) Uani 1 1 d . . . . . H36A H 0.1155 0.7928 0.2226 0.092 Uiso 1 1 calc R U . . . C37 C 0.1746(3) 0.6231(3) 0.2867(2) 0.0672(8) Uani 1 1 d . . . . . H37A H 0.1957 0.6211 0.3465 0.081 Uiso 1 1 calc R U . . . C38 C 0.1900(3) 0.5258(2) 0.2741(2) 0.0539(6) Uani 1 1 d . . . . . H38A H 0.2203 0.4569 0.3256 0.065 Uiso 1 1 calc R U . . . C39 C 0.1609(2) 0.5279(2) 0.18495(18) 0.0467(5) Uani 1 1 d . . . . . N1 N 0.15664(17) 0.26400(15) 0.42571(14) 0.0381(4) Uani 1 1 d . . . . . N2 N 0.40593(18) 0.23612(16) 0.30177(15) 0.0436(4) Uani 1 1 d . . . . . N3 N 0.21688(19) 0.17760(18) 0.21369(16) 0.0483(5) Uani 1 1 d . . . . . N4 N 0.17618(19) 0.42981(17) 0.17351(15) 0.0474(5) Uani 1 1 d . . . . . C40 C 0.2295(10) 0.2824(11) 0.8568(9) 0.175(5) Uani 0.601(8) 1 d D U P A 1 H40A H 0.2341 0.2308 0.9268 0.263 Uiso 0.601(8) 1 calc R U P A 1 H40B H 0.2183 0.2486 0.8135 0.263 Uiso 0.601(8) 1 calc R U P A 1 H40C H 0.1596 0.3518 0.8572 0.263 Uiso 0.601(8) 1 calc R U P A 1 C41 C 0.3468(9) 0.3066(9) 0.8150(11) 0.263(8) Uani 0.601(8) 1 d DG U P A 1 C42 C 0.4178(13) 0.3136(12) 0.8713(8) 0.244(7) Uani 0.601(8) 1 d DG U P A 1 H42 H 0.3982 0.2947 0.9438 0.293 Uiso 0.601(8) 1 calc R U P A 1 C43 C 0.5174(13) 0.3481(13) 0.8215(13) 0.272(8) Uani 0.601(8) 1 d G U P A 1 H43 H 0.5659 0.3529 0.8599 0.326 Uiso 0.601(8) 1 calc R U P A 1 C44 C 0.5461(11) 0.3757(12) 0.7154(13) 0.334(9) Uani 0.601(8) 1 d G U P A 1 H44 H 0.6142 0.3993 0.6813 0.400 Uiso 0.601(8) 1 calc R U P A 1 C45 C 0.4752(15) 0.3688(14) 0.6591(9) 0.317(9) Uani 0.601(8) 1 d G U P A 1 H45 H 0.4948 0.3876 0.5866 0.380 Uiso 0.601(8) 1 calc R U P A 1 C46 C 0.3755(13) 0.3342(13) 0.7090(11) 0.294(8) Uani 0.601(8) 1 d DG U P A 1 H46 H 0.3270 0.3295 0.6705 0.353 Uiso 0.601(8) 1 calc R U P A 1 C47 C 0.4944(19) 0.4819(19) 0.6425(18) 0.253(11) Uani 0.399(8) 1 d D U P A 2 H47A H 0.5549 0.4892 0.6698 0.379 Uiso 0.399(8) 1 calc R U P A 2 H47B H 0.4302 0.5549 0.6199 0.379 Uiso 0.399(8) 1 calc R U P A 2 H47C H 0.5357 0.4533 0.5843 0.379 Uiso 0.399(8) 1 calc R U P A 2 C48 C 0.4399(19) 0.4068(17) 0.7207(14) 0.293(13) Uani 0.399(8) 1 d DG U P A 2 C49 C 0.5048(17) 0.2939(19) 0.7346(18) 0.297(13) Uani 0.399(8) 1 d DG U P A 2 H49 H 0.5837 0.2700 0.6958 