#------------------------------------------------------------------------------ #$Date: 2018-02-04 00:26:57 +0200 (Sun, 04 Feb 2018) $ #$Revision: 206122 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/43/4514337.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4514337 loop_ _publ_author_name 'Korvorapun, Korkit' 'Kaplaneris, Nikolaos' 'Rogge, Torben' 'Warratz, Svenja' 'St\"uckl, A. Claudia' 'Ackermann, Lutz' _publ_section_title ; Sequential meta-/ortho-C--H Functionalizations by One-Pot Ruthenium(II/III) Catalysis ; _journal_issue 2 _journal_name_full 'ACS Catalysis' _journal_page_first 886 _journal_paper_doi 10.1021/acscatal.7b03648 _journal_volume 8 _journal_year 2018 _chemical_formula_moiety 'C21 H27 N3 O' _chemical_formula_sum 'C21 H27 N3 O' _chemical_formula_weight 337.45 _space_group_crystal_system triclinic _space_group_IT_number 2 _space_group_name_Hall '-P 1' _space_group_name_H-M_alt 'P -1' _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2017-07-14 _audit_creation_method ; Olex2 1.2 (compiled 2017.03.28 svn.r3405 for OlexSys, GUI svn.r5337) ; _cell_angle_alpha 89.316(2) _cell_angle_beta 85.141(2) _cell_angle_gamma 82.592(2) _cell_formula_units_Z 4 _cell_length_a 10.1934(6) _cell_length_b 10.7135(6) _cell_length_c 17.2661(11) _cell_measurement_reflns_used 3012 _cell_measurement_temperature 100 _cell_measurement_theta_max 29.00 _cell_measurement_theta_min 2.43 _cell_volume 1863.12(19) _computing_cell_refinement 'SAINT v8.37A (Bruker, 2015)' _computing_data_reduction 'SAINT v8.37A (Bruker, 2015)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 99.99 _diffrn_measured_fraction_theta_full 0.997 _diffrn_measured_fraction_theta_max 0.997 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0272 _diffrn_reflns_av_unetI/netI 0.0158 _diffrn_reflns_Laue_measured_fraction_full 0.997 _diffrn_reflns_Laue_measured_fraction_max 0.997 _diffrn_reflns_limit_h_max 14 _diffrn_reflns_limit_h_min -14 _diffrn_reflns_limit_k_max 15 _diffrn_reflns_limit_k_min -15 _diffrn_reflns_limit_l_max 25 _diffrn_reflns_limit_l_min -25 _diffrn_reflns_number 105267 _diffrn_reflns_point_group_measured_fraction_full 0.997 _diffrn_reflns_point_group_measured_fraction_max 0.997 _diffrn_reflns_theta_full 25.242 _diffrn_reflns_theta_max 31.533 _diffrn_reflns_theta_min 2.252 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.075 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.9717 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0966 before and 0.0456 after correction. The Ratio of minimum to maximum transmission is 0.9717. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.203 _exptl_crystal_description block _exptl_crystal_F_000 728 _exptl_crystal_size_max 0.417 _exptl_crystal_size_mid 0.182 _exptl_crystal_size_min 0.144 _refine_diff_density_max 0.461 _refine_diff_density_min -0.190 _refine_diff_density_rms 0.043 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.043 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 453 _refine_ls_number_reflns 12396 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.043 _refine_ls_R_factor_all 0.0432 _refine_ls_R_factor_gt 0.0394 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0579P)^2^+0.5345P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1086 _refine_ls_wR_factor_ref 0.1119 _reflns_Friedel_coverage 0.000 _reflns_number_gt 11294 _reflns_number_total 12396 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs7b03648_si_003.cif _cod_data_source_block mo_0069_cg_0m _cod_depositor_comments 'Adding full bibliography for 4514336--4514340.cif.' _cod_database_code 4514337 _shelx_shelxl_version_number 2014/7 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C2(H2), C23(H23) 2.b Secondary CH2 refined with riding coordinates: C3(H3A,H3B), C4(H4A,H4B), C5(H5A,H5B), C17(H17A,H17B), C18(H18A,H18B), C19(H19A,H19B), C20(H20A,H20B), C21(H21A,H21B), C24(H24A,H24B), C25(H25A,H25B), C26(H26A,H26B), C38(H38A,H38B), C39(H39A,H39B), C40(H40A,H40B), C41(H41A, H41B), C42(H42A,H42B) 2.c Aromatic/amide H refined with riding coordinates: C8(H8), C9(H9), C10(H10), C12(H12), C14(H14), C15(H15), C16(H16), C29(H29), C31(H31), C32(H32), C33(H33), C35(H35), C36(H36), C37(H37) 2.d Idealised Me refined as rotating group: C6(H6A,H6B,H6C), C27(H27A,H27B,H27C) ; _shelx_res_file ; mo_0069_cg_0m.res created by SHELXL-2014/7 TITL mo_0069_cg_0m_a.res in P-1 REM Old TITL mo_0069_CG_0m in P-1 REM SHELXT solution in P-1 REM R1 0.156, Rweak 0.008, Alpha 0.038, Orientation as input REM Formula found by SHELXT: C42 N6 O2 CELL 0.71073 10.1934 10.7135 17.2661 89.316 85.141 82.592 ZERR 4 0.0006 0.0006 0.0011 0.002 0.002 0.002 LATT 1 SFAC C H N O UNIT 84 108 12 4 L.S. 4 0 0 PLAN 20 TEMP -173.16 BOND $H list 4 fmap 2 53 acta OMIT 2 1 0 OMIT 2 0 2 OMIT 2 0 3 OMIT 6 0 9 OMIT 0 6 3 OMIT -3 0 12 OMIT 1 0 3 OMIT 0 0 15 OMIT 0 0 13 REM REM REM WGHT 0.057900 0.534500 FVAR 1.01464 O1 4 0.323172 -0.298682 0.254247 11.00000 0.02189 0.01363 = 0.02020 0.00069 -0.00047 -0.00393 N1 3 0.277727 -0.140145 0.341499 11.00000 0.02115 0.01771 = 0.01256 0.00078 0.00022 -0.00575 N2 3 0.182007 0.362253 0.191640 11.00000 0.01731 0.01650 = 0.02556 -0.00150 -0.00546 -0.00143 N3 3 0.020575 0.361671 0.099213 11.00000 0.02216 0.01799 = 0.01993 0.00058 -0.00596 0.00418 C1 1 0.328316 -0.187976 0.271609 11.00000 0.01209 0.01455 = 0.01374 0.00215 -0.00218 -0.00159 C2 1 0.386746 -0.100333 0.211135 11.00000 0.01251 0.01283 = 0.01303 0.00171 -0.00108 -0.00144 AFIX 13 H2 2 0.431561 -0.038052 0.238509 11.00000 -1.20000 AFIX 0 C3 1 0.489914 -0.176594 0.154412 11.00000 0.01444 0.01503 = 0.01550 0.00205 0.00073 0.00020 AFIX 23 H3A 2 0.556236 -0.227911 0.184198 11.00000 -1.20000 H3B 2 0.445259 -0.234695 0.124595 11.00000 -1.20000 AFIX 0 C4 1 0.560477 -0.091551 0.098160 11.00000 0.01988 0.01996 = 0.02368 0.00882 0.00641 0.00421 AFIX 23 H4A 2 0.596934 -0.028079 0.128425 11.00000 -1.20000 H4B 2 0.494630 -0.046033 0.065471 11.00000 -1.20000 AFIX 0 C5 1 0.673180 -0.161604 0.045177 11.00000 0.01857 0.02499 = 0.01696 0.00408 0.00356 0.00203 AFIX 23 H5A 2 0.640356 -0.233524 0.020849 11.00000 -1.20000 H5B 2 0.700310 -0.104323 0.003094 11.00000 -1.20000 AFIX 0 C6 1 0.793464 -0.210137 0.088323 11.00000 0.01616 0.02318 = 0.02394 -0.00095 0.00111 -0.00118 AFIX 137 H6A 2 0.865374 -0.247528 0.051151 11.00000 -1.50000 H6B 2 0.769662 -0.273982 0.126234 11.00000 -1.50000 H6C 2 0.822919 -0.140198 0.115405 11.00000 -1.50000 AFIX 0 C7 1 0.271897 -0.029863 0.171038 11.00000 0.01184 0.01379 = 0.01255 0.00137 -0.00092 -0.00189 C8 1 0.195647 -0.095683 0.126335 11.00000 0.01620 0.01478 = 0.01633 0.00007 -0.00225 -0.00328 AFIX 43 H8 2 0.216813 -0.184168 0.120116 11.00000 -1.20000 AFIX 0 C9 1 0.088842 -0.032047 0.090910 11.00000 0.01584 0.01911 = 0.01644 -0.00051 -0.00377 -0.00482 AFIX 43 H9 2 0.036647 -0.077606 0.061258 11.00000 -1.20000 AFIX 0 C10 1 0.057900 0.097619 0.098551 11.00000 0.01299 0.01932 = 0.01512 0.00041 -0.00260 -0.00165 AFIX 43 H10 2 -0.015561 0.140365 0.074506 11.00000 -1.20000 AFIX 0 C11 1 0.134997 0.164952 0.141641 11.00000 0.01233 0.01428 = 0.01330 0.00034 -0.00085 -0.00075 C12 1 0.240397 0.100214 0.178689 11.00000 0.01243 0.01409 = 0.01356 0.00072 -0.00154 -0.00187 AFIX 43 H12 2 0.291157 0.145478 0.209456 11.00000 -1.20000 AFIX 0 C13 1 0.110314 0.304525 0.144932 11.00000 0.01328 0.01522 = 0.01488 0.00040 -0.00042 0.00059 C14 1 0.002711 0.487776 0.101165 11.00000 0.02427 0.01874 = 0.02184 0.00224 -0.00279 0.00524 AFIX 43 H14 2 -0.060514 0.531667 0.069905 11.00000 -1.20000 AFIX 0 C15 1 0.072198 0.556619 0.146623 11.00000 0.02251 0.01500 = 0.02625 0.00127 0.00274 0.00078 AFIX 43 H15 2 0.058924 0.646029 0.147067 11.00000 -1.20000 AFIX 0 C16 1 0.162529 0.488018 0.191648 11.00000 0.01918 0.01721 = 0.02996 -0.00235 -0.00247 -0.00248 AFIX 43 H16 2 0.212378 0.532092 0.223668 11.00000 -1.20000 AFIX 0 C17 1 0.218080 -0.221898 0.399305 11.00000 0.02607 0.02752 = 0.01564 0.00334 0.00128 -0.01113 AFIX 23 H17A 2 0.214085 -0.305072 0.375876 11.00000 -1.20000 H17B 2 0.126292 -0.184402 0.416012 11.00000 -1.20000 AFIX 0 C18 1 0.299765 -0.238384 0.469516 11.00000 0.03742 0.02770 = 0.01588 0.00529 -0.00320 -0.00694 AFIX 23 H18A 2 0.389056 -0.282919 0.453638 11.00000 -1.20000 H18B 2 0.256188 -0.290127 0.509341 11.00000 -1.20000 AFIX 0 C19 1 0.313010 -0.110494 0.503915 11.00000 0.03983 0.03314 = 0.01552 -0.00005 -0.00473 -0.00686 AFIX 23 H19A 2 0.372682 -0.122015 0.546501 11.00000 -1.20000 H19B 2 0.224902 -0.070766 0.525965 11.00000 -1.20000 AFIX 0 C20 1 0.368865 -0.024645 0.441569 11.00000 0.03191 0.02613 = 0.01912 -0.00370 -0.00498 -0.00706 AFIX 23 H20A 2 0.368751 0.060218 0.463666 11.00000 -1.20000 H20B 2 0.461859 -0.058469 0.424942 11.00000 -1.20000 AFIX 0 C21 1 0.286985 -0.014566 0.371214 11.00000 0.02546 0.01792 = 0.01610 -0.00208 -0.00087 -0.00182 AFIX 23 H21A 2 0.196838 0.028788 0.386277 11.00000 -1.20000 H21B 2 0.329193 0.035745 0.330030 11.00000 -1.20000 AFIX 0 O2 4 0.488962 0.210947 0.287107 11.00000 0.02474 0.01395 = 0.02180 0.00286 0.00015 -0.00210 N4 3 0.510314 0.343073 0.184878 11.00000 0.01914 0.01399 = 0.01431 -0.00023 0.00009 -0.00369 N5 3 0.689935 0.847132 0.307689 11.00000 0.01635 0.01851 = 0.02285 -0.00117 -0.00272 -0.00167 N6 3 0.924311 0.783964 0.293846 11.00000 0.01543 0.02420 = 0.02259 -0.00080 -0.00081 -0.00421 C22 1 0.492829 0.319245 0.261853 11.00000 0.01412 0.01479 = 0.01520 0.00076 -0.00118 -0.00129 C23 1 0.486839 0.430168 0.317596 11.00000 0.01567 0.01462 = 0.01356 0.00082 -0.00165 -0.00154 AFIX 13 H23 2 0.428093 0.503126 0.297348 11.00000 -1.20000 AFIX 0 C24 1 0.429596 0.397382 0.399267 11.00000 0.01885 0.02152 = 0.01340 0.00140 -0.00109 -0.00264 AFIX 23 H24A 2 0.482127 0.319913 0.417309 11.00000 -1.20000 H24B 2 0.439359 0.466225 0.435245 11.00000 -1.20000 AFIX 0 C25 1 0.283797 0.377103 0.403363 11.00000 0.01892 0.02412 = 0.01530 0.00103 0.00002 -0.00377 AFIX 23 H25A 2 0.231597 0.451865 0.381781 11.00000 -1.20000 H25B 2 0.274456 0.303593 0.371015 11.00000 -1.20000 AFIX 0 C26 1 0.228219 0.355006 0.486425 