0.356 Uiso 0.399(8) 1 calc R U P A 2 C50 C 0.454(3) 0.2161(15) 0.805(2) 0.348(14) Uani 0.399(8) 1 d DG U P A 2 H50 H 0.4986 0.1390 0.8150 0.417 Uiso 0.399(8) 1 calc R U P A 2 C51 C 0.339(3) 0.251(2) 0.8622(16) 0.326(14) Uani 0.399(8) 1 d G U P A 2 H51 H 0.3043 0.1980 0.9105 0.391 Uiso 0.399(8) 1 calc R U P A 2 C52 C 0.274(2) 0.364(3) 0.8482(18) 0.353(14) Uani 0.399(8) 1 d G U P A 2 H52 H 0.1951 0.3879 0.8870 0.424 Uiso 0.399(8) 1 calc R U P A 2 C53 C 0.325(2) 0.4418(17) 0.7774(19) 0.319(13) Uani 0.399(8) 1 d DG U P A 2 H53 H 0.2802 0.5189 0.7679 0.383 Uiso 0.399(8) 1 calc R U P A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Zn1 0.04126(16) 0.04384(16) 0.03868(15) -0.01034(11) -0.00821(11) -0.01625(12) C1 0.0548(15) 0.0595(15) 0.0457(13) -0.0207(12) -0.0070(11) -0.0215(12) C2 0.0434(12) 0.0347(11) 0.0418(12) -0.0113(9) -0.0104(9) -0.0102(9) C3 0.0463(13) 0.0448(12) 0.0454(12) -0.0115(10) -0.0123(10) -0.0176(10) C4 0.0412(12) 0.0439(12) 0.0464(12) -0.0037(10) -0.0123(10) -0.0179(10) C5 0.0489(15) 0.084(2) 0.0653(17) -0.0241(15) -0.0121(13) -0.0273(15) C6 0.0412(12) 0.0458(12) 0.0365(11) -0.0152(9) -0.0030(9) -0.0176(10) C7 0.0481(13) 0.0483(13) 0.0410(12) -0.0128(10) -0.0070(10) -0.0204(11) C8 0.0596(16) 0.0616(16) 0.0508(14) -0.0141(12) -0.0011(12) -0.0350(14) C9 0.0507(15) 0.082(2) 0.0653(17) -0.0342(15) 0.0070(13) -0.0366(15) C10 0.0387(13) 0.0710(18) 0.0629(16) -0.0352(14) -0.0017(11) -0.0145(12) C11 0.0454(13) 0.0519(14) 0.0499(13) -0.0222(11) -0.0063(10) -0.0145(11) C12 0.0508(16) 0.0466(15) 0.088(2) -0.0214(14) -0.0140(14) -0.0060(12) C13 0.0538(15) 0.0424(13) 0.0690(17) -0.0082(12) -0.0132(13) -0.0180(12) C14 0.0388(12) 0.0749(18) 0.0413(12) -0.0153(12) -0.0054(10) -0.0225(12) C15 0.0547(17) 0.115(3) 0.0474(15) -0.0058(16) -0.0051(13) -0.0442(18) C16 0.067(2) 0.199(5) 0.0486(18) -0.027(3) 0.0088(17) -0.072(3) C17 0.068(2) 0.217(6) 0.082(3) -0.094(4) 0.019(2) -0.053(3) C18 0.0559(19) 0.127(3) 0.101(3) -0.074(3) 0.0013(18) -0.020(2) C19 0.0470(15) 0.079(2) 0.0634(17) -0.0340(15) -0.0055(13) -0.0151(14) C20 0.077(2) 0.0531(17) 0.083(2) -0.0182(16) -0.0117(17) -0.0086(16) C21 0.089(3) 0.112(3) 0.092(3) 0.034(2) -0.011(2) -0.061(3) C22 