11.00000 0.02337 0.02979 = 0.01597 0.00096 0.00174 -0.00740 AFIX 23 H26A 2 0.286274 0.285812 0.509622 11.00000 -1.20000 H26B 2 0.229915 0.431905 0.517361 11.00000 -1.20000 AFIX 0 C27 1 0.086964 0.321880 0.491683 11.00000 0.02726 0.04169 = 0.02368 -0.00224 0.00445 -0.01455 AFIX 137 H27A 2 0.085215 0.243407 0.463420 11.00000 -1.50000 H27B 2 0.028834 0.389818 0.468678 11.00000 -1.50000 H27C 2 0.055887 0.311085 0.546336 11.00000 -1.50000 AFIX 0 C28 1 0.626235 0.466379 0.318698 11.00000 0.01559 0.01697 = 0.01266 0.00073 -0.00214 -0.00130 C29 1 0.647719 0.592033 0.313401 11.00000 0.01453 0.01684 = 0.01353 0.00045 -0.00186 -0.00088 AFIX 43 H29 2 0.574238 0.655630 0.310289 11.00000 -1.20000 AFIX 0 C30 1 0.775840 0.626191 0.312586 11.00000 0.01470 0.01843 = 0.01286 -0.00013 -0.00153 -0.00158 C31 1 0.883419 0.532363 0.318183 11.00000 0.01422 0.02297 = 0.01731 -0.00045 -0.00194 0.00015 AFIX 43 H31 2 0.970783 0.554461 0.317807 11.00000 -1.20000 AFIX 0 C32 1 0.862761 0.406867 0.324294 11.00000 0.01706 0.02167 = 0.02194 0.00026 -0.00344 0.00281 AFIX 43 H32 2 0.936063 0.343359 0.328283 11.00000 -1.20000 AFIX 0 C33 1 0.735046 0.373780 0.324598 11.00000 0.01902 0.01736 = 0.01925 0.00159 -0.00353 0.00048 AFIX 43 H33 2 0.721686 0.287748 0.328839 11.00000 -1.20000 AFIX 0 C34 1 0.797738 0.760167 0.304550 11.00000 0.01486 0.01998 = 0.01345 -0.00079 -0.00161 -0.00267 C35 1 0.711763 0.967034 0.297345 11.00000 0.02055 0.01908 = 0.02662 -0.00165 -0.00357 -0.00218 AFIX 43 H35 2 0.637835 1.031047 0.299085 11.00000 -1.20000 AFIX 0 C36 1 0.838518 1.001045 0.284181 11.00000 0.02388 0.02105 = 0.02562 -0.00096 -0.00159 -0.00705 AFIX 43 H36 2 0.853003 1.086182 0.275836 11.00000 -1.20000 AFIX 0 C37 1 0.942749 0.904555 0.283834 11.00000 0.01850 0.02616 = 0.02405 -0.00146 0.00035 -0.00780 AFIX 43 H37 2 1.030955 0.924813 0.276174 11.00000 -1.20000 AFIX 0 C38 1 0.530774 0.239244 0.129608 11.00000 0.02796 0.02033 = 0.01898 -0.00575 0.00437 -0.00952 AFIX 23 H38A 2 0.460178 0.249909 0.093187 11.00000 -1.20000 H38B 2 0.525280 0.158835 0.157805 11.00000 -1.20000 AFIX 0 C39 1 0.666157 0.235058 0.084088 11.00000 0.03100 0.02158 = 0.02437 -0.00409 0.00996 -0.00433 AFIX 23 H39A 2 0.676632 0.167214 0.044768 11.00000 -1.20000 H39B 2 0.736967 0.215948 0.119916 11.00000 -1.20000 AFIX 0 C40 1 0.680257 0.360735 0.043743 11.00000 0.03442 0.02664 = 0.02092 -0.00103 0.00941 -0.00884 AFIX 23 H40A 2 0.617985 0.374151 0.002545 11.00000 -1.20000 H40B 2 0.771659 0.359366 0.018990 11.00000 -1.20000 AFIX 0 C41 1 0.650616 0.468529 0.102418 11.00000 0.02923 0.02050 = 0.02235 0.00160 0.00446 -0.00881 AFIX 23 H41A 2 0.721096 0.461910 0.138887 11.00000 -1.20000 H41B 2 0.650966 0.549859 0.074621 11.00000 -1.20000 AFIX 0 C42 1 0.516368 0.465573 0.148101 11.00000 0.02350 0.01640 = 0.01507 0.00309 -0.00168 -0.00169 AFIX 23 H42A 2 0.502794 0.532088 0.188353 11.00000 -1.20000 H42B 2 0.444693 0.482480 0.112657 11.00000 -1.20000 AFIX 0 HKLF 4 REM mo_0069_cg_0m_a.res in P-1 REM R1 = 0.0394 for 11294 Fo > 4sig(Fo) and 0.0432 for all 12396 data REM 453 parameters refined using 0 restraints END WGHT 0.0579 0.5328 REM Highest difference peak 0.461, deepest hole -0.190, 1-sigma level 0.043 Q1 1 0.2496 0.0364 0.1798 11.00000 0.05 0.46 Q2 1 0.1244 0.2362 0.1428 11.00000 0.05 0.45 Q3 1 0.8232 0.5796 0.3160 11.00000 0.05 0.44 Q4 1 0.4998 0.3817 0.2873 11.00000 0.05 0.43 Q5 1 0.3544 -0.1421 0.2419 11.00000 0.05 0.43 Q6 1 0.6424 0.5258 0.3160 11.00000 0.05 0.42 Q7 1 0.0956 0.1334 0.1189 11.00000 0.05 0.42 Q8 1 0.2223 -0.0632 0.1555 11.00000 0.05 0.39 Q9 1 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1017.25 24.5256 6 5 2 0 1021.48 22.1710 10 -6 -2 0 3.16657 0.84174 10 -6 -2 0 2.84516 0.52132 2 -6 -2 0 1.57020 0.96451 9 -6 -2 0 0.58768 0.93608 4 -6 -2 0 2.65695 0.56407 2 -6 -2 0 0.89230 0.88379 7 6 2 0 3.04965 1.42818 6 6 2 0 3.06938 0.91101 2 6 2 0 2.48192 1.11645 4 6 2 0 3.18815 1.04483 10 6 2 0 2.21551 1.10104 9 6 2 0 3.01732 0.70597 3 6 2 0 3.01770 0.98701 2 6 2 0 3.03595 0.96551 10 -7 -2 0 256.533 8.87525 4 -7 -2 0 255.046 7.33636 10 -7 -2 0 248.003 6.14128 2 -7 -2 0 245.251 7.52019 10 -7 -2 0 250.871 5.95801 2 -7 -2 0 242.365 8.84891 9 -7 -2 0 250.900 8.48157 7 7 2 0 246.670 8.12257 4 7 2 0 249.545 9.49170 6 7 2 0 252.326 7.49941 2 7 2 0 240.768 7.40559 10 7 2 0 255.216 9.10517 9 7 2 0 243.053 8.40003 2 7 2 0 257.659 7.74757 10 7 2 0 251.953 6.42128 3 -8 -2 0 182.273 4.71372 2 -8 -2 0 185.000 7.75983 4 -8 -2 0 185.533 4.91572 2 -8 -2 0 175.416 7.75138 9 -8 -2 0 186.774 6.24223 10 -8 -2 0 188.009 7.35170 7 -8 -2 0 185.185 6.56394 10 8 2 0 175.832 6.89886 4 8 2 0 193.846 8.53544 6 8 2 0 188.735 6.31141 2 8 2 0 184.859 4.95737 3 8 2 0 178.046 6.34469 8 8 2 0 184.425 6.70229 10 8 2 0 174.129 7.84036 9 8 2 0 178.321 6.50789 2 -9 -2 0 410.662 9.25509 2 -9 -2 0 408.044 11.8295 10 -9 -2 0 408.333 11.3437 10 -9 -2 0 392.715 12.6334 7 -9 -2 0 412.208 13.4507 4 9 2 0 411.922 14.4328 6 9 2 0 401.338 11.4749 2 9 2 0 413.274 11.8075 2 9 2 0 411.656 12.1025 10 9 2 0 418.136 13.9007 9 9 2 0 400.799 9.03057 3 9 2 0 385.603 11.3479 8 -10 -2 0 327.370 7.49074 2 -10 -2 0 312.719 12.0330 4 -10 -2 0 308.990 10.2877 10 -10 -2 0 333.747 11.5521 7 -10 -2 0 324.263 9.97556 10 10 2 0 327.148 10.5414 2 10 2 0 331.685 10.4713 10 10 2 0 319.710 10.7903 10 10 2 0 326.476 10.3321 2 10 2 0 320.663 10.1260 8 10 2 0 343.099 12.8441 9 -11 -2 0 1168.43 27.8599 10 -11 -2 0 1169.14 29.8668 7 -11 -2 0 1139.26 30.8940 4 11 2 0 1232.61 36.1852 9 11 2 0 1178.52 29.2744 10 11 2 0 1172.08 28.6296 2 11 2 0 1185.32 28.5245 10 11 2 0 1157.85 28.4982 2 -12 -2 0 192.725 8.94900 7 -12 -2 0 180.635 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11.2741 2 1 -3 0 478.737 11.5672 10 1 -3 0 490.621 11.7052 3 1 -3 0 482.259 11.6667 10 -1 3 0 499.674 10.9064 9 -1 3 0 504.544 11.3813 2 -1 3 0 500.392 11.6921 10 -1 3 0 475.227 11.5798 3 -1 3 0 467.136 11.5719 10 -1 3 0 480.445 11.5740 8 -1 3 0 482.834 11.4435 2 0 -3 0 31.3317 1.92440 8 0 -3 0 34.4233 1.76721 10 0 -3 0 33.2985 1.15507 9 0 -3 0 33.1836 1.80688 5 0 -3 0 31.7988 1.60653 2 0 -3 0 32.0232 1.74967 10 0 -3 0 33.2489 1.51480 2 0 3 0 32.7218 1.95425 8 0 3 0 35.4042 1.63733 2 0 3 0 29.5912 1.91047 3 0 3 0 34.0706 1.76543 2 0 3 0 34.2748 1.78373 10 0 3 0 31.5092 1.75271 10 0 3 0 33.3600 1.98362 7 0 3 0 34.4826 1.15177 9 -1 -3 0 32.4289 1.69162 5 -1 -3 0 32.6171 2.07180 7 -1 -3 0 28.3800 0.97894 2 -1 -3 0 31.2203 1.48315 10 -1 -3 0 31.1532 1.03177 2 -1 -3 0 31.5482 1.90165 8 -1 -3 0 33.3886 2.03357 3 1 3 0 37.2238 2.11986 3 1 3 0 30.6895 1.04204 9 1 3 0 30.6825 1.47050 10 1 3 0 32.6896 1.32962 2 1 3 0 34.1329 1.44202 2 1 3 0 29.3907 1.50632 10 1 3 0 33.3684 1.68617 5 -2 -3 0 84.3256 3.56480 7 -2 -3 0 85.0790 3.05234 5 -2 -3 0 89.0775 3.29441 3 -2 -3 0 86.2660 2.34135 10 2 3 0 83.0249 2.65621 9 2 3 0 86.4935 2.17251 2 2 3 0 86.5966 3.03358 5 2 3 0 85.1602 3.36911 4 2 3 0 87.1565 2.54027 10 2 3 0 86.2716 2.44360 10 2 3 0 83.4343 3.49305 7 2 3 0 85.1911 3.27475 3 2 3 0 85.1038 3.41311 6 2 3 0 84.8233 2.17714 2 -3 -3 0 184.371 5.49403 3 -3 -3 0 202.121 6.36858 7 -3 -3 0 193.199 6.13214 4 -3 -3 0 195.376 4.53790 10 -3 -3 0 193.886 4.72670 10 -3 -3 0 197.575 5.52988 9 3 3 0 191.248 6.13726 7 3 3 0 200.943 5.56246 9 3 3 0 195.277 5.71329 5 3 3 0 198.031 4.43215 2 3 3 0 195.853 4.69062 10 3 3 0 192.864 5.65543 3 3 3 0 198.803 4.78136 10 3 3 0 193.503 4.39897 2 3 3 0 190.682 6.34232 6 -4 -3 0 127.764 5.02541 4 -4 -3 0 129.319 4.69052 9 -4 -3 0 133.439 4.21154 3 -4 -3 0 132.538 5.14058 7 -4 -3 0 131.896 3.59537 10 4 3 0 134.400 5.48022 6 4 3 0 136.020 4.96211 4 4 3 0 134.904 4.84094 5 4 3 0 134.732 4.39873 3 4 3 0 131.774 4.97354 7 4 3 0 143.752 4.84599 9 4 3 0 138.037 3.77986 10 4 3 0 133.772 3.56805 2 4 3 0 133.421 3.39425 2 -5 -3 0 270.866 6.77545 10 -5 -3 0 267.915 6.92534 3 -5 -3 0 268.764 8.48516 7 -5 -3 0 271.021 8.21442 9 -5 -3 0 259.337 8.39446 4 5 3 0 264.319 6.82003 10 5 3 0 277.755 8.28053 9 5 3 0 251.409 8.08382 4 5 3 0 269.058 6.72854 2 5 3 0 271.059 6.85440 10 5 3 0 266.514 7.26043 3 5 3 0 271.375 8.14229 7 5 3 0 269.591 9.03622 6 5 3 0 275.297 6.46325 2 -6 -3 0 293.831 7.78136 10 -6 -3 0 296.097 9.45836 7 -6 -3 0 293.971 9.35150 9 6 3 0 307.741 7.82261 2 6 3 0 286.902 7.41605 2 6 3 0 299.036 7.91994 10 6 3 0 305.798 7.89858 10 6 3 0 297.460 9.15124 4 6 3 0 313.437 9.55993 9 6 3 0 286.364 7.83645 3 -7 -3 0 159.159 6.80837 9 -7 -3 0 165.548 5.38969 10 -7 -3 0 161.643 6.91031 4 -7 -3 0 162.945 5.16570 10 -7 -3 0 148.227 6.55946 7 7 3 0 157.973 5.46050 10 7 3 0 157.896 7.39813 6 7 3 0 162.014 5.13617 2 7 3 0 171.819 6.55532 4 7 3 0 166.026 5.40966 10 7 3 0 169.282 5.16498 3 7 3 0 171.451 7.01821 9 7 3 0 167.668 5.44317 2 -8 -3 0 3.08202 1.52644 9 -8 -3 0 3.94344 1.08191 10 -8 -3 0 3.92513 1.58258 4 -8 -3 0 1.88392 1.44136 7 -8 -3 0 3.86448 1.16915 10 8 3 0 3.79733 1.26579 2 8 3 0 2.55098 1.57350 9 8 3 0 3.44963 1.23735 10 8 3 0 1.95188 1.09390 4 8 3 0 3.19566 0.98441 3 8 3 0 3.44674 1.19728 10 8 3 0 3.24477 1.25008 2 8 3 0 7.58134 2.26619 6 -9 -3 0 154.354 7.15017 7 -9 -3 0 142.678 5.68669 10 -9 -3 0 147.207 7.42795 4 -9 -3 0 150.175 7.48277 9 -9 -3 0 147.700 5.44354 10 9 3 0 147.828 5.69228 2 9 3 0 148.152 5.78872 10 9 3 0 157.014 5.97226 2 9 3 0 141.048 5.83760 8 9 3 0 153.946 7.61711 9 9 3 0 150.384 6.06172 10 9 3 0 149.837 4.55392 3 -10 -3 0 200.198 9.18987 4 -10 -3 0 183.058 7.96818 10 -10 -3 0 204.110 8.76392 7 -10 -3 0 195.064 6.84012 10 10 3 0 191.123 9.17261 9 10 3 0 187.770 7.24545 8 10 3 0 203.478 7.29072 2 10 3 0 202.892 7.70867 10 10 3 0 189.944 7.21159 10 10 3 0 202.623 7.40587 2 -11 -3 0 449.503 15.1545 7 -11 -3 0 465.863 12.8967 10 -11 -3 0 446.010 15.8573 4 11 3 0 441.535 13.8841 10 11 3 0 481.811 13.6414 10 11 3 0 466.968 16.2380 9 11 3 0 456.985 13.6661 2 11 3 0 470.940 13.5090 2 -12 -3 0 39.9567 4.42115 7 -12 -3 0 47.1377 5.34240 4 -12 -3 0 42.4555 3.31732 10 12 3 0 41.4796 3.99484 10 12 3 0 33.0991 4.44969 9 12 3 0 36.7647 3.83142 2 12 3 0 44.0847 4.00921 10 -13 -3 0 21.5123 4.32245 4 -13 -3 0 16.9526 4.29430 7 -13 -3 0 20.5126 2.81216 10 13 3 0 18.8446 4.25577 2 13 3 0 17.8458 3.16992 10 13 3 0 18.2755 4.04339 9 -14 -3 0 9.27738 2.81694 7 14 3 0 8.54645 2.89649 2 14 3 0 3.75543 2.26063 10 14 3 0 10.0128 3.45737 9 13 -4 0 0.72851 3.88124 9 13 -4 0 1.03573 2.45756 10 13 -4 0 4.09017 4.66724 2 -13 4 0 -0.3939 1.85110 10 -13 4 0 -2.3478 1.56264 2 -13 4 0 2.32989 2.33963 4 -13 4 0 -0.5335 1.56425 7 12 -4 0 5.24847 2.92928 9 12 -4 0 4.32330 2.77926 2 12 -4 0 0.26548 2.12057 10 -12 4 0 1.40964 2.05274 10 -12 4 0 6.49455 2.34599 4 -12 4 0 2.53669 1.79458 7 -12 4 0 3.96603 1.91938 2 11 -4 0 73.8882 6.49638 9 11 -4 0 66.6933 2.24423 3 11 -4 0 63.1073 5.70080 2 11 -4 0 73.7521 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6.14597 2 7 -4 0 141.385 6.86008 9 7 -4 0 130.386 6.76262 10 7 -4 0 127.278 6.42076 10 -7 4 0 130.340 6.60952 10 -7 4 0 129.282 6.61904 9 -7 4 0 133.659 6.47605 10 -7 4 0 136.368 5.64259 8 -7 4 0 127.646 6.01188 2 -7 4 0 135.590 5.88647 2 -7 4 0 140.483 6.00048 4 6 -4 0 125.410 6.29812 10 6 -4 0 123.814 5.77053 2 6 -4 0 138.198 5.82526 8 6 -4 0 133.661 5.98996 2 6 -4 0 125.067 6.02840 10 6 -4 0 127.292 5.10182 6 6 -4 0 124.182 4.97134 3 6 -4 0 128.352 6.10457 9 -6 4 0 140.523 5.77263 2 -6 4 0 117.989 5.92900 9 -6 4 0 123.871 6.15158 10 -6 4 0 128.241 5.66761 2 -6 4 0 136.434 6.20006 10 -6 4 0 138.310 5.33841 8 5 -4 0 106.295 5.38613 10 5 -4 0 102.194 4.88904 2 5 -4 0 106.117 4.99922 2 5 -4 0 104.666 4.86015 8 5 -4 0 101.639 4.36780 3 5 -4 0 103.563 4.09126 6 5 -4 0 111.280 5.98616 9 5 -4 0 95.0370 5.02239 10 -5 4 0 114.668 4.53989 8 -5 4 0 118.134 4.98528 2 -5 4 0 114.373 5.46146 10 -5 4 0 115.285 5.44174 10 -5 4 0 108.977 5.11911 9 -5 4 0 100.761 4.76288 2 4 -4 0 248.315 7.90220 8 4 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130.033 5.58210 5 -4 -8 0 125.573 3.84608 10 4 8 0 127.261 6.51212 8 4 8 0 129.139 6.34412 3 4 8 0 131.328 3.76249 9 4 8 0 134.250 4.76066 2 4 8 0 126.232 5.00333 10 4 8 0 129.385 6.06441 6 4 8 0 120.407 6.13929 4 4 8 0 131.664 4.70371 10 4 8 0 127.652 4.40439 2 4 8 0 120.837 6.58189 7 -5 -8 0 2059.00 46.4415 3 -5 -8 0 2116.29 48.4860 7 5 8 0 2054.08 46.8188 3 5 8 0 2007.73 46.9483 4 5 8 0 2085.16 48.0436 7 5 8 0 2072.36 47.5295 8 5 8 0 2101.25 43.5421 9 5 8 0 2034.25 45.2907 5 5 8 0 2099.77 47.1594 6 5 8 0 2037.31 43.0982 10 5 8 0 2067.62 43.6396 2 5 8 0 2081.00 43.5504 10 -6 -8 0 1.27249 1.75121 7 -6 -8 0 1.76767 1.45202 3 6 8 0 0.64504 1.49173 7 6 8 0 1.75028 0.95672 2 6 8 0 1.78659 0.75533 10 6 8 0 0.85934 1.35657 4 6 8 0 2.64119 1.47584 5 6 8 0 0.64966 1.00872 9 6 8 0 -0.2014 1.30711 3 6 8 0 0.97506 1.47390 6 6 8 0 0.05290 1.24066 8 6 8 0 0.45817 0.79125 10 6 8 0 1.93016 0.88319 2 -7 -8 0 144.292 6.36556 3 -7 -8 0 133.548 7.73145 7 7 8 0 139.406 4.51449 10 7 8 0 136.969 6.31974 5 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2.98958 2.03495 2 -7 10 -3 3.19169 2.27197 10 -7 10 -3 2.94271 1.97226 8 -7 10 -3 1.08295 1.54855 7 -7 10 -3 8.63693 2.90644 2 7 -10 3 10.2577 3.09903 3 7 -10 3 1.49578 2.01122 2 7 -10 3 3.51622 2.18920 10 7 -10 3 3.24664 1.90901 9 -8 10 -3 7.21227 2.93773 10 -8 10 -3 8.62034 3.03807 2 -8 10 -3 9.40423 2.57686 8 8 -10 3 3.24566 2.64293 10 8 -10 3 10.2775 3.09014 2 8 -10 3 5.48769 2.33462 9 8 -10 3 5.74996 2.70111 3 -9 10 -3 18.6019 5.85694 2 -9 10 -3 7.68593 3.25659 10 -9 10 -3 6.82734 2.34928 8 9 -10 3 9.52507 2.88199 9 9 -10 3 8.81155 3.06409 10 9 -10 3 15.6686 3.38448 3 9 -10 3 18.4471 3.90116 2 -10 10 -3 233.377 10.4158 8 -10 10 -3 230.033 11.1192 4 -10 10 -3 227.913 12.0245 10 -10 10 -3 235.156 11.1424 2 10 -10 3 227.848 11.1508 9 10 -10 3 247.333 12.0023 2 10 -10 3 231.836 10.5149 3 10 -10 3 236.434 12.4375 10 12 9 -3 31.6900 4.17244 9 12 9 -3 24.6627 2.95639 10 12 9 -3 35.0009 3.13425 10 12 9 -3 29.7956 3.67585 2 -12 -9 3 31.7713 6.01839 7 11 9 -3 120.911 6.99363 9 11 9 -3 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14.1583 10 0 -6 3 565.210 14.6641 7 0 -6 3 553.616 13.2692 2 0 -6 3 559.458 13.5057 2 0 -6 3 553.051 16.2928 3 -1 6 -3 0.36564 0.94408 10 -1 6 -3 0.42754 0.98151 10 -1 6 -3 0.45123 1.10282 2 -1 6 -3 1.84972 1.13629 8 -1 6 -3 0.00361 0.85746 2 -1 6 -3 -0.0932 0.77588 7 1 -6 3 0.52387 0.83032 8 1 -6 3 -0.5888 0.78914 10 1 -6 3 0.35410 0.85222 10 1 -6 3 1.69195 1.21900 3 1 -6 3 0.23653 0.45370 9 1 -6 3 0.84838 0.93027 2 1 -6 3 0.07729 0.97639 2 -2 6 -3 617.046 16.0918 2 -2 6 -3 618.288 13.7830 6 -2 6 -3 614.446 16.1112 8 -2 6 -3 618.343 16.5072 10 -2 6 -3 610.759 15.6519 2 -2 6 -3 613.199 16.4034 10 -2 6 -3 609.667 15.8417 7 2 -6 3 596.217 15.7821 2 2 -6 3 596.430 16.2483 10 2 -6 3 607.615 16.4714 10 2 -6 3 614.668 16.5237 8 2 -6 3 615.400 16.4237 3 2 -6 3 607.344 14.2764 9 -3 6 -3 1107.62 25.6723 7 -3 6 -3 1096.25 25.8539 2 -3 6 -3 1088.93 23.6861 6 -3 6 -3 1085.47 26.7130 10 -3 6 -3 1135.46 26.2842 2 -3 6 -3 1123.47 26.0121 8 -3 6 -3 1097.28 26.7308 10 3 -6 3 1087.27 25.7268 2 3 -6 3 1099.39 26.2232 2 3 -6 3 1060.37 26.7304 10 3 -6 3 1091.72 26.6041 10 3 -6 3 1111.37 24.8216 9 3 -6 3 1087.09 26.3798 3 3 -6 3 1055.23 26.4829 8 -4 6 -3 165.376 6.29272 7 -4 6 -3 165.669 7.27423 10 -4 6 -3 170.449 6.96491 2 -4 6 -3 170.011 6.74323 2 -4 6 -3 179.780 5.47477 6 -4 6 -3 170.053 6.55551 8 -4 6 -3 166.102 7.36716 10 4 -6 3 169.651 7.48608 10 4 -6 3 175.078 7.11228 3 4 -6 3 161.581 6.23876 9 4 -6 3 173.495 6.86530 2 4 -6 3 169.283 7.31761 10 4 -6 3 163.787 6.93206 2 4 -6 3 156.475 6.93602 8 -5 6 -3 60.3953 4.06182 2 -5 6 -3 59.3685 4.58961 10 -5 6 -3 64.4521 3.96079 8 -5 6 -3 52.4987 3.78943 9 -5 6 -3 58.3928 4.21728 2 -5 6 -3 62.0261 3.25129 6 -5 6 -3 58.9002 4.52435 10 5 -6 3 62.4322 4.43615 2 5 -6 3 53.8362 4.54300 10 5 -6 3 65.2259 4.34864 3 5 -6 3 59.3056 3.96578 9 5 -6 3 54.3074 4.09420 2 5 -6 3 67.7111 4.77004 10 5 -6 3 57.8096 4.22269 8 -6 6 -3 78.4806 5.41406 10 -6 6 -3 80.0103 5.38875 10 -6 6 -3 79.8690 5.02746 2 -6 6 -3 77.8640 4.46047 8 -6 6 -3 73.3224 6.10396 2 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35.0340 3.82163 10 12 5 -3 36.6613 5.08202 9 12 5 -3 33.1908 3.59980 10 12 5 -3 40.6347 3.91778 2 -12 -5 3 32.0909 5.12064 4 -12 -5 3 34.9214 3.12718 10 -12 -5 3 34.5804 5.44121 7 11 5 -3 33.9560 4.17766 5 11 5 -3 39.5689 3.28896 2 11 5 -3 35.2053 3.57465 10 11 5 -3 27.5281 4.17669 9 11 5 -3 32.8046 3.45963 10 11 5 -3 30.3898 3.23275 2 -11 -5 3 35.7852 3.00929 10 -11 -5 3 26.1478 4.17163 4 -11 -5 3 26.6808 6.30477 7 10 5 -3 47.0974 4.62851 9 10 5 -3 48.2965 3.66281 10 10 5 -3 43.7873 4.04504 5 10 5 -3 51.4352 3.67890 10 10 5 -3 48.7407 3.36861 2 10 5 -3 46.9508 3.65225 2 -10 -5 3 51.8057 4.97721 7 -10 -5 3 45.4242 3.16967 10 -10 -5 3 42.2158 3.01229 10 9 5 -3 4.63466 1.50586 2 9 5 -3 5.61425 1.94248 5 9 5 -3 6.79548 2.08785 9 9 5 -3 7.69178 1.82639 10 9 5 -3 4.10651 1.59676 2 9 5 -3 7.60501 1.72409 10 -9 -5 3 4.99907 1.42003 10 -9 -5 3 5.85533 2.50267 7 -9 -5 3 5.98071 2.35220 4 -9 -5 3 6.72060 2.10315 9 -9 -5 3 6.81054 1.59492 10 8 5 -3 59.9579 3.40363 10 8 5 -3 61.8238 4.19012 5 8 5 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5 5 -3 615.612 14.9962 9 5 5 -3 587.636 16.1295 4 5 5 -3 618.468 13.9458 2 5 5 -3 597.152 16.2514 7 5 5 -3 591.510 17.6798 10 5 5 -3 609.711 14.3898 10 5 5 -3 596.919 14.5366 5 5 5 -3 594.119 14.4063 2 -5 -5 3 618.117 15.1461 3 -5 -5 3 616.612 14.1491 10 -5 -5 3 602.761 14.9836 9 -5 -5 3 593.965 14.3766 10 4 5 -3 87.0179 3.32307 5 4 5 -3 89.0479 3.22671 2 4 5 -3 92.3853 3.58142 10 4 5 -3 88.8192 3.57841 2 4 5 -3 86.4401 4.44169 4 4 5 -3 88.7745 3.79450 10 4 5 -3 94.7752 3.60016 9 4 5 -3 87.6131 4.56698 7 -4 -5 3 84.2258 4.04953 3 -4 -5 3 88.9186 3.52653 9 -4 -5 3 86.7783 3.54228 10 -4 -5 3 87.8023 4.07517 10 3 5 -3 121.909 3.80811 9 3 5 -3 119.778 5.38784 8 3 5 -3 123.996 4.32415 10 3 5 -3 113.968 5.19763 7 3 5 -3 125.845 4.61255 10 3 5 -3 121.674 3.99512 2 3 5 -3 122.866 3.69864 5 3 5 -3 125.344 5.28217 4 3 5 -3 129.146 4.40949 2 -3 -5 3 120.593 3.36609 2 -3 -5 3 111.855 4.21752 10 -3 -5 3 120.848 3.77795 9 -3 -5 3 122.962 5.01761 3 -3 -5 3 121.459 4.20339 10 -3 -5 3 124.204 5.62137 7 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8.36252 8 6 -3 -3 255.153 6.72530 3 6 -3 -3 260.578 8.81346 2 6 -3 -3 268.778 9.53576 9 6 -3 -3 266.175 9.35793 10 6 -3 -3 264.130 8.67005 6 6 -3 -3 254.956 8.66529 2 -6 3 3 240.135 8.47175 2 -6 3 3 262.257 8.35248 2 -6 3 3 255.370 9.15283 10 -6 3 3 254.719 9.34739 9 -6 3 3 266.336 8.25875 8 -6 3 3 263.263 8.99362 10 -6 3 3 267.444 8.28091 4 5 -3 -3 65.0015 3.56183 6 5 -3 -3 70.3323 3.98321 10 5 -3 -3 69.9094 4.13783 10 5 -3 -3 73.3326 4.21911 9 5 -3 -3 67.4195 3.74698 2 5 -3 -3 68.8277 3.85315 2 5 -3 -3 66.9197 3.54886 8 5 -3 -3 68.2614 2.78367 3 -5 3 3 70.6202 3.42664 4 -5 3 3 67.9945 3.88287 10 -5 3 3 66.9777 3.99042 10 -5 3 3 66.8591 3.41344 8 -5 3 3 67.0752 4.03117 9 -5 3 3 73.9128 3.71333 2 -5 3 3 63.1702 3.65141 2 4 -3 -3 41.4257 2.17032 3 4 -3 -3 43.1584 2.63960 8 4 -3 -3 34.9318 2.61533 2 4 -3 -3 42.6100 2.82597 2 4 -3 -3 35.9030 2.80931 9 4 -3 -3 37.5248 2.75699 10 -4 3 3 38.7705 2.16829 3 -4 3 3 37.1393 2.72067 10 -4 3 3 41.5754 2.48470 8 -4 3 3 39.0415 2.73222 2 -4 3 3 42.2253 2.70717 2 3 -3 -3 73.9191 3.65584 10 3 -3 -3 80.8260 3.09516 3 3 -3 -3 82.0468 3.56257 2 3 -3 -3 78.8240 3.76201 9 3 -3 -3 81.0343 3.67773 10 3 -3 -3 71.1386 3.39751 2 3 -3 -3 72.8973 3.34106 8 -3 3 3 75.3010 3.62766 9 -3 3 3 80.0674 3.25695 8 -3 3 3 71.8344 3.08411 3 -3 3 3 77.5705 3.64584 10 -3 3 3 76.4686 3.51077 2 -3 3 3 78.7746 3.43414 2 -3 3 3 76.4773 3.68916 10 2 -3 -3 1163.14 25.7158 10 2 -3 -3 1132.09 25.3346 8 2 -3 -3 1152.53 25.6008 9 2 -3 -3 1144.24 25.2529 2 2 -3 -3 1140.13 25.2565 2 2 -3 -3 1169.09 25.1441 3 -2 3 3 1181.85 25.4269 2 -2 3 3 1199.73 25.6952 10 -2 3 3 1156.22 25.6994 10 -2 3 3 1137.38 25.2125 3 -2 3 3 1162.82 25.0348 8 -2 3 3 1161.22 25.5988 9 -2 3 3 1179.25 25.3147 2 1 -3 -3 342.870 9.08324 10 1 -3 -3 375.941 9.21664 3 1 -3 -3 362.325 9.08054 10 1 -3 -3 346.594 8.83317 2 1 -3 -3 360.409 9.14599 8 1 -3 -3 369.062 8.86445 2 1 -3 -3 374.209 9.26942 9 -1 3 3 366.679 8.95839 2 -1 3 3 365.498 8.90737 