0.0575(18) 0.103(3) 0.096(2) -0.062(2) -0.0030(17) -0.0254(18) C23 0.076(2) 0.094(3) 0.099(3) -0.064(2) -0.0067(19) -0.014(2) C24 0.115(3) 0.076(2) 0.103(3) -0.050(2) -0.006(2) -0.039(2) C25 0.0768(19) 0.0537(15) 0.0498(14) -0.0117(12) -0.0129(13) -0.0334(14) C26 0.101(3) 0.076(2) 0.0541(16) -0.0061(14) -0.0231(16) -0.059(2) C27 0.071(2) 0.099(2) 0.0524(16) -0.0053(16) -0.0169(14) -0.0527(19) C28 0.0554(17) 0.092(2) 0.0486(15) -0.0171(15) -0.0094(12) -0.0338(16) C29 0.0529(15) 0.0646(16) 0.0418(13) -0.0161(12) -0.0091(11) -0.0248(13) C30 0.0574(15) 0.0487(13) 0.0367(11) -0.0063(10) -0.0127(10) -0.0267(12) C31 0.0718(19) 0.0636(17) 0.0473(14) -0.0051(12) -0.0215(13) -0.0285(15) C32 0.100(3) 0.086(2) 0.0477(16) 0.0057(15) -0.0304(17) -0.042(2) C33 0.083(2) 0.068(2) 0.0586(18) 0.0131(15) -0.0254(16) -0.0291(18) C34 0.0516(15) 0.0489(14) 0.0575(16) 0.0005(12) -0.0020(12) -0.0191(12) C35 0.074(2) 0.0457(15) 0.079(2) -0.0030(15) 0.0052(17) -0.0228(15) C36 0.080(2) 0.0481(16) 0.091(2) -0.0239(16) 0.0198(19) -0.0306(16) C37 0.080(2) 0.0634(18) 0.0629(17) -0.0257(15) 0.0087(15) -0.0361(16) C38 0.0621(16) 0.0460(14) 0.0511(14) -0.0114(11) -0.0044(12) -0.0229(12) C39 0.0426(13) 0.0437(12) 0.0451(13) -0.0066(10) -0.0022(10) -0.0167(10) N1 0.0385(10) 0.0371(9) 0.0384(9) -0.0095(8) -0.0076(7) -0.0141(8) N2 0.0416(10) 0.0470(11) 0.0390(10) -0.0069(8) -0.0059(8) -0.0187(9) N3 0.0445(11) 0.0543(12) 0.0511(12) -0.0213(10) -0.0075(9) -0.0175(9) N4 0.0511(12) 0.0481(11) 0.0395(10) -0.0041(8) -0.0124(9) -0.0195(9) C40 0.158(9) 0.241(13) 0.160(9) -0.085(8) -0.055(7) -0.061(8) C41 0.218(10) 0.344(15) 0.262(11) -0.107(10) -0.050(8) -0.110(10) C42 0.219(11) 0.327(14) 0.238(11) -0.102(9) -0.050(8) -0.121(10) C43 0.248(12) 0.366(15) 0.257(12) -0.102(10) -0.045(9) -0.150(11) C44 0.324(14) 0.412(17) 0.307(12) -0.107(11) -0.048(9) -0.173(12) C45 0.291(13) 0.385(16) 0.313(12) -0.134(10) -0.037(9) -0.137(11) C46 0.284(13) 0.372(16) 0.269(11) -0.124(10) -0.035(8) -0.138(11) C47 0.181(15) 0.198(15) 0.335(19) -0.066(13) -0.098(13) -0.004(11) C48 0.294(16) 0.267(14) 0.316(17) -0.097(10) -0.058(11) -0.084(10) C49 0.310(16) 0.253(14) 0.304(18) -0.087(10) -0.050(12) -0.075(10) C50 0.353(17) 