2 -1 3 3 365.632 9.14649 9 -1 3 3 375.356 9.18460 10 -1 3 3 364.149 8.90242 8 -1 3 3 369.311 9.19177 10 -1 3 3 366.590 9.29343 3 0 -3 -3 632.142 14.6343 8 0 -3 -3 642.236 14.2423 10 0 -3 -3 636.330 14.3576 10 0 -3 -3 618.282 14.0082 2 0 -3 -3 651.624 15.2059 5 0 -3 -3 667.267 14.9171 3 0 -3 -3 648.562 13.9784 2 0 -3 -3 626.899 13.9781 6 0 3 3 654.938 14.3879 10 0 3 3 659.248 14.3421 10 0 3 3 659.070 14.1551 2 0 3 3 650.877 14.4970 8 0 3 3 654.446 15.0139 3 0 3 3 660.739 14.5994 9 0 3 3 629.331 14.1233 2 -1 -3 -3 1995.76 42.7865 8 -1 -3 -3 2095.86 43.2027 3 -1 -3 -3 2021.16 42.0601 10 -1 -3 -3 2051.35 42.8156 6 -1 -3 -3 2034.14 43.5015 5 1 3 3 2100.32 43.4921 5 1 3 3 2087.84 42.7650 8 1 3 3 2035.66 42.0499 10 1 3 3 2061.91 42.6874 4 1 3 3 2144.26 41.9144 2 1 3 3 2057.58 42.7018 6 1 3 3 2016.00 43.2747 3 1 3 3 2061.63 41.9036 2 1 3 3 2093.94 42.1172 10 -2 -3 -3 159.380 4.88890 4 -2 -3 -3 165.521 5.41897 5 -2 -3 -3 161.065 4.97195 3 -2 -3 -3 163.501 5.25329 6 2 3 3 159.902 5.29851 7 2 3 3 157.743 5.09612 6 2 3 3 163.870 3.71004 10 2 3 3 163.496 4.72975 8 2 3 3 158.969 4.78592 4 2 3 3 160.642 5.09337 3 2 3 3 153.545 5.22116 5 2 3 3 166.563 3.70619 10 -3 -3 -3 1848.19 38.4991 3 -3 -3 -3 1842.65 38.8310 4 -3 -3 -3 1820.92 39.0663 7 -3 -3 -3 1804.45 39.3406 5 -3 -3 -3 1798.98 39.5150 6 3 3 3 1840.82 38.6384 4 3 3 3 1857.26 39.4048 6 3 3 3 1872.80 38.7793 3 3 3 3 1743.52 39.0016 7 3 3 3 1810.44 39.2684 5 -4 -3 -3 923.827 21.6445 6 -4 -3 -3 896.241 20.6992 7 -4 -3 -3 885.749 20.6049 4 4 3 3 903.279 18.3961 10 4 3 3 877.342 20.6700 9 4 3 3 885.089 18.4968 10 4 3 3 874.825 20.3119 4 4 3 3 889.593 20.5323 7 4 3 3 880.760 20.1087 3 4 3 3 889.036 21.0106 5 4 3 3 884.165 21.2933 6 -5 -3 -3 28.1165 2.44765 4 -5 -3 -3 25.4031 2.26998 7 5 3 3 26.5312 1.37237 10 5 3 3 24.5808 1.18169 2 5 3 3 26.8600 2.42396 9 5 3 3 25.7408 1.24224 2 5 3 3 28.5212 2.22012 7 5 3 3 25.5203 1.44169 10 5 3 3 26.3490 2.64008 6 5 3 3 26.3949 2.99255 5 5 3 3 27.9568 2.03657 3 -6 -3 -3 136.222 3.83258 10 -6 -3 -3 145.855 5.69583 7 -6 -3 -3 143.944 5.96517 4 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4.12837 10 2 -6 -5 80.4268 4.58260 2 2 -6 -5 78.6430 4.18502 3 2 -6 -5 78.4366 4.36403 8 -2 6 5 79.4429 4.37695 3 -2 6 5 74.1955 4.05780 10 -2 6 5 74.5938 4.17778 10 -2 6 5 82.4375 4.08460 2 -2 6 5 83.2969 4.05228 2 -2 6 5 76.4574 3.87097 8 1 -6 -5 423.079 11.1545 2 1 -6 -5 421.907 11.7678 10 1 -6 -5 432.341 11.5049 10 1 -6 -5 438.889 10.9335 2 1 -6 -5 432.573 12.8618 5 1 -6 -5 442.974 12.2208 3 1 -6 -5 425.451 9.89983 6 1 -6 -5 411.289 12.1347 8 -1 6 5 438.313 11.9442 10 -1 6 5 406.453 12.2392 3 -1 6 5 418.898 11.4362 9 -1 6 5 451.624 11.7792 10 -1 6 5 435.796 11.4111 2 -1 6 5 436.151 11.4822 2 0 -6 -5 26.7763 2.59259 3 0 -6 -5 26.1126 1.77670 6 0 -6 -5 28.5370 1.74688 2 0 -6 -5 26.1008 2.21436 10 0 -6 -5 23.7038 2.37961 8 0 -6 -5 24.4387 2.76850 5 0 -6 -5 24.4049 1.74848 2 0 6 5 25.5367 2.12339 9 0 6 5 26.3308 2.03769 2 0 6 5 26.8323 2.69350 3 0 6 5 30.3063 2.70242 10 0 6 5 27.8047 2.30318 8 0 6 5 29.2999 2.25693 10 0 6 5 28.1606 2.15980 2 -1 -6 -5 777.535 17.8346 6 -1 -6 -5 725.637 21.2784 5 -1 -6 -5 762.947 18.7985 8 -1 -6 -5 762.923 19.0392 3 -1 -6 -5 745.252 17.1859 10 1 6 5 784.378 17.7973 10 1 6 5 746.070 17.3246 2 1 6 5 777.297 18.4175 8 1 6 5 774.338 19.4958 3 1 6 5 748.296 19.2504 5 1 6 5 773.110 17.3473 2 1 6 5 785.859 17.5530 10 1 6 5 764.964 17.4200 6 1 6 5 778.502 18.0481 9 -2 -6 -5 2.94962 0.77243 10 -2 -6 -5 4.24427 1.26248 8 -2 -6 -5 2.66103 0.77296 10 -2 -6 -5 4.38898 1.28874 3 -2 -6 -5 2.99180 1.15733 6 2 6 5 1.85308 0.95995 8 2 6 5 3.06045 0.75016 2 2 6 5 2.89323 1.08052 4 2 6 5 1.20316 1.18292 3 2 6 5 2.29563 1.33386 5 2 6 5 1.61729 0.80133 2 2 6 5 3.76754 1.09364 6 2 6 5 0.93872 1.02227 7 2 6 5 2.24304 0.75521 10 2 6 5 1.87432 0.75677 10 -3 -6 -5 1941.72 43.1208 5 -3 -6 -5 1978.44 42.4033 6 -3 -6 -5 1880.90 42.1602 3 3 6 5 1923.32 41.8516 6 3 6 5 1915.01 39.3959 10 3 6 5 1918.04 43.2791 7 3 6 5 1881.56 39.3980 2 3 6 5 1898.17 42.7621 5 3 6 5 1970.26 41.7642 8 3 6 5 1882.14 39.2957 2 3 6 5 1954.03 43.1265 4 3 6 5 1890.78 39.5842 10 3 6 5 1897.38 42.7625 3 -4 -6 -5 11.6395 1.93337 3 -4 -6 -5 14.5642 2.53930 5 -4 -6 -5 10.6211 1.98254 6 4 6 5 13.1184 2.23769 5 4 6 5 11.2108 1.92576 4 4 6 5 7.74163 1.67365 6 4 6 5 12.7065 2.29663 7 4 6 5 9.61717 1.92291 3 4 6 5 10.2668 1.76963 8 -5 -6 -5 40.5593 3.73971 6 -5 -6 -5 43.7071 3.81424 5 5 6 5 44.2463 3.49384 6 5 6 5 43.4005 3.43398 3 5 6 5 43.5099 3.60027 7 5 6 5 39.1195 3.07211 4 5 6 5 42.1085 3.11024 9 5 6 5 45.2023 3.56574 5 5 6 5 42.8649 3.03482 8 -6 -6 -5 28.2807 3.09284 4 6 6 5 29.9926 3.02027 3 6 6 5 27.6708 3.43541 5 6 6 5 29.2948 2.71935 8 6 6 5 29.6010 2.85080 9 6 6 5 35.6053 3.29171 7 6 6 5 30.9935 3.25132 6 6 6 5 24.1517 2.69131 4 -7 -6 -5 34.3841 3.47778 7 -7 -6 -5 32.6049 3.52595 4 7 6 5 31.5859 3.17571 3 7 6 5 31.1900 3.14471 4 7 6 5 29.5964 3.05470 7 7 6 5 24.9355 3.18168 9 7 6 5 31.2855 3.58294 5 7 6 5 30.1835 3.45909 6 7 6 5 29.2167 2.90286 8 -8 -6 -5 109.168 6.34758 4 -8 -6 -5 115.059 6.23575 7 8 6 5 106.987 5.59521 3 8 6 5 104.985 3.36523 2 8 6 5 101.602 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5 5.84760 2.47693 10 -7 7 5 2.28722 1.68643 4 -7 7 5 3.50892 2.01736 9 -7 7 5 3.73322 2.55197 2 6 -7 -5 1177.68 29.5239 10 6 -7 -5 1133.41 25.0264 6 6 -7 -5 1177.50 28.7791 2 6 -7 -5 1135.38 29.3315 9 6 -7 -5 1133.95 27.2028 3 -6 7 5 1223.62 28.1228 8 -6 7 5 1148.20 28.5217 2 -6 7 5 1184.24 29.5745 10 -6 7 5 1075.71 29.3316 9 -6 7 5 1130.75 30.0760 10 5 -7 -5 7.32507 2.25962 9 5 -7 -5 9.15207 2.09606 10 5 -7 -5 8.68849 2.22484 8 5 -7 -5 13.9516 2.32115 3 5 -7 -5 9.22022 2.31446 2 5 -7 -5 11.9967 2.95896 2 -5 7 5 11.4093 2.38797 9 -5 7 5 10.2785 2.15178 8 -5 7 5 17.9270 3.16952 10 -5 7 5 13.0006 2.58134 2 -5 7 5 9.40467 2.38984 10 4 -7 -5 39.8899 3.28835 3 4 -7 -5 36.7069 3.55419 9 4 -7 -5 37.9176 3.45949 2 4 -7 -5 27.0973 3.60382 8 4 -7 -5 34.8684 3.29204 2 -4 7 5 32.0504 3.08178 8 -4 7 5 35.4415 3.39253 9 -4 7 5 38.9487 3.87740 10 -4 7 5 36.3765 3.46944 2 -4 7 5 36.1969 3.41123 3 -4 7 5 39.8952 3.67900 10 3 -7 -5 1126.20 26.2834 2 3 -7 -5 1132.33 28.4274 5 3 -7 -5 1092.17 26.5935 2 3 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2457.05 51.1589 2 -2 4 6 2460.85 51.8080 10 -2 4 6 2416.50 51.4502 3 -2 4 6 2388.72 52.0560 9 -2 4 6 2350.30 52.8229 10 1 -4 -6 1846.79 41.2712 10 1 -4 -6 1935.61 40.8301 8 1 -4 -6 1926.55 40.8160 3 1 -4 -6 1873.11 42.0013 5 1 -4 -6 1901.90 40.4138 2 1 -4 -6 1864.32 40.2914 2 1 -4 -6 1908.62 40.7951 10 -1 4 6 1914.61 41.3896 9 -1 4 6 1882.79 41.1907 3 -1 4 6 1947.71 40.9264 10 -1 4 6 1942.73 41.0143 10 -1 4 6 1920.26 40.1713 8 -1 4 6 1895.41 40.6259 2 -1 4 6 1943.58 40.5066 2 0 -4 -6 1950.31 41.8385 2 0 -4 -6 2024.31 44.0735 5 0 -4 -6 1942.73 42.3940 10 0 -4 -6 1976.71 42.3821 10 0 -4 -6 2019.16 41.9604 2 0 -4 -6 2056.36 43.0573 3 0 -4 -6 1993.10 42.6137 8 0 -4 -6 2084.99 42.5262 6 0 4 6 1973.46 42.1176 2 0 4 6 2031.35 42.5561 10 0 4 6 2042.48 43.3396 9 0 4 6 2001.52 43.3258 3 0 4 6 2026.09 42.3470 2 0 4 6 2010.28 42.0576 8 0 4 6 2056.25 42.5685 10 -1 -4 -6 60.1747 2.60773 10 -1 -4 -6 65.4416 2.11597 2 -1 -4 -6 66.3130 3.83178 5 -1 -4 -6 62.7433 2.85755 8 -1 -4 -6 58.6169 2.58978 10 -1 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334.030 12.9974 10 -3 8 -9 350.600 11.0202 6 3 -8 9 353.590 12.7359 8 3 -8 9 373.884 13.4729 10 3 -8 9 354.110 13.0715 3 3 -8 9 353.895 12.1420 2 3 -8 9 358.956 10.6548 9 -4 8 -9 11.8370 2.38470 8 -4 8 -9 18.9271 3.62402 10 -4 8 -9 14.2332 2.43861 6 -4 8 -9 13.9603 2.95679 10 -4 8 -9 17.0196 2.49599 7 -4 8 -9 10.2936 2.92884 2 4 -8 9 17.1437 3.20695 2 4 -8 9 15.8839 3.35421 10 4 -8 9 11.9482 3.15429 3 4 -8 9 15.1198 3.00409 8 4 -8 9 16.5036 2.46744 9 -5 8 -9 87.2221 6.48803 10 -5 8 -9 75.3291 4.02827 7 -5 8 -9 74.5198 4.98194 8 -5 8 -9 81.0980 4.82588 6 5 -8 9 76.0588 4.92467 9 5 -8 9 75.2020 5.72820 2 5 -8 9 76.7129 7.14546 8 5 -8 9 89.5393 6.29191 3 5 -8 9 80.2636 6.27049 10 -6 8 -9 231.650 7.45889 7 -6 8 -9 243.705 9.30052 8 -6 8 -9 243.161 10.5185 2 -6 8 -9 245.171 9.19542 6 -6 8 -9 246.910 13.2960 10 6 -8 9 243.531 10.4159 2 6 -8 9 239.738 12.6126 10 6 -8 9 235.058 10.9449 3 6 -8 9 244.063 9.64086 9 -7 8 -9 19.1648 4.20465 8 -7 8 -9 22.2962 1.99644 7 -7 8 -9 18.2547 3.55540 10 -7 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53.6252 4.15020 9 7 7 -9 38.6074 3.17249 2 7 7 -9 44.0601 4.29470 2 7 7 -9 45.8456 4.02486 10 -7 -7 9 42.9480 3.81015 10 -7 -7 9 45.9596 2.72771 2 -7 -7 9 56.9190 10.7751 7 -7 -7 9 47.6007 2.69965 2 -7 -7 9 42.7181 3.64912 9 -7 -7 9 34.6531 3.44912 3 6 7 -9 57.3834 4.67310 2 6 7 -9 57.3653 4.50855 10 6 7 -9 46.0609 3.43465 2 6 7 -9 48.7493 3.96663 10 6 7 -9 58.2748 4.10647 9 -6 -7 9 57.3019 3.39758 2 -6 -7 9 48.7311 5.07945 7 -6 -7 9 61.0829 4.38996 3 -6 -7 9 54.9478 3.82320 9 -6 -7 9 58.5809 3.48286 2 -6 -7 9 55.7080 4.23166 10 5 7 -9 2020.87 45.5366 10 5 7 -9 1943.90 45.5745 4 5 7 -9 1925.12 44.1453 10 5 7 -9 1944.91 44.8598 2 -5 -7 9 1935.14 42.2384 2 -5 -7 9 2019.34 44.8678 10 -5 -7 9 1976.31 44.8124 3 -5 -7 9 2033.68 42.6660 2 -5 -7 9 1997.20 47.2815 7 -5 -7 9 1819.59 43.6200 10 -5 -7 9 1972.64 43.1441 9 4 7 -9 394.616 11.5177 2 4 7 -9 406.412 14.0657 8 4 7 -9 403.388 13.2524 10 4 7 -9 401.485 12.4531 10 4 7 -9 398.196 12.9301 2 4 7 -9 441.886 16.5647 4 -4 -7 9 416.266 12.8807 10 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5.19921 2.69929 10 2 -7 9 15.8942 2.11091 9 2 -7 9 15.7367 2.90313 8 2 -7 9 14.3848 3.13542 10 -3 7 -9 465.566 15.1534 2 -3 7 -9 487.551 13.7808 6 -3 7 -9 474.644 14.3928 8 -3 7 -9 477.387 15.3109 10 -3 7 -9 482.245 13.1000 7 -3 7 -9 496.374 15.9528 10 3 -7 9 459.424 16.3717 2 3 -7 9 484.691 15.7099 10 3 -7 9 496.883 14.7193 2 3 -7 9 478.925 14.9814 8 3 -7 9 491.875 15.7407 10 3 -7 9 481.030 13.3960 9 -4 7 -9 91.1684 5.03699 6 -4 7 -9 107.096 6.46318 2 -4 7 -9 101.474 5.54467 8 -4 7 -9 90.7789 6.30094 10 -4 7 -9 100.670 4.37165 7 -4 7 -9 97.1841 6.25819 10 4 -7 9 98.9399 6.35606 10 4 -7 9 100.498 