0.288(15) 0.355(19) -0.093(11) -0.021(12) -0.097(11) C51 0.339(17) 0.285(16) 0.341(19) -0.105(11) -0.031(13) -0.103(11) C52 0.373(17) 0.295(15) 0.359(19) -0.112(11) -0.016(13) -0.104(11) C53 0.325(16) 0.271(15) 0.344(18) -0.117(11) -0.021(12) -0.090(10) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Zn Zn 0.2839 1.4301 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle N3 Zn1 N1 123.48(8) N3 Zn1 N2 119.01(8) N1 Zn1 N2 96.30(8) N3 Zn1 N4 100.61(8) N1 Zn1 N4 111.25(8) N2 Zn1 N4 105.40(8) C2 C1 H1A 109.5 C2 C1 H1B 109.5 H1A C1 H1B 109.5 C2 C1 H1C 109.5 H1A C1 H1C 109.5 H1B C1 H1C 109.5 N1 C2 C3 124.8(2) N1 C2 C1 119.3(2) C3 C2 C1 115.8(2) C4 C3 C2 128.8(2) C4 C3 H3A 115.6 C2 C3 H3A 115.6 N2 C4 C3 124.6(2) N2 C4 C5 119.2(2) C3 C4 C5 116.2(2) C4 C5 H5A 109.5 C4 C5 H5B 109.5 H5A C5 H5B 109.5 C4 C5 H5C 109.5 H5A C5 H5C 109.5 H5B C5 H5C 109.5 C11 C6 C7 121.0(2) C11 C6 N1 120.2(2) C7 C6 N1 118.7(2) C8 C7 C6 118.8(2) C8 C7 C13 120.8(2) C6 C7 C13 120.4(2) C9 C8 C7 120.7(3) C9 C8 H8A 119.7 C7 C8 H8A 119.7 C10 C9 C8 119.7(2) C10 C9 H9A 120.1 C8 C9 H9A 120.1 C9 C10 C11 121.5(3) C9 C10 H10A 119.2 C11 C10 H10A 119.2 C10 C11 C6 118.2(2) C10 C11 C12 120.9(2) C6 C11 C12 120.9(2) C11 C12 H12A 109.5 C11 C12 H12B 109.5 H12A C12 H12B 109.5 C11 C12 H12C 109.5 H12A C12 H12C 109.5 H12B C12 H12C 109.5 C7 C13 H13A 109.5 C7 C13 H13B 109.5 H13A C13 H13B 109.5 C7 C13 H13C 109.5 H13A C13 H13C 109.5 H13B C13 H13C 109.5 C19 C14 C15 121.4(3) C19 C14 N2 119.0(2) C15 C14 N2 119.5(3) C14 C15 C16 117.3(4) C14 C15 C21 121.7(3) C16 C15 C21 121.1(4) C17 C16 C15 121.9(4) C17 C16 H16A 119.0 C15 C16 H16A 119.0 C16 C17 C18 120.4(4) C16 C17 H17A 119.8 C18 C17 H17A 119.8 C17 C18 C19 120.5(4) C17 C18 H18A 119.8 C19 C18 H18A 119.8 C18 C19 C14 118.5(3) C18 C19 C20 120.9(3) C14 C19 C20 120.5(3) C19 C20 H20A 109.5 C19 C20 H20B 109.5 H20A C20 H20B 109.5 C19 C20 H20C 109.5 H20A C20 H20C 109.5 H20B C20 H20C 109.5 C15 C21 H21A 109.5 C15 C21 H21B 109.5 H21A C21 H21B 109.5 C15 C21 H21C 109.5 H21A C21 H21C 109.5 H21B C21 H21C 109.5 C23 C22 N3 123.2(3) C23 C22 H22A 118.4 N3 C22 H22A 118.4 C22 C23 C24 122.0(3) C22 C23 H23A 119.0 C24 C23 H23A 119.0 C23 C24 C25 113.3(3) C23 C24 H24A 108.9 C25 C24 H24A 108.9 C23 C24 H24B 108.9 C25 C24 H24B 108.9 H24A C24 H24B 107.7 C26 C25 C30 119.3(3) C26 C25 C24 121.9(3) C30 C25 C24 118.8(3) C27 C26 C25 122.3(3) C27 C26 H26A 118.9 C25 C26 H26A 118.9 C28 C27 C26 118.4(3) C28 C27 H27A 120.8 C26 C27 H27A 120.8 C27 C28 C29 121.0(3) C27 C28 H28A 119.5 C29 C28 H28A 119.5 C28 C29 C30 122.0(3) C28 C29 H29A 119.0 C30 C29 H29A 119.0 N3 C30 C29 120.4(2) N3 C30 C25 122.5(2) C29 C30 C25 117.1(2) N4 C31 C32 123.5(3) N4 C31 H31A 118.3 C32 C31 H31A 118.3 C33 C32 C31 119.1(3) C33 C32 H32A 120.5 C31 C32 H32A 120.5 C32 C33 C34 119.7(3) C32 C33 H33A 120.2 C34 C33 H33A 120.2 C33 C34 C39 118.3(3) C33 C34 C35 123.2(3) C39 C34 C35 118.5(3) C36 C35 C34 121.1(3) C36 C35 H35A 119.4 C34 C35 H35A 119.4 C35 C36 C37 120.3(3) C35 C36 H36A 119.8 C37 C36 H36A 119.8 C38 C37 C36 120.7(3) C38 C37 H37A 119.7 C36 C37 H37A 119.7 C37 C38 C39 120.0(3) C37 C38 H38A 120.0 C39 C38 H38A 120.0 N4 C39 C38 119.4(2) N4 C39 C34 121.3(2) C38 C39 C34 119.3(2) C2 N1 C6 117.43(19) C2 N1 Zn1 120.95(16) C6 N1 Zn1 120.92(14) C4 N2 C14 119.5(2) C4 N2 Zn1 121.09(16) C14 N2 Zn1 119.16(15) C30 N3 C22 115.0(2) C30 N3 Zn1 124.35(16) C22 N3 Zn1 120.59(18) C31 N4 C39 118.0(2) C31 N4 Zn1 114.68(18) C39 N4 Zn1 127.28(16) C41 C40 H40A 109.5 C41 C40 H40B 109.5 H40A C40 H40B 109.5 C41 C40 H40C 109.5 H40A C40 H40C 109.5 H40B C40 H40C 109.5 C42 C41 C46 120.0 C42 C41 C40 125.9(10) C46 C41 C40 113.8(10) C43 C42 C41 120.0 C43 C42 H42 120.0 C41 C42 H42 120.0 C44 C43 C42 120.0 C44 C43 H43 120.0 C42 C43 H43 120.0 C43 C44 C45 120.0 C43 C44 H44 120.0 C45 C44 H44 120.0 C46 C45 C44 120.0 C46 C45 H45 120.0 C44 C45 H45 120.0 C45 C46 C41 120.0 C45 C46 H46 120.0 C41 C46 H46 120.0 C48 C47 H47A 109.5 C48 C47 H47B 109.5 H47A C47 H47B 109.5 C48 C47 H47C 109.5 H47A C47 H47C 109.5 H47B C47 H47C 109.5 C49 C48 C53 120.0 C49 C48 C47 116.8(15) C53 C48 C47 123.1(15) C50 C49 C48 120.0 C50 C49 H49 120.0 C48 C49 H49 120.0 C49 C50 C51 120.0 C49 C50 H50 120.0 C51 C50 H50 120.0 C50 C51 C52 120.0 C50 C51 H51 120.0 C52 C51 H51 120.0 C53 C52 C51 120.0 C53 C52 H52 120.0 C51 C52 H52 120.0 C52 C53 C48 120.0 C52 C53 H53 120.0 C48 C53 H53 120.0 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance Zn1 N3 1.949(2) Zn1 