5.90678 2 4 -7 9 95.7124 5.82747 8 4 -7 9 95.1576 5.85264 2 4 -7 9 100.873 5.21729 9 4 -7 9 106.374 6.63568 10 -5 7 -9 52.3479 3.99714 8 -5 7 -9 46.5210 3.81558 6 -5 7 -9 44.4148 4.78425 10 -5 7 -9 43.7740 4.38131 2 -5 7 -9 49.9136 2.85926 7 -5 7 -9 41.5235 4.36846 10 5 -7 9 41.9817 4.47200 10 5 -7 9 42.6799 4.11735 8 5 -7 9 40.9690 4.12519 2 5 -7 9 50.9000 4.94754 10 5 -7 9 50.4361 4.03991 9 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13.6656 3.51474 9 -11 7 -9 27.7175 4.19720 2 -11 7 -9 15.5670 3.55205 10 -11 7 -9 9.48654 3.09746 4 -11 7 -9 18.7722 3.22791 8 11 -7 9 15.2465 3.37710 3 11 -7 9 19.5001 4.31778 2 11 -7 9 18.5108 4.07176 9 11 -7 9 17.5117 4.28611 10 12 6 -9 247.045 12.2762 9 12 6 -9 286.543 11.8099 10 12 6 -9 260.142 11.5757 2 -12 -6 9 271.455 17.0197 7 -12 -6 9 267.769 10.6372 10 11 6 -9 132.464 7.57150 2 11 6 -9 135.591 7.16209 10 11 6 -9 129.799 6.56346 5 11 6 -9 150.482 8.71568 9 11 6 -9 138.713 7.83689 10 -11 -6 9 133.250 9.29111 7 -11 -6 9 130.899 7.06715 10 10 6 -9 128.571 6.30448 5 10 6 -9 145.070 7.75972 2 10 6 -9 131.319 7.18139 10 10 6 -9 134.192 9.85907 9 10 6 -9 140.188 7.71800 10 -10 -6 9 134.363 4.05301 3 -10 -6 9 151.809 7.34690 10 -10 -6 9 123.403 8.78720 7 9 6 -9 312.614 11.6751 10 9 6 -9 281.703 10.6223 10 9 6 -9 320.584 12.0444 9 9 6 -9 298.418 9.54438 5 9 6 -9 295.311 11.3384 2 -9 -6 9 310.094 11.0378 10 -9 -6 9 304.030 8.70821 3 -9 -6 9 297.809 8.15417 2 -9 -6 9 305.363 8.16774 2 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34.1190 10 5 6 -9 1465.31 33.0178 2 5 6 -9 1498.16 33.9170 9 -5 -6 9 1479.56 32.6997 2 -5 -6 9 1453.41 33.5094 9 -5 -6 9 1419.82 32.4640 2 -5 -6 9 1502.24 34.2468 3 -5 -6 9 1399.52 33.7150 10 -5 -6 9 1477.32 36.5998 7 -5 -6 9 1486.71 34.5285 10 4 6 -9 2.30414 1.21579 2 4 6 -9 0.82970 1.54084 2 4 6 -9 0.35057 1.19682 10 4 6 -9 -0.4875 1.25746 10 4 6 -9 0.78089 1.34298 4 -4 -6 9 3.78747 1.72512 7 -4 -6 9 2.25169 1.16313 2 -4 -6 9 1.46925 1.31690 10 -4 -6 9 0.39103 0.95576 10 -4 -6 9 1.91656 1.50433 3 -4 -6 9 1.31042 1.12560 2 -4 -6 9 -0.5901 0.86729 9 3 6 -9 1036.83 26.2103 8 3 6 -9 973.357 25.4098 10 3 6 -9 1026.93 25.2516 2 3 6 -9 957.070 25.0599 4 3 6 -9 1003.39 23.6130 2 3 6 -9 997.556 24.7005 10 -3 -6 9 1003.85 23.3079 9 -3 -6 9 1016.31 25.0649 3 -3 -6 9 1012.27 26.1624 7 -3 -6 9 1029.12 23.7621 2 -3 -6 9 1031.82 25.2283 10 -3 -6 9 1027.25 24.7021 10 -3 -6 9 993.406 23.6636 2 2 6 -9 163.429 7.35435 10 2 6 -9 164.031 7.46238 8 2 6 -9 165.040 7.23808 2 2 6 -9 159.781 6.09842 2 2 6 -9 156.651 6.71759 10 -2 -6 9 161.244 5.67907 9 -2 -6 9 163.346 6.78909 10 -2 -6 9 165.316 6.31153 2 -2 -6 9 162.053 7.05763 10 -2 -6 9 158.426 6.21586 2 -2 -6 9 179.035 7.63657 7 1 6 -9 347.850 11.7772 10 1 6 -9 362.454 11.7998 8 1 6 -9 344.510 10.2543 2 1 6 -9 358.248 11.2880 10 1 6 -9 347.452 10.6656 7 1 6 -9 337.387 11.3943 2 -1 -6 9 348.452 9.57549 9 -1 -6 9 342.996 11.3968 10 -1 -6 9 338.611 10.4103 2 -1 -6 9 361.341 11.5123 7 -1 -6 9 346.273 10.5918 2 -1 -6 9 347.454 11.2068 10 0 6 -9 112.086 5.69940 10 0 6 -9 112.029 5.10662 7 0 6 -9 119.407 6.32510 10 0 6 -9 112.376 5.08065 2 0 6 -9 119.349 6.09978 2 0 6 -9 123.737 6.10365 8 0 -6 9 121.169 5.46964 2 0 -6 9 115.484 5.52403 2 0 -6 9 134.096 5.95317 7 0 -6 9 112.459 3.15813 5 0 -6 9 121.508 6.13284 10 0 -6 9 121.800 5.94168 10 0 -6 9 113.053 4.64479 9 -1 6 -9 765.337 20.8900 10 -1 6 -9 740.747 19.0228 2 -1 6 -9 765.129 18.7026 7 -1 6 -9 758.948 20.0922 8 -1 6 -9 753.325 20.2522 10 -1 6 -9 795.927 20.6364 2 1 -6 9 773.145 20.6683 10 1 -6 9 774.792 19.5478 2 1 -6 9 768.724 19.3776 7 1 -6 9 740.336 17.3124 5 1 -6 9 785.501 19.8795 2 1 -6 9 722.756 20.2250 10 -2 6 -9 301.592 10.8218 2 -2 6 -9 322.750 9.12542 7 -2 6 -9 295.520 11.1082 10 -2 6 -9 293.240 10.6243 10 -2 6 -9 313.160 10.3127 8 -2 6 -9 300.384 9.77491 2 -2 6 -9 316.004 9.88525 6 2 -6 9 310.967 10.1626 2 2 -6 9 292.019 10.7510 10 2 -6 9 302.540 11.0367 10 2 -6 9 302.585 9.32437 7 2 -6 9 302.704 10.4212 2 2 -6 9 317.765 9.43573 9 2 -6 9 290.750 10.2103 8 -3 6 -9 152.228 7.30288 10 -3 6 -9 164.368 6.66254 6 -3 6 -9 151.122 6.50128 2 -3 6 -9 159.415 5.57676 7 -3 6 -9 163.682 7.88603 10 -3 6 -9 157.314 7.42631 2 -3 6 -9 163.917 6.80623 8 3 -6 9 173.763 6.62981 9 3 -6 9 155.806 7.18006 2 3 -6 9 161.474 7.12947 8 3 -6 9 163.647 7.05936 2 3 -6 9 158.911 7.65708 10 -4 6 -9 6.36504 2.31745 2 -4 6 -9 3.38664 1.54241 6 -4 6 -9 2.53183 1.41613 10 -4 6 -9 6.30873 2.13202 10 -4 6 -9 4.73304 1.60761 8 -4 6 -9 4.84029 1.15623 7 -4 6 -9 5.25654 1.99278 2 4 -6 9 2.65800 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38.3542 4.99760 2 8 -6 9 34.1900 4.16232 8 8 -6 9 37.7038 4.93083 9 8 -6 9 45.4004 5.74723 10 -9 6 -9 32.0096 4.62176 10 -9 6 -9 29.2005 4.08313 6 -9 6 -9 32.6654 4.11792 2 -9 6 -9 32.4329 3.41102 8 9 -6 9 29.6808 4.50692 2 9 -6 9 31.9043 4.71964 9 9 -6 9 34.2705 4.87223 10 -10 6 -9 3.15890 1.59581 8 -10 6 -9 2.53998 1.96222 4 -10 6 -9 1.59740 2.49471 10 -10 6 -9 2.91430 2.29359 6 -10 6 -9 0.55337 1.96135 2 10 -6 9 1.12310 2.07205 9 10 -6 9 -0.0466 2.05706 2 10 -6 9 6.10042 3.16570 10 -11 6 -9 9.87692 3.22576 10 -11 6 -9 6.22127 1.99372 8 -11 6 -9 10.6203 2.78480 2 -11 6 -9 4.64055 2.53231 4 11 -6 9 11.8180 3.38302 10 11 -6 9 3.24362 2.66881 9 11 -6 9 6.02483 2.55171 3 11 -6 9 0.54905 2.67108 2 -12 6 -9 100.256 7.66684 4 -12 6 -9 110.746 7.85425 10 -12 6 -9 101.233 6.52597 2 12 -6 9 106.723 8.25390 10 12 -6 9 94.8087 6.68624 3 12 -6 9 107.503 7.92354 2 13 5 -9 72.6830 9.63174 9 13 5 -9 79.6651 6.56237 2 13 5 -9 83.0960 6.68594 10 -13 -5 9 82.4910 7.83646 7 12 5 -9 152.483 9.48731 9 12 5 -9 147.878 8.39358 2 12 5 -9 144.547 8.38067 10 -12 -5 9 158.949 10.3111 7 -12 -5 9 136.437 7.56059 10 11 5 -9 6.21303 2.40558 10 11 5 -9 11.0568 3.27458 9 11 5 -9 12.2525 2.86593 2 11 5 -9 14.6807 2.60840 10 -11 -5 9 10.0004 2.44755 10 -11 -5 9 10.8162 1.48070 2 -11 -5 9 17.3183 4.40072 7 10 5 -9 2.70298 1.92975 10 10 5 -9 3.64852 2.51205 2 10 5 -9 2.86114 2.39497 9 10 5 -9 6.97263 2.23096 10 -10 -5 9 4.68042 2.37318 7 9 5 -9 17.1590 3.18790 9 9 5 -9 21.3166 3.46525 10 9 5 -9 12.9681 2.57675 10 9 5 -9 10.2015 2.81380 2 -9 -5 9 16.0420 2.13577 2 -9 -5 9 14.9301 2.71758 10 -9 -5 9 16.3102 2.08432 2 -9 -5 9 11.8752 3.35336 7 -9 -5 9 17.1516 1.52148 3 8 5 -9 68.8542 4.95180 2 8 5 -9 71.9775 5.37448 9 8 5 -9 63.6624 4.65540 10 8 5 -9 63.7582 4.95289 10 8 5 -9 62.2695 4.20141 2 -8 -5 9 75.0472 6.03445 7 -8 -5 9 63.3396 4.86205 9 -8 -5 9 70.1882 4.77191 10 -8 -5 9 61.2101 3.53684 2 -8 -5 9 69.7123 3.64264 2 -8 -5 9 70.6554 3.47090 3 7 5 -9 1.34703 1.22844 4 7 5 -9 0.43044 1.54731 9 7 5 -9 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5 -9 173.084 7.21673 2 4 5 -9 162.761 6.88751 4 4 5 -9 150.429 6.97165 10 -4 -5 9 159.216 6.00482 2 -4 -5 9 166.019 7.64585 7 -4 -5 9 166.106 6.59588 10 -4 -5 9 174.653 6.48943 9 -4 -5 9 169.810 7.00914 10 -4 -5 9 172.858 6.14634 2 3 5 -9 145.977 6.69064 10 3 5 -9 151.333 6.56886 2 3 5 -9 149.186 6.32617 10 3 5 -9 156.087 6.51020 4 3 5 -9 146.756 5.60256 2 -3 -5 9 142.217 6.85288 7 -3 -5 9 155.854 5.77302 9 -3 -5 9 152.906 6.56398 10 -3 -5 9 139.528 6.05217 10 -3 -5 9 140.282 5.65270 2 2 5 -9 18.1093 2.63421 10 2 5 -9 16.7059 2.78306 2 2 5 -9 19.0304 2.27038 2 2 5 -9 15.8568 2.76314 10 2 5 -9 19.3206 2.83600 8 -2 -5 9 16.1028 1.89500 9 -2 -5 9 20.7232 2.93467 10 -2 -5 9 17.3891 2.50966 10 -2 -5 9 16.6299 2.25020 2 -2 -5 9 19.4563 2.34954 2 -2 -5 9 19.6665 2.88421 7 1 5 -9 184.763 7.64520 10 1 5 -9 179.193 6.41280 2 1 5 -9 179.916 7.08257 10 1 5 -9 186.103 7.46824 8 1 5 -9 185.905 7.44077 2 -1 -5 9 190.904 7.47419 7 -1 -5 9 190.240 7.30717 10 -1 -5 9 183.404 6.26940 9 -1 -5 9 187.828 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65.9384 4.51178 10 -3 5 -9 254.210 9.51084 10 -3 5 -9 254.337 7.14973 7 -3 5 -9 280.982 9.82186 2 -3 5 -9 271.803 8.73453 8 -3 5 -9 254.836 8.63443 2 -3 5 -9 266.511 10.0619 10 -3 5 -9 273.547 9.01689 6 3 -5 9 261.049 9.41914 2 3 -5 9 269.898 8.88240 9 3 -5 9 260.869 8.99960 8 3 -5 9 242.839 8.90063 2 3 -5 9 258.173 9.79212 10 3 -5 9 250.928 9.75940 10 -4 5 -9 91.9812 5.34420 2 -4 5 -9 88.2122 4.42399 8 -4 5 -9 84.8945 5.49882 10 -4 5 -9 81.6064 4.47356 2 -4 5 -9 86.8201 4.79841 6 -4 5 -9 76.7003 5.10102 10 4 -5 9 87.4915 5.26352 2 4 -5 9 78.3846 4.61063 8 4 -5 9 91.6309 4.92529 9 4 -5 9 76.9815 5.22965 10 4 -5 9 81.4954 5.36077 10 4 -5 9 88.1241 5.04289 2 -5 5 -9 45.9324 4.10866 2 -5 5 -9 45.9197 3.48543 2 -5 5 -9 44.2501 3.76785 6 -5 5 -9 54.7792 5.25246 10 -5 5 -9 53.1098 4.69365 10 -5 5 -9 49.1880 3.30591 8 5 -5 9 47.7077 4.31605 10 5 -5 9 52.8907 4.60455 10 5 -5 9 43.0886 3.64647 8 5 -5 9 45.6614 4.05297 2 5 -5 9 49.5857 3.96445 9 -6 5 -9 304.157 11.4917 10 -6 5 -9 295.364 10.4745 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79.7472 5.88010 10 6 9 -10 77.1107 5.21403 10 6 9 -10 73.6894 5.87584 2 -6 -9 10 78.2670 6.92492 7 -6 -9 10 80.1280 5.67819 3 -6 -9 10 88.2320 5.68385 10 -6 -9 10 69.8782 4.08949 9 -6 -9 10 81.6470 3.42441 2 -6 -9 10 77.5066 3.50779 2 5 9 -10 128.458 8.17975 8 5 9 -10 130.547 6.69679 10 5 9 -10 141.878 7.58261 10 5 9 -10 128.315 7.35296 2 -5 -9 10 117.081 6.67355 10 -5 -9 10 133.323 5.16681 9 -5 -9 10 117.644 7.16130 3 -5 -9 10 136.888 5.76250 2 -5 -9 10 136.068 5.28846 2 -5 -9 10 127.968 8.32592 7 4 9 -10 30.3215 4.34073 2 4 9 -10 34.7321 3.81129 10 4 9 -10 35.3412 5.05497 10 -4 -9 10 42.0499 5.03937 3 -4 -9 10 34.3884 3.00462 2 -4 -9 10 35.2827 2.41803 9 -4 -9 10 34.5141 2.78679 2 -4 -9 10 35.8855 4.04889 10 -4 -9 10 30.4158 4.30210 7 3 9 -10 253.053 10.5239 10 3 9 -10 239.801 9.61227 10 3 9 -10 238.051 10.8046 8 3 9 -10 227.417 9.97083 2 -3 -9 10 234.446 10.3908 3 -3 -9 10 229.816 8.22817 2 -3 -9 10 237.077 9.77447 10 -3 -9 10 225.085 7.98509 2 -3 -9 10 246.672 10.9290 7 -3 -9 10 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73.6436 5.01095 2 3 6 -10 76.3875 4.81434 4 3 6 -10 75.0689 5.15554 8 -3 -6 10 67.7024 4.44970 10 -3 -6 10 70.7830 4.07457 2 -3 -6 10 68.1518 4.28076 9 -3 -6 10 70.5468 5.03974 7 -3 -6 10 67.9764 4.01800 2 -3 -6 10 70.1274 4.68735 10 2 6 -10 17.4397 2.84967 10 2 6 -10 24.4200 3.28853 10 2 6 -10 20.6462 2.60375 2 2 6 -10 24.2939 3.38733 2 2 6 -10 15.8923 2.57098 8 -2 -6 10 19.1344 2.16893 9 -2 -6 10 24.8715 2.99873 2 -2 -6 10 25.7394 3.60843 7 -2 -6 10 24.2877 2.88709 2 -2 -6 10 24.5680 2.75054 10 -2 -6 10 24.4721 3.91544 10 1 6 -10 76.4147 4.74616 10 1 6 -10 72.1858 4.06583 2 1 6 -10 78.3107 5.22043 10 1 6 -10 78.5058 5.04118 8 1 6 -10 77.4385 5.16200 2 -1 -6 10 82.6579 4.94243 7 -1 -6 10 73.5499 3.81568 9 -1 -6 10 69.7529 4.56278 10 -1 -6 10 77.6811 5.00202 10 -1 -6 10 77.6871 4.39981 2 -1 -6 10 80.2054 4.48286 2 0 6 -10 58.7277 3.74336 2 0 6 -10 62.6518 4.39662 10 0 6 -10 60.5247 4.41031 8 0 6 -10 64.1883 4.90850 10 0 6 -10 68.0038 4.89032 2 0 -6 10 71.0870 4.90061 10 0 -6 10 63.4021 4.18641 2 0 -6 10 66.1713 3.64841 9 0 -6 10 63.5183 4.24214 7 0 -6 10 62.9745 4.06354 2 0 -6 10 64.1161 4.40741 10 -1 6 -10 1936.21 45.7751 10 -1 6 -10 1968.99 43.5768 2 -1 6 -10 2029.99 45.4368 2 -1 6 -10 1923.39 44.9242 10 -1 6 -10 2012.79 44.7674 8 1 -6 10 2004.62 43.8706 7 1 -6 10 2013.00 45.6014 10 1 -6 10 1917.04 41.3401 5 1 -6 10 1903.74 45.0066 10 1 -6 10 1921.96 44.2721 2 1 -6 10 1990.66 44.1189 2 -2 6 -10 710.226 19.9191 10 -2 6 -10 739.123 17.9178 7 -2 6 -10 732.595 20.1455 2 -2 6 -10 722.105 19.1995 8 -2 6 -10 709.000 18.5939 2 -2 6 -10 736.521 20.7222 10 -2 6 -10 738.845 19.0223 6 2 -6 10 684.338 19.9906 10 2 -6 10 723.870 20.4088 10 2 -6 10 703.407 19.4530 2 2 -6 10 748.835 18.2683 7 2 -6 10 739.998 19.3200 2 2 -6 10 712.370 17.4605 5 -3 6 -10 11.6407 2.16852 6 -3 6 -10 13.4511 2.37809 8 -3 6 -10 10.8999 2.49967 10 -3 6 -10 6.78144 2.33547 2 -3 6 -10 12.2923 2.60904 2 -3 6 -10 6.07742 2.36698 10 -3 6 -10 12.3831 1.69075 7 3 -6 10 8.89463 2.00496 8 3 -6 10 11.0264 2.71217 10 3 -6 10 10.0046 2.59267 10 3 -6 10 11.0931 2.49787 2 3 -6 10 9.40961 1.94562 9 3 -6 10 9.51409 2.79067 2 -4 6 -10 72.2146 5.51052 10 -4 6 -10 71.0488 5.17393 2 -4 6 -10 70.1202 4.32508 8 -4 6 -10 66.1706 4.29014 2 -4 6 -10 63.2749 4.40718 6 -4 6 -10 62.2057 4.94312 10 4 -6 10 61.6636 4.31895 9 4 -6 10 72.5440 5.38986 10 4 -6 10 64.1239 4.86250 2 4 -6 10 68.2951 4.85258 2 4 -6 10 70.7858 4.65225 8 -5 6 -10 15.1360 3.05280 10 -5 6 -10 16.5027 3.08667 10 -5 6 -10 16.4383 3.21052 2 -5 6 -10 15.2954 2.36583 8 -5 6 -10 18.8594 3.02809 6 5 -6 10 17.0487 2.87282 8 5 -6 10 18.0865 2.91609 9 5 -6 10 18.2441 3.26252 2 5 -6 10 18.3635 3.58694 10 5 -6 10 19.9609 3.72065 10 -6 6 -10 4.80064 1.49074 8 -6 6 -10 5.31065 1.94020 6 -6 6 -10 5.24763 2.15805 2 -6 6 -10 3.68675 2.13706 10 6 -6 10 5.06881 1.88437 8 6 -6 10 4.61795 2.12713 2 6 -6 10 3.85029 1.96451 10 6 -6 10 8.02829 2.47655 10 6 -6 10 1.04159 1.50511 9 -7 6 -10 483.915 15.5814 6 -7 6 -10 517.752 15.8644 2 -7 6 -10 501.328 16.9693 10 -7 6 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4 -12 6 -10 98.0612 7.66939 10 12 -6 10 88.5472 6.73522 3 12 -6 10 101.496 8.10987 10 12 -6 10 95.5463 7.76294 2 12 -6 10 97.1096 8.27857 9 12 5 -10 0.36023 2.01886 2 12 5 -10 -2.3756 2.16915 9 12 5 -10 0.19073 2.53117 10 -12 -5 10 1.80252 2.07093 10 -12 -5 10 4.89211 6.04140 7 11 5 -10 18.4722 3.71169 2 11 5 -10 27.4437 3.83446 10 11 5 -10 21.4677 4.15778 10 11 5 -10 27.0946 4.79519 9 -11 -5 10 19.3074 4.23727 7 -11 -5 10 19.4564 3.48751 10 10 5 -10 403.322 14.0881 10 10 5 -10 438.819 15.0941 10 10 5 -10 425.185 15.5914 9 10 5 -10 426.148 14.7138 2 -10 -5 10 404.740 16.4252 7 -10 -5 10 408.198 11.5085 2 -10 -5 10 424.813 14.2319 10 -10 -5 10 419.146 11.4301 2 9 5 -10 16.0917 3.10602 10 9 5 -10 15.1094 3.45703 9 9 5 -10 15.8850 2.88121 10 9 5 -10 12.1213 3.17187 2 -9 -5 10 7.18970 2.34019 7 -9 -5 10 14.8110 2.81134 10 -9 -5 10 14.0004 1.48721 3 -9 -5 10 13.7835 2.10543 2 -9 -5 10 12.4437 2.08176 2 8 5 -10 0.94752 1.89817 2 8 5 -10 -0.0493 1.74923 9 8 5 -10 0.90006 1.55884 10 -8 -5 10 2.02566 1.09954 2 -8 -5 10 3.14535 1.78301 10 -8 -5 10 0.39440 1.22581 2 -8 -5 10 -0.7441 0.89693 9 -8 -5 10 0.71592 0.93805 3 -8 -5 10 1.38541 2.10184 7 7 5 -10 225.425 9.27222 9 7 5 -10 221.399 9.05258 2 7 5 -10 205.775 7.75183 2 7 5 -10 215.487 9.16445 10 7 5 -10 205.437 8.44840 10 -7 -5 10 221.522 7.46031 2 -7 -5 10 199.786 9.79654 7 -7 -5 10 206.465 8.67599 9 -7 -5 10 206.031 7.34169 2 -7 -5 10 220.861 7.48473 3 6 5 -10 108.397 5.99082 9 6 5 -10 104.922 3.65915 5 6 5 -10 100.228 4.99877 2 6 5 -10 111.792 6.31649 10 6 5 -10 113.565 6.23353 2 6 5 -10 99.1215 5.53633 10 6 5 -10 100.450 5.66789 4 -6 -5 10 108.604 6.77580 7 -6 -5 10 97.0069 5.60253 10 -6 -5 10 106.198 4.88183 2 -6 -5 10 108.572 5.25029 3 -6 -5 10 100.893 4.77223 2 -6 -5 10 103.249 5.58323 9 5 5 -10 247.554 8.33319 2 5 5 -10 271.489 9.55307 9 5 5 -10 264.817 9.97998 10 5 5 -10 259.923 9.33337 10 5 5 -10 261.406 9.68671 2 5 5 -10 256.487 9.37109 4 -5 -5 10 253.927 9.50697 10 -5 -5 10 262.423 8.42516 2 -5 -5 10 254.775 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10.2422 2 1 5 -10 283.581 9.74204 10 1 5 -10 293.814 10.4940 10 -1 -5 10 306.341 10.0277 7 -1 -5 10 290.608 8.93666 9 -1 -5 10 314.006 10.5238 10 -1 -5 10 291.654 9.96278 10 -1 -5 10 284.429 9.38316 2 -1 -5 10 285.648 9.20883 2 0 5 -10 867.774 21.1442 2 0 5 -10 908.599 22.4323 8 0 5 -10 874.149 22.3959 10 0 5 -10 895.208 23.2526 10 0 5 -10 870.446 22.6545 2 0 -5 10 907.453 21.7886 2 0 -5 10 878.949 21.9551 2 0 -5 10 887.307 18.7857 5 0 -5 10 880.772 22.5747 10 0 -5 10 845.230 21.7315 7 0 -5 10 896.030 21.2635 9 0 -5 10 895.682 22.9323 10 -1 5 -10 61.3165 4.01323 8 -1 5 -10 51.7298 3.41214 2 -1 5 -10 55.1074 4.31644 2 -1 5 -10 62.3841 4.25189 10 -1 5 -10 59.9141 4.61526 10 1 -5 10 58.8887 4.38335 10 1 -5 10 59.1292 3.61183 7 1 -5 10 56.9181 2.74906 5 1 -5 10 59.1157 3.95884 2 1 -5 10 60.5664 4.29005 10 1 -5 10 58.8231 3.88418 2 -2 5 -10 100.499 5.61424 10 -2 5 -10 112.747 5.32538 8 -2 5 -10 111.761 5.99567 2 -2 5 -10 108.079 6.21279 10 -2 5 -10 106.818 5.00341 2 2 -5 10 118.590 6.23826 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74.6175 5.88152 4 -10 5 -10 71.0895 6.33487 6 -10 5 -10 82.1384 5.57283 2 -10 5 -10 80.8937 6.39377 10 10 -5 10 72.4210 6.48788 9 10 -5 10 85.0009 6.75543 10 10 -5 10 78.9372 6.31896 2 -11 5 -10 20.9774 3.22736 2 -11 5 -10 15.9245 4.14706 10 -11 5 -10 19.1177 3.91817 4 -11 5 -10 16.1957 3.80562 6 11 -5 10 15.8684 3.48875 2 11 -5 10 16.4784 4.06588 10 11 -5 10 14.8769 3.71540 9 -12 5 -10 5.32904 2.24854 2 -12 5 -10 5.40879 2.51735 10 -12 5 -10 3.19291 2.79009 4 12 -5 10 7.75689 3.03577 10 12 -5 10 1.87184 2.66996 9 12 -5 10 4.07381 2.91754 2 13 4 -10 22.2988 4.58105 2 13 4 -10 9.31122 3.93420 9 13 4 -10 18.5817 4.17623 10 -13 -4 10 19.3086 4.13509 10 -13 -4 10 17.1355 4.37157 7 12 4 -10 5.93752 2.63117 10 12 4 -10 -2.1822 2.30959 9 12 4 -10 5.20056 2.54010 2 -12 -4 10 -0.0199 2.31683 7 -12 -4 10 1.21762 2.14377 10 -12 -4 10 1.40013 1.33552 2 11 4 -10 12.4711 2.88745 10 11 4 -10 14.3647 3.40778 10 11 4 -10 11.9411 3.56213 9 11 4 -10 11.2450 3.01989 2 -11 -4 10 13.2510 2.15483 2 -11 -4 10 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3 -5 -6 11 771.611 22.3168 7 -5 -6 11 750.303 20.6700 10 -5 -6 11 741.330 19.5559 9 -5 -6 11 725.813 18.7587 2 4 6 -11 248.581 9.39024 10 4 6 -11 256.451 9.57982 4 4 6 -11 253.806 10.0189 2 4 6 -11 265.501 10.3837 10 4 6 -11 240.398 8.48004 2 -4 -6 11 252.227 8.75318 9 -4 -6 11 263.105 8.73608 2 -4 -6 11 239.772 9.55982 10 -4 -6 11 259.810 10.6744 7 -4 -6 11 253.751 9.46397 3 -4 -6 11 254.162 8.56657 2 3 6 -11 825.481 22.3495 8 3 6 -11 806.219 22.1348 10 3 6 -11 784.701 21.0651 10 3 6 -11 809.424 21.3005 4 3 6 -11 816.024 21.7637 2 3 6 -11 790.065 20.8749 2 -3 -6 11 784.906 21.5245 10 -3 -6 11 793.691 20.1543 2 -3 -6 11 808.662 20.1481 2 -3 -6 11 791.592 22.1146 7 -3 -6 11 776.644 19.7640 9 2 6 -11 313.654 11.4354 8 2 6 -11 306.904 10.7702 10 2 6 -11 320.267 11.6636 10 2 6 -11 337.888 13.0854 2 2 6 -11 320.815 11.4028 2 -2 -6 11 307.358 10.1364 2 -2 -6 11 309.280 9.57462 9 -2 -6 11 312.603 11.3076 7 -2 -6 11 317.781 10.1698 2 -2 -6 11 313.465 11.2002 10 1 6 -11 299.495 10.9418 2 1 6 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4.82449 6 -6 6 -11 69.6917 5.40162 2 6 -6 11 73.6835 5.02247 8 6 -6 11 72.0571 5.27262 9 6 -6 11 60.4548 5.11833 2 6 -6 11 64.7171 5.66972 10 6 -6 11 68.5835 5.76141 10 -7 6 -11 9.95756 2.98647 10 -7 6 -11 5.68932 2.21617 6 -7 6 -11 10.9308 2.12961 8 7 -6 11 4.69210 2.45620 10 7 -6 11 14.4911 3.33393 2 7 -6 11 6.48246 2.46841 9 7 -6 11 6.91292 2.13419 8 -8 6 -11 300.662 12.5430 10 -8 6 -11 275.010 11.4001 6 -8 6 -11 281.893 9.37531 8 -8 6 -11 263.993 10.8145 2 8 -6 11 271.314 12.2541 10 8 -6 11 263.609 10.7799 8 8 -6 11 277.269 11.5944 2 8 -6 11 283.755 12.0343 9 -9 6 -11 47.2675 3.80555 8 -9 6 -11 38.9500 5.84752 10 -9 6 -11 38.4335 4.97279 6 -9 6 -11 42.0955 4.55740 2 9 -6 11 45.3728 5.27631 9 9 -6 11 55.3779 5.44180 2 9 -6 11 41.4288 5.74659 10 -10 6 -11 250.958 9.16342 8 -10 6 -11 263.341 11.2420 4 -10 6 -11 229.812 11.5508 10 -10 6 -11 265.174 10.5906 2 -10 6 -11 236.248 11.2833 6 10 -6 11 262.800 12.0079 2 10 -6 11 246.319 12.2301 10 10 -6 11 253.123 12.1823 9 -11 6 -11 225.914 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17.2428 2.87987 7 -5 -5 11 23.4589 2.91314 2 -5 -5 11 21.9684 2.70915 2 -5 -5 11 18.7936 2.66917 3 -5 -5 11 22.3093 3.22606 10 4 5 -11 53.2916 4.45826 2 4 5 -11 57.1053 3.99043 4 4 5 -11 51.1257 5.02015 2 4 5 -11 45.3590 4.25198 10 4 5 -11 50.3532 3.97005 10 -4 -5 11 51.9089 3.73599 9 -4 -5 11 55.3009 4.61454 7 -4 -5 11 49.1839 3.40938 2 -4 -5 11 48.9851 4.14502 10 -4 -5 11 47.9782 3.47967 2 3 5 -11 64.5546 4.40666 10 3 5 -11 67.0269 3.88788 2 3 5 -11 62.8894 4.84369 2 3 5 -11 60.1755 4.70630 10 3 5 -11 71.6475 4.42581 4 -3 -5 11 70.6461 4.06474 2 -3 -5 11 72.7910 4.22393 2 -3 -5 11 67.9423 4.07994 9 -3 -5 11 69.5324 4.76601 10 -3 -5 11 64.5588 4.23470 10 -3 -5 11 63.7701 4.74783 7 2 5 -11 18.1167 2.97992 10 2 5 -11 22.7110 2.86803 4 2 5 -11 18.8687 2.54913 8 2 5 -11 15.4522 2.40399 10 2 5 -11 22.4335 2.41406 2 2 5 -11 19.4409 3.00020 2 -2 -5 11 25.7304 3.28927 10 -2 -5 11 18.5496 2.36355 9 -2 -5 11 19.8726 2.88961 7 -2 -5 11 19.1839 2.70697 10 -2 -5 11 21.1328 2.73771 2 1 5 -11 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7 6 5 -12 73.5399 4.84902 4 6 5 -12 73.2325 5.08444 10 6 5 -12 82.5580 5.89366 10 6 5 -12 72.5270 2.71460 5 6 5 -12 74.1237 5.52636 2 -6 -5 12 78.9530 4.43911 2 -6 -5 12 75.9303 5.11490 9 -6 -5 12 80.8129 6.09480 7 -6 -5 12 73.2937 5.21404 10 -6 -5 12 79.6384 4.48787 2 -6 -5 12 73.1468 4.49800 3 5 5 -12 115.513 6.12795 10 5 5 -12 115.438 6.70789 2 5 5 -12 121.431 6.12211 4 5 5 -12 116.696 5.52494 2 5 5 -12 118.519 6.98427 10 -5 -5 12 121.986 6.11171 9 -5 -5 12 122.417 7.16535 7 -5 -5 12 129.399 6.74518 10 -5 -5 12 116.372 5.59055 2 -5 -5 12 120.995 5.62107 2 4 5 -12 -0.9058 1.64260 2 4 5 -12 -0.5908 1.50196 10 4 5 -12 0.49045 1.15813 4 4 5 -12 0.51720 1.13386 10 4 5 -12 1.90814 1.38484 2 -4 -5 12 0.11711 1.21296 7 -4 -5 12 2.91229 1.45682 2 -4 -5 12 1.49350 1.56774 10 -4 -5 12 1.90307 1.45105 2 -4 -5 12 1.21588 1.12821 9 3 5 -12 97.4764 5.51236 10 3 5 -12 94.0792 4.74712 2 3 5 -12 102.656 6.18724 10 3 5 -12 97.7399 5.27827 4 3 5 -12 97.0613 5.90909 2 -3 -5 12 99.0985 5.14163 9 -3 -5 12 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12.7922 2 -1 5 -12 454.683 14.9562 10 -1 5 -12 465.070 14.5943 2 -1 5 -12 472.355 13.6289 8 1 -5 12 444.036 13.7426 2 1 -5 12 489.491 13.8175 2 1 -5 12 460.944 13.0141 7 1 -5 12 442.939 11.2758 5 1 -5 12 442.723 14.3054 10 1 -5 12 437.880 14.5092 10 -2 5 -12 401.406 13.9954 10 -2 5 -12 460.540 15.9690 2 -2 5 -12 423.943 13.6406 2 -2 5 -12 413.523 12.3151 8 -2 5 -12 415.552 13.3918 10 -2 5 -12 394.051 12.8146 6 2 -5 12 409.867 12.7378 2 2 -5 12 388.918 13.5679 10 2 -5 12 413.486 11.5181 7 2 -5 12 378.122 14.1474 2 2 -5 12 398.840 11.0785 5 2 -5 12 391.775 13.3860 10 -3 5 -12 35.6376 3.17236 2 -3 5 -12 39.1705 3.87724 6 -3 5 -12 40.5829 4.48457 10 -3 5 -12 41.6933 4.20576 2 -3 5 -12 40.4769 6.30857 10 -3 5 -12 37.1300 3.21790 8 3 -5 12 38.5092 4.13300 10 3 -5 12 43.0724 2.70242 7 3 -5 12 38.6031 3.95283 10 3 -5 12 42.9863 3.77485 2 3 -5 12 36.1876 3.09654 5 -4 5 -12 518.860 13.9641 8 -4 5 -12 490.115 15.3716 6 -4 5 -12 487.773 15.8077 10 -4 5 -12 518.112 15.8702 2 -4 5 -12 530.743 16.7677 10 -4 5 -12 489.906 14.2505 2 4 -5 12 506.372 16.3755 10 4 -5 12 506.115 16.4074 10 4 -5 12 505.934 15.3454 9 4 -5 12 492.208 14.5140 5 4 -5 12 517.724 15.4327 2 -5 5 -12 497.840 15.5985 2 -5 5 -12 482.497 13.3685 8 -5 5 -12 509.312 16.6506 10 -5 5 -12 485.554 15.4460 6 -5 5 -12 567.309 22.2115 10 5 -5 12 479.176 14.3724 8 5 -5 12 510.472 17.5200 10 5 -5 12 485.746 15.3008 2 5 -5 12 463.423 14.7707 5 5 -5 12 503.255 15.6089 9 -6 5 -12 777.799 19.0877 8 -6 5 -12 786.572 22.0484 6 -6 5 -12 781.732 21.5950 2 -6 5 -12 750.417 22.5830 10 6 -5 12 776.411 22.0368 9 6 -5 12 789.799 22.9873 10 6 -5 12 755.440 20.5158 8 6 -5 12 778.617 22.9373 10 6 -5 12 805.636 21.9449 2 -7 5 -12 227.118 7.41917 8 -7 5 -12 202.224 9.96263 10 -7 5 -12 211.399 9.10883 2 -7 5 -12 197.025 9.41558 6 7 -5 12 212.350 10.1897 10 7 -5 12 212.364 10.1547 10 7 -5 12 205.391 9.55176 2 7 -5 12 206.675 8.51258 8 7 -5 12 203.147 9.67114 9 -8 5 -12 42.6716 5.56298 10 -8 5 -12 42.9448 3.31386 8 -8 5 -12 37.1552 5.01083 2 -8 5 -12 47.3628 4.97453 6 8 -5 12 36.0017 4.65464 2 8 -5 12 46.9119 5.03686 10 8 -5 12 39.0454 3.96963 8 -9 5 -12 57.1092 4.80572 2 -9 5 -12 53.6328 3.79699 8 -9 5 -12 52.6828 8.45970 6 -9 5 -12 50.6382 5.27397 10 -9 5 -12 51.4078 4.77198 4 9 -5 12 61.7802 5.79967 10 9 -5 12 59.5296 5.78511 9 9 -5 12 57.4819 5.48555 2 9 -5 12 49.3005 4.39429 8 -10 5 -12 34.1636 3.44902 8 -10 5 -12 40.2412 5.16458 10 -10 5 -12 40.0711 5.09120 4 -10 5 -12 41.8906 4.30114 2 -10 5 -12 45.3485 5.97461 6 10 -5 12 39.6282 5.53643 2 10 -5 12 40.6770 5.71866 10 10 -5 12 36.2286 5.55195 9 -11 5 -12 37.4240 4.92372 10 -11 5 -12 32.9435 4.76813 4 -11 5 -12 33.3621 5.23922 6 -11 5 -12 34.6097 4.28665 2 11 -5 12 34.5601 5.26444 2 11 -5 12 30.5064 5.02146 9 -12 5 -12 331.711 14.1234 4 -12 5 -12 303.177 14.4590 6 -12 5 -12 332.192 11.7455 2 -12 5 -12 335.184 14.2540 10 12 -5 12 328.168 14.3726 2 12 -5 12 322.915 15.1635 9 12 -5 12 347.147 15.0221 10 12 4 -12 46.9654 6.16271 10 12 4 -12 33.7934 6.65698 9 -12 -4 12 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1.22198 2.14926 7 -10 -6 14 -1.0929 0.70776 3 -10 -6 14 -0.1070 1.58293 2 -10 -6 14 -1.5159 1.99319 10 9 6 -14 23.9336 4.41342 10 9 6 -14 25.8373 4.55403 2 -9 -6 14 30.8575 4.36882 10 -9 -6 14 33.2955 5.71182 7 -9 -6 14 29.9248 2.88037 3 8 6 -14 -1.1189 2.17955 2 8 6 -14 -1.8938 1.79729 10 -8 -6 14 -1.4439 1.04125 3 -8 -6 14 0.50414 1.92177 10 -8 -6 14 -2.6411 1.88635 7 -8 -6 14 1.09092 1.45200 2 7 6 -14 148.148 8.43190 2 7 6 -14 123.134 7.99873 10 7 6 -14 130.083 7.56931 10 -7 -6 14 142.785 6.81292 3 -7 -6 14 134.721 7.81960 10 -7 -6 14 134.779 6.43439 2 -7 -6 14 131.890 8.80661 7 6 6 -14 131.979 8.00273 2 6 6 -14 139.775 8.33080 10 6 6 -14 121.013 7.08029 10 -6 -6 14 124.738 7.46626 10 -6 -6 14 126.835 6.36335 2 -6 -6 14 130.901 6.71354 3 -6 -6 14 126.936 8.28027 7 5 6 -14 173.408 13.1841 2 5 6 -14 178.241 9.18088 10 5 6 -14 145.594 8.18181 10 -5 -6 14 140.033 12.3749 7 -5 -6 14 164.237 7.69388 3 -5 -6 14 164.296 8.40457 10 -5 -6 14 165.751 9.60425 9 4 6 -14 135.511 7.78684 8 4 6 -14 130.933 7.58183 2 4 6 -14 131.173 10.7756 10 4 6 -14 138.449 6.79701 4 -4 -6 14 124.964 6.39145 9 -4 -6 14 138.525 7.59628 10 -4 -6 14 118.104 6.04918 2 -4 -6 14 132.891 7.75170 7 3 6 -14 42.0610 4.37118 4 3 6 -14 43.5424 4.43503 8 3 6 -14 35.8128 4.65620 2 3 6 -14 42.6918 4.77399 10 -3 -6 14 43.9226 3.72310 2 -3 -6 14 35.4913 3.66840 2 -3 -6 14 40.0042 4.97581 7 -3 -6 14 43.0643 4.49974 10 -3 -6 14 40.8730 3.62692 9 2 6 -14 67.6321 5.16908 8 2 6 -14 60.7873 4.50653 4 2 6 -14 65.6615 5.64008 10 2 6 -14 65.3010 5.48459 2 -2 -6 14 59.8112 4.18160 9 -2 -6 14 51.6565 4.02259 2 -2 -6 14 57.7314 4.99604 10 -2 -6 14 66.4759 5.10863 7 -2 -6 14 66.9159 4.68469 2 1 6 -14 1.94761 1.45048 10 1 6 -14 5.33056 2.46434 2 1 6 -14 3.09426 1.68699 8 1 6 -14 5.37551 2.28134 10 -1 -6 14 4.02901 1.86543 2 -1 -6 14 3.17853 1.77202 7 -1 -6 14 2.32005 1.44479 9 -1 -6 14 2.95237 1.93432 10 -1 -6 14 0.26733 0.92960 2 0 6 -14 347.436 12.9927 2 0 6 -14 343.452 12.1016 8 0 6 -14 344.171 13.4186 10 0 6 -14 342.323 12.4254 10 0 -6 14 372.941 12.0974 2 0 -6 14 338.526 11.7232 7 0 -6 14 336.960 11.3199 9 0 -6 14 346.341 13.0494 10 -1 6 -14 3.59737 2.53088 2 -1 6 -14 3.63636 2.00890 10 -1 6 -14 6.07626 2.01930 8 -1 6 -14 5.48401 2.30680 10 1 -6 14 9.40366 2.28166 7 1 -6 14 10.6234 2.23057 9 1 -6 14 7.02295 1.21532 5 1 -6 14 10.9260 2.50665 2 1 -6 14 6.72444 2.41860 10 -2 6 -14 313.521 12.2163 10 -2 6 -14 323.574 12.5239 2 -2 6 -14 320.504 13.0066 10 -2 6 -14 332.839 11.3074 8 -2 6 -14 326.289 12.0194 6 2 -6 14 353.432 13.2079 10 2 -6 14 331.214 10.6604 7 2 -6 14 316.658 9.39879 5 2 -6 14 347.645 11.9630 2 -3 6 -14 241.667 8.99308 8 -3 6 -14 249.572 10.6607 2 -3 6 -14 232.953 10.9705 10 -3 6 -14 233.271 9.92846 6 3 -6 14 239.335 9.87049 2 3 -6 14 239.738 7.84737 7 3 -6 14 248.537 11.0326 10 3 -6 14 240.144 8.31223 5 -4 6 -14 29.2009 4.56738 2 -4 6 -14 31.2143 4.46033 6 -4 6 -14 24.9228 3.07329 8 -4 6 -14 26.7739 4.62562 10 4 -6 14 27.1996 4.12875 10 4 -6 14 30.5322 3.14151 5 -5 6 -14 104.545 6.66809 6 -5 6 -14 99.3329 7.20372 10 -5 6 -14 108.788 7.03960 2 -5 6 -14 105.265 5.27132 8 5 -6 14 96.3228 7.09276 10 5 -6 14 97.8780 6.28927 9 5 -6 14 99.1890 5.84002 5 5 -6 14 90.9950 6.36890 2 -6 6 -14 123.931 5.66678 8 -6 6 -14 121.617 7.48644 2 -6 6 -14 123.764 8.13741 10 -6 6 -14 111.962 7.19827 6 6 -6 14 141.483 8.46207 10 6 -6 14 118.494 7.20601 9 6 -6 14 119.611 7.41265 2 -7 6 -14 42.9279 4.85801 6 -7 6 -14 43.5273 5.36674 2 -7 6 -14 39.2097 3.33954 8 -7 6 -14 45.5169 6.28595 10 7 -6 14 33.4109 5.04294 10 7 -6 14 43.6706 4.06952 8 7 -6 14 40.0725 5.61086 9 7 -6 14 37.2456 4.96667 2 -8 6 -14 27.0330 4.03345 2 -8 6 -14 28.4346 3.11563 8 -8 6 -14 31.6236 4.72263 6 -8 6 -14 34.9811 5.23088 10 8 -6 14 37.8258 5.22107 2 8 -6 14 31.1959 3.98708 8 8 -6 14 29.8242 4.43469 10 8 -6 14 38.5203 5.20700 9 -9 6 -14 123.720 5.75173 8 -9 6 -14 107.203 6.95113 4 -9 6 -14 126.505 8.29021 6 -9 6 -14 115.181 8.20268 10 -9 6 -14 100.351 6.92874 2 9 -6 14 125.145 8.56428 9 9 -6 14 115.740 8.04109 2 9 -6 14 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125.417 6.75848 10 -4 -4 14 132.126 6.24220 2 -4 -4 14 130.425 7.15248 10 -4 -4 14 136.825 6.33469 2 -4 -4 14 130.683 7.26731 7 -4 -4 14 126.773 7.42904 9 3 4 -14 357.222 13.1004 10 3 4 -14 353.524 12.6090 2 3 4 -14 348.188 10.9824 4 3 4 -14 341.707 11.9934 10 -3 -4 14 334.637 11.3844 2 -3 -4 14 364.614 11.5335 2 -3 -4 14 372.061 12.8352 10 -3 -4 14 355.589 12.5284 7 -3 -4 14 357.271 11.9357 9 2 4 -14 2.96571 1.89559 10 2 4 -14 4.59650 1.76716 10 2 4 -14 5.66938 1.56572 4 2 4 -14 7.91293 2.59211 2 -2 -4 14 7.09764 2.01471 10 -2 -4 14 4.71588 1.90703 7 -2 -4 14 3.81571 1.53941 2 -2 -4 14 2.63159 1.74156 10 -2 -4 14 5.15328 1.87119 2 -2 -4 14 2.33319 1.22526 9 1 4 -14 66.2640 5.31983 10 1 4 -14 69.1391 4.65219 8 1 4 -14 70.4190 5.36297 2 1 4 -14 59.5703 4.52770 10 -1 -4 14 71.1140 5.25061 10 -1 -4 14 69.1214 4.71377 9 -1 -4 14 93.9880 6.93813 10 -1 -4 14 69.0933 4.51421 2 -1 -4 14 62.0879 4.34814 2 -1 -4 14 63.0004 4.53216 7 0 4 -14 12.4610 2.37502 10 0 4 -14 11.0039 2.54864 10 0 4 -14 16.3456 3.17957 2 0 4 -14 17.5145 2.57297 2 0 4 -14 13.1930 2.30579 8 0 -4 14 16.3849 2.64114 7 0 -4 14 19.5955 2.97557 9 0 -4 14 17.3457 2.86663 2 0 -4 14 20.2187 4.13531 10 0 -4 14 17.4647 1.78781 5 0 -4 14 21.4616 3.51759 10 0 -4 14 18.1824 2.86452 2 -1 4 -14 -0.1819 1.59069 10 -1 4 -14 2.99415 2.06056 2 -1 4 -14 3.99758 2.60304 10 -1 4 -14 2.36160 1.47480 8 -1 4 -14 1.55947 1.28404 2 1 -4 14 1.80229 1.60072 10 1 -4 14 1.00379 1.42907 7 1 -4 14 3.66929 1.72564 2 1 -4 14 2.82381 1.17722 5 1 -4 14 3.54181 1.88133 10 -2 4 -14 102.763 5.05772 2 -2 4 -14 90.2832 5.65248 10 -2 4 -14 95.3274 6.10240 2 -2 4 -14 