N1 1.9991(18) Zn1 N2 2.003(2) Zn1 N4 2.177(2) C1 C2 1.513(3) C1 H1A 0.9800 C1 H1B 0.9800 C1 H1C 0.9800 C2 N1 1.328(3) C2 C3 1.404(3) C3 C4 1.401(3) C3 H3A 0.9500 C4 N2 1.326(3) C4 C5 1.513(3) C5 H5A 0.9800 C5 H5B 0.9800 C5 H5C 0.9800 C6 C11 1.398(3) C6 C7 1.398(3) C6 N1 1.436(3) C7 C8 1.388(4) C7 C13 1.507(3) C8 C9 1.380(4) C8 H8A 0.9500 C9 C10 1.379(4) C9 H9A 0.9500 C10 C11 1.385(4) C10 H10A 0.9500 C11 C12 1.497(4) C12 H12A 0.9800 C12 H12B 0.9800 C12 H12C 0.9800 C13 H13A 0.9800 C13 H13B 0.9800 C13 H13C 0.9800 C14 C19 1.396(4) C14 C15 1.398(4) C14 N2 1.431(3) C15 C16 1.400(6) C15 C21 1.499(6) C16 C17 1.350(7) C16 H16A 0.9500 C17 C18 1.378(7) C17 H17A 0.9500 C18 C19 1.390(4) C18 H18A 0.9500 C19 C20 1.503(5) C20 H20A 0.9800 C20 H20B 0.9800 C20 H20C 0.9800 C21 H21A 0.9800 C21 H21B 0.9800 C21 H21C 0.9800 C22 C23 1.358(5) C22 N3 1.410(4) C22 H22A 0.9500 C23 C24 1.422(5) C23 H23A 0.9500 C24 C25 1.494(5) C24 H24A 0.9900 C24 H24B 0.9900 C25 C26 1.402(4) C25 C30 1.414(3) C26 C27 1.371(5) C26 H26A 0.9500 C27 C28 1.368(4) C27 H27A 0.9500 C28 C29 1.383(4) C28 H28A 0.9500 C29 C30 1.392(4) C29 H29A 0.9500 C30 N3 1.387(3) C31 N4 1.323(3) C31 C32 1.403(4) C31 H31A 0.9500 C32 C33 1.355(5) C32 H32A 0.9500 C33 C34 1.400(5) C33 H33A 0.9500 C34 C39 1.415(3) C34 C35 1.417(4) C35 C36 1.343(5) C35 H35A 0.9500 C36 C37 1.405(5) C36 H36A 0.9500 C37 C38 1.369(4) C37 H37A 0.9500 C38 C39 1.407(4) C38 H38A 0.9500 C39 N4 1.374(3) C40 C41 1.502(11) C40 H40A 0.9800 C40 H40B 0.9800 C40 H40C 0.9800 C41 C42 1.3900 C41 C46 1.3900 C42 C43 1.3900 C42 H42 0.9500 C43 C44 1.3900 C43 H43 0.9500 C44 C45 1.3900 C44 H44 0.9500 C45 C46 1.3900 C45 H45 0.9500 C46 H46 0.9500 C47 C48 1.427(15) C47 H47A 0.9800 C47 H47B 0.9800 C47 H47C 0.9800 C48 C49 1.3900 C48 C53 1.3900 C49 C50 1.3900 C49 H49 0.9500 C50 C51 1.3900 C50 H50 0.9500 C51 C52 1.3900 C51 H51 0.9500 C52 C53 1.3900 C52 H52 0.9500 C53 H53 0.9500 loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion N1 C2 C3 C4 -15.8(4) C1 C2 C3 C4 162.5(2) C2 C3 C4 N2 13.0(4) C2 C3 C4 C5 -165.4(2) C11 C6 C7 C8 -1.1(3) N1 C6 C7 C8 -179.1(2) C11 C6 C7 C13 178.3(2) N1 C6 C7 C13 0.3(3) C6 C7 C8 C9 1.8(4) C13 C7 C8 C9 -177.6(2) C7 C8 C9 C10 -1.0(4) C8 C9 C10 C11 -0.6(4) C9 C10 C11 C6 1.2(4) C9 C10 C11 C12 -178.2(3) C7 C6 C11 C10 -0.4(3) N1 C6 C11 C10 177.6(2) C7 C6 C11 C12 179.1(2) N1 C6 C11 C12 -3.0(4) C19 C14 C15 C16 2.0(4) N2 C14 C15 C16 -174.0(3) C19 C14 C15 C21 -177.5(3) N2 C14 C15 C21 6.5(4) C14 C15 C16 C17 -1.0(6) C21 C15 C16 C17 178.5(4) C15 C16 C17 C18 -0.6(7) C16 C17 C18 C19 1.1(6) C17 C18 C19 C14 -0.1(5) C17 C18 C19 C20 176.8(3) C15 C14 C19 C18 -1.5(4) N2 C14 C19 C18 174.5(3) C15 C14 C19 C20 -178.5(3) N2 C14 C19 C20 -2.4(4) N3 C22 C23 C24 3.5(6) C22 C23 C24 C25 16.3(6) C23 C24 C25 C26 163.9(3) C23 C24 C25 C30 -20.1(5) C30 C25 C26 C27 -0.9(4) C24 C25 C26 C27 175.1(3) C25 C26 C27 C28 0.4(4) C26 C27 C28 C29 1.1(4) C27 C28 C29 C30 -2.1(4) C28 C29 C30 N3 -179.3(2) C28 C29 C30 C25 1.6(4) C26 C25 C30 N3 -179.2(2) C24 C25 C30 N3 4.7(4) C26 C25 C30 C29 -0.1(4) C24 C25 C30 C29 -176.2(3) N4 C31 C32 C33 -3.1(5) C31 C32 C33 C34 3.4(5) C32 C33 C34 C39 -0.3(5) C32 C33 C34 C35 178.0(3) C33 C34 C35 C36 -176.7(3) C39 C34 C35 C36 1.6(5) C34 C35 C36 C37 0.3(5) C35 C36 C37 C38 -1.7(5) C36 C37 C38 C39 1.1(4) C37 C38 C39 N4 -179.7(2) C37 C38 C39 C34 0.9(4) C33 C34 C39 N4 -3.2(4) C35 C34 C39 N4 178.4(2) C33 C34 C39 C38 176.2(3) C35 C34 C39 C38 -2.2(4) C3 C2 N1 C6 169.5(2) C1 C2 N1 C6 -8.7(3) C3 C2 N1 Zn1 -1.0(3) C1 C2 N1 Zn1 -179.24(16) C11 C6 N1 C2 97.9(3) C7 C6 N1 C2 -84.1(3) C11 C6 N1 Zn1 -91.6(2) C7 C6 N1 Zn1 86.4(2) C3 C4 N2 C14 -169.1(2) C5 C4 N2 C14 9.3(3) C3 C4 N2 Zn1 5.8(3) C5 C4 N2 Zn1 -175.85(19) C19 C14 N2 C4 87.1(3) C15 C14 N2 C4 -96.8(3) C19 C14 N2 Zn1 -87.9(3) C15 C14 N2 Zn1 88.2(3) C29 C30 N3 C22 -164.0(3) C25 C30 N3 C22 15.0(4) C29 C30 N3 Zn1 14.0(3) C25 C30 N3 Zn1 -166.88(19) C23 C22 N3 C30 -19.8(5) C23 C22 N3 Zn1 162.1(3) C32 C31 N4 C39 -0.4(4) C32 C31 N4 Zn1 -178.9(3) C38 C39 N4 C31 -175.9(2) C34 C39 N4 C31 3.6(4) C38 C39 N4 Zn1 2.4(3) C34 C39 N4 Zn1 -178.11(18) C46 C41 C42 C43 0.0 C40 C41 C42 C43 -173.2(8) C41 C42 C43 C44 0.0 C42 C43 C44 C45 0.0 C43 C44 C45 C46 0.0 C44 C45 C46 C41 0.0 C42 C41 C46 C45 0.0 C40 C41 C46 C45 174.0(7) C53 C48 C49 C50 0.0 C47 C48 C49 C50 -176.5(8) C48 C49 C50 C51 0.0 C49 C50 C51 C52 0.0 C50 C51 C52 C53 0.0 C51 C52 C53 C48 0.0 C49 C48 C53 C52 0.0 C47 C48 C53 C52 176.2(9)