98.3421 6.56273 10 -2 4 -14 110.595 5.25164 8 -2 4 -14 90.7630 5.89789 6 2 -4 14 95.2931 5.91344 10 2 -4 14 97.7597 5.55117 2 2 -4 14 103.131 4.71049 7 2 -4 14 104.950 4.86328 5 2 -4 14 100.854 6.29360 10 -3 4 -14 69.6994 5.00955 10 -3 4 -14 69.8982 4.17266 2 -3 4 -14 63.4929 5.03645 2 -3 4 -14 70.9733 5.32137 6 -3 4 -14 69.7851 5.66006 10 3 -4 14 69.1155 3.43253 7 3 -4 14 68.4677 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10 5 2 24 10.4245 5.03216 2 2 -3 -24 6.97883 3.74323 10 2 -3 -24 -2.1536 2.80836 2 2 -3 -24 -1.3185 2.47661 6 2 -3 -24 7.38347 3.35326 5 -2 3 24 -3.6761 2.17813 2 -2 3 24 -0.4885 2.11190 10 1 -3 -24 325.418 13.1448 2 1 -3 -24 291.121 14.1862 10 1 -3 -24 336.693 14.5226 5 1 -3 -24 322.064 17.0771 6 -1 3 24 314.357 14.2608 10 -1 3 24 313.927 12.8621 2 0 -3 -24 48.4187 6.38133 10 0 -3 -24 56.8032 5.71827 2 0 -3 -24 55.9089 6.34390 5 0 3 24 46.4664 5.45034 2 0 3 24 44.3765 5.98335 10 -1 -3 -24 38.4583 5.78641 5 -1 -3 -24 51.7015 6.84403 10 -1 -3 -24 53.0614 5.31049 2 1 3 24 39.8847 5.38783 10 -2 -3 -24 24.3192 3.44814 2 -2 -3 -24 25.1759 5.55995 6 -2 -3 -24 25.3722 4.49781 10 -2 -3 -24 24.5232 4.70442 5 2 3 24 18.1334 3.93036 10 2 3 24 18.8454 3.85124 2 -3 -3 -24 15.3402 4.26844 6 -3 -3 -24 12.3000 3.38720 10 3 3 24 13.7219 3.16481 2 3 3 24 8.40357 2.99196 10 -4 -3 -24 4.54639 3.50084 6 -4 -3 -24 10.2477 3.34053 10 -4 -3 -24 5.52505 1.98992 2 4 3 24 8.54957 2.80589 2 4 3 24 8.02584 2.87631 10 -5 -3 -24 18.7364 4.87666 6 -5 -3 -24 21.0261 4.33287 10 5 3 24 28.9957 4.72253 10 5 3 24 22.4868 4.22238 2 1 -4 -24 65.0958 6.95778 5 1 -4 -24 61.7070 7.28379 10 1 -4 -24 50.9536 7.11795 6 1 -4 -24 63.9792 6.21706 2 -1 4 24 64.0034 5.82601 2 -1 4 24 50.9582 6.91056 10 0 -4 -24 5.38858 4.24494 6 0 -4 -24 9.88018 3.37945 5 0 -4 -24 6.17252 2.68742 2 0 -4 -24 5.13006 3.88227 10 0 4 24 2.72825 2.41667 2 0 4 24 6.45821 2.85495 10 -1 -4 -24 159.892 9.47427 2 -1 -4 -24 179.771 16.4705 6 -1 -4 -24 165.184 9.94465 10 -1 -4 -24 148.354 9.96343 5 1 4 24 173.773 9.94967 10 1 4 24 160.315 10.4172 2 -2 -4 -24 4.94491 3.21080 5 -2 -4 -24 2.57421 3.41268 10 -2 -4 -24 1.35330 2.16646 2 -2 -4 -24 -2.9298 2.31447 6 2 4 24 1.88539 2.42777 10 -3 -4 -24 30.7711 8.60268 5 -3 -4 -24 18.1661 3.56939 2 -3 -4 -24 24.1147 5.00084 6 -3 -4 -24 29.6206 4.52589 10 3 4 24 22.6151 4.40059 10 3 4 24 17.5405 3.89077 2 -4 -4 -24 35.0982 4.86108 10 -4 -4 -24 48.2514 6.89470 6 4 4 24 44.4985 5.80787 10 4 4 24 43.4491 5.15103 2 -1 -5 -24 19.6207 4.83262 6 -1 -5 -24 22.2503 3.40449 2 -1 -5 -24 20.5857 4.32440 10 -1 -5 -24 23.6411 5.07887 5 1 5 24 11.8439 3.29054 2 1 5 24 20.0348 4.19480 10 -2 -5 -24 35.5205 5.99623 5 -2 -5 -24 30.3557 5.27873 6 -2 -5 -24 33.8989 5.16913 10 2 5 24 23.9860 4.79814 2 2 5 24 33.1070 5.17401 10 -3 -5 -24 72.3692 7.65174 6 -3 -5 -24 72.8573 7.72547 5 -3 -5 -24 61.6451 8.40639 10 3 5 24 72.7868 6.38950 10 0 2 -25 -5.6858 2.67950 10 0 2 -25 -3.7642 2.95820 2 0 2 -25 1.06309 3.16238 6 0 -2 25 5.09600 3.11873 2 0 -2 25 6.25687 2.90786 10 0 -2 25 -2.7472 1.62889 7 -1 2 -25 282.852 14.5615 10 -1 2 -25 264.884 14.6078 6 1 -2 25 274.251 11.1875 7 1 -2 25 265.276 13.7231 10 1 -2 25 270.889 12.6951 2 -2 2 -25 117.039 9.18759 10 -2 2 -25 114.027 8.32532 2 -2 2 -25 118.331 9.97832 6 2 -2 25 116.187 6.60604 7 2 -2 25 110.658 8.88435 10 2 -2 25 110.273 8.26512 2 1 1 -25 8.74206 4.07677 2 1 1 -25 4.96559 2.38324 8 1 1 -25 13.6541 4.67650 10 1 1 -25 12.0176 4.18629 6 -1 -1 25 8.03407 3.11171 10 -1 -1 25 6.25194 3.46789 2 -1 -1 25 4.77033 2.92793 7 0 1 -25 0.32884 2.91630 6 0 1 -25 5.57516 4.08614 2 0 -1 25 7.31113 2.88044 10 0 -1 25 2.44482 2.05893 7 0 -1 25 6.73894 3.04140 2 -1 1 -25 20.4650 4.71118 2 -1 1 -25 28.6678 5.60704 6 -1 1 -25 29.9792 5.34046 10 1 -1 25 30.1190 4.71423 2 1 -1 25 27.7593 4.04687 7 1 -1 25 33.3287 5.97879 10 -2 1 -25 44.3339 5.56256 2 -2 1 -25 43.9628 5.72973 10 -2 1 -25 32.7260 5.74696 6 2 -1 25 43.2361 6.65347 10 2 -1 25 49.8770 6.07648 2 -3 1 -25 -0.1001 2.72372 10 -3 1 -25 5.06243 3.09878 2 -3 1 -25 2.37635 3.33966 6 3 -1 25 1.21341 1.49490 7 3 -1 25 -0.3832 2.24074 10 3 -1 25 1.60499 2.55574 2 1 0 -25 3.10847 3.22972 10 1 0 -25 17.0135 4.21136 6 1 0 -25 11.4120 2.94776 8 1 0 -25 11.8721 3.48915 5 -1 0 25 12.4166 4.07127 10 -1 0 25 6.78307 2.93535 7 -1 0 25 13.2131 3.39313 2 0 0 -25 7.17788 3.62083 2 0 0 -25 6.64658 3.55905 6 0 0 -25 11.2715 3.94826 10 0 0 25 3.05374 3.11617 10 0 0 25 4.51154 2.58976 7 0 0 25 6.66564 2.91264 2 -1 0 -25 71.8652 6.75888 2 -1 0 -25 68.1488 7.41972 10 -1 0 -25 60.3661 7.37697 6 1 0 25 69.0123 6.34228 2 1 0 25 70.3076 7.01580 10 1 0 25 70.0696 5.63084 7 -2 0 -25 4.99922 3.49282 10 -2 0 -25 0.26322 2.67795 2 -2 0 -25 1.38689 3.23024 6 2 0 25 4.99959 3.13728 10 2 0 25 0.56480 2.02480 7 2 0 25 -1.8040 2.22078 2 -3 0 -25 1.97136 2.64077 2 -3 0 -25 1.80335 3.17154 6 -3 0 -25 -2.1914 2.96017 10 3 0 25 4.98478 2.52246 10 3 0 25 -3.1887 2.18531 2 3 0 25 1.99996 1.57099 7 1 -1 -25 22.9032 4.71370 2 1 -1 -25 32.0874 4.82919 5 1 -1 -25 24.3474 4.84196 10 1 -1 -25 19.5455 4.44947 6 -1 1 25 21.6415 4.47669 2 -1 1 25 34.9840 6.40920 10 0 -1 -25 176.547 11.4184 6 0 -1 -25 184.529 11.3972 10 0 -1 -25 182.962 10.0249 2 0 -1 -25 180.506 9.91964 5 0 1 25 175.051 9.64092 2 0 1 25 175.049 10.5909 10 -1 -1 -25 41.5443 6.32568 6 -1 -1 -25 51.3730 6.51402 10 -1 -1 -25 45.4579 5.43845 2 1 1 25 38.7822 5.80357 10 1 1 25 45.8986 5.60759 2 -2 -1 -25 209.886 9.85412 2 -2 -1 -25 183.896 11.0471 10 -2 -1 -25 203.491 12.4395 6 2 1 25 194.638 10.1948 2 2 1 25 195.534 11.2174 10 2 1 25 198.576 9.04900 7 -3 -1 -25 -2.5855 2.78468 10 -3 -1 -25 -0.0516 2.88308 6 -3 -1 -25 0.54311 2.53578 2 3 1 25 2.22272 2.40829 10 3 1 25 -0.6587 2.27006 2 3 1 25 -1.7156 1.83892 7 0 -2 -25 59.1231 6.45717 5 0 -2 -25 48.4686 5.63829 2 0 -2 -25 40.3133 6.18030 6 0 -2 -25 49.3748 6.76698 10 0 2 25 37.6150 5.87495 10 0 2 25 41.2289 5.35561 2 -1 -2 -25 8.44573 3.62503 6 -1 -2 -25 4.05900 3.12304 5 -1 -2 -25 7.01454 3.30354 2 -1 -2 -25 14.3854 4.06690 10 1 2 25 6.52813 3.36602 10 1 2 25 9.88043 3.18421 2 -2 -2 -25 3.31093 2.71913 2 -2 -2 -25 -2.9912 2.50697 6 -2 -2 -25 2.32499 3.67346 10 2 2 25 0.61245 2.20060 2 2 2 25 4.26197 2.41288 10 -3 -2 -25 3.45138 3.16013 6 -3 -2 -25 0.59419 2.89211 10 3 2 25 -1.7615 2.06829 2 3 2 25 2.86880 2.39826 10 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type numerical _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.9717 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 0.71062 10.196 10.715 17.275 89.315 85.137 82.608 ) ; _shelx_hkl_checksum 20293 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O1 O 0.32317(6) -0.29868(5) 0.25425(4) 0.01851(11) Uani 1 1 d . N1 N 0.27773(7) -0.14014(6) 0.34150(4) 0.01696(12) Uani 1 1 d . N2 N 0.18201(7) 0.36225(7) 0.19164(4) 0.01963(13) Uani 1 1 d . N3 N 0.02058(7) 0.36167(7) 0.09921(4) 0.02038(14) Uani 1 1 d . C1 C 0.32832(7) -0.18798(7) 0.27161(4) 0.01342(12) Uani 1 1 d . C2 C 0.38675(7) -0.10033(7) 0.21114(4) 0.01282(12) Uani 1 1 d . H2 H 0.4316 -0.0381 0.2385 0.015 Uiso 1 1 calc R C3 C 0.48991(7) -0.17659(7) 0.15441(4) 0.01530(13) Uani 1 1 d . H3A H 0.5562 -0.2279 0.1842 0.018 Uiso 1 1 calc R H3B H 0.4453 -0.2347 0.1246 0.018 Uiso 1 1 calc R C4 C 0.56048(8) -0.09155(8) 0.09816(5) 0.02231(16) Uani 1 1 d . H4A H 0.5969 -0.0281 0.1284 0.027 Uiso 1 1 calc R H4B H 0.4946 -0.0460 0.0655 0.027 Uiso 1 1 calc R C5 C 0.67318(8) -0.16160(8) 0.04518(5) 0.02092(15) Uani 1 1 d . H5A H 0.6404 -0.2335 0.0208 0.025 Uiso 1 1 calc R H5B H 0.7003 -0.1043 0.0031 0.025 Uiso 1 1 calc R C6 C 0.79346(8) -0.21014(8) 0.08832(5) 0.02136(15) Uani 1 1 d . H6A H 0.8654 -0.2475 0.0512 0.032 Uiso 1 1 calc GR H6B H 0.7697 -0.2740 0.1262 0.032 Uiso 1 1 calc GR H6C H 0.8229 -0.1402 0.1154 0.032 Uiso 1 1 calc GR C7 C 0.27190(7) -0.02986(7) 0.17104(4) 0.01272(12) Uani 1 1 d . C8 C 0.19565(8) -0.09568(7) 0.12634(4) 0.01561(13) Uani 1 1 d . H8 H 0.2168 -0.1842 0.1201 0.019 Uiso 1 1 calc R C9 C 0.08884(8) -0.03205(7) 0.09091(5) 0.01676(13) Uani 1 1 d . H9 H 0.0366 -0.0776 0.0613 0.020 Uiso 1 1 calc R C10 C 0.05790(7) 0.09762(7) 0.09855(4) 0.01577(13) Uani 1 1 d . H10 H -0.0156 0.1404 0.0745 0.019 Uiso 1 1 calc R C11 C 0.13500(7) 0.16495(7) 0.14164(4) 0.01340(12) Uani 1 1 d . C12 C 0.24040(7) 0.10021(7) 0.17869(4) 0.01332(12) Uani 1 1 d . H12 H 0.2912 0.1455 0.2095 0.016 Uiso 1 1 calc R C13 C 0.11031(7) 0.30453(7) 0.14493(4) 0.01472(13) Uani 1 1 d . C14 C 0.00271(9) 0.48778(8) 0.10116(5) 0.02229(16) Uani 1 1 d . H14 H -0.0605 0.5317 0.0699 0.027 Uiso 1 1 calc R C15 C 0.07220(9) 0.55662(8) 0.14662(5) 0.02182(16) Uani 1 1 d . H15 H 0.0589 0.6460 0.1471 0.026 Uiso 1 1 calc R C16 C 0.16253(8) 0.48802(8) 0.19165(6) 0.02206(16) Uani 1 1 d . H16 H 0.2124 0.5321 0.2237 0.026 Uiso 1 1 calc R C17 C 0.21808(9) -0.22190(9) 0.39931(5) 0.02261(16) Uani 1 1 d . H17A H 0.2141 -0.3051 0.3759 0.027 Uiso 1 1 calc R H17B H 0.1263 -0.1844 0.4160 0.027 Uiso 1 1 calc R C18 C 0.29977(11) -0.23838(9) 0.46952(5) 0.02674(18) Uani 1 1 d . H18A H 0.3891 -0.2829 0.4536 0.032 Uiso 1 1 calc R H18B H 0.2562 -0.2901 0.5093 0.032 Uiso 1 1 calc R C19 C 0.31301(11) -0.11049(10) 0.50392(5) 0.02917(19) Uani 1 1 d . H19A H 0.3727 -0.1220 0.5465 0.035 Uiso 1 1 calc R H19B H 0.2249 -0.0708 0.5260 0.035 Uiso 1 1 calc R C20 C 0.36886(10) -0.02464(9) 0.44157(5) 0.02523(17) Uani 1 1 d . H20A H 0.3688 0.0602 0.4637 0.030 Uiso 1 1 calc R H20B H 0.4619 -0.0585 0.4249 0.030 Uiso 1 1 calc R C21 C 0.28698(9) -0.01457(8) 0.37121(5) 0.01995(15) Uani 1 1 d . H21A H 0.1968 0.0288 0.3863 0.024 Uiso 1 1 calc R H21B H 0.3292 0.0357 0.3300 0.024 Uiso 1 1 calc R O2 O 0.48896(6) 0.21095(5) 0.28711(4) 0.02034(12) Uani 1 1 d . N4 N 0.51031(7) 0.34307(6) 0.18488(4) 0.01576(12) Uani 1 1 d . N5 N 0.68994(7) 0.84713(7) 0.30769(4) 0.01922(13) Uani 1 1 d . N6 N 0.92431(7) 0.78396(7) 0.29385(4) 0.02063(13) Uani 1 1 d . C22 C 0.49283(7) 0.31924(7) 0.26185(4) 0.01476(13) Uani 1 1 d . C23 C 0.48684(7) 0.43017(7) 0.31760(4) 0.01463(13) Uani 1 1 d . H23 H 0.4281 0.5031 0.2973 0.018 Uiso 1 1 calc R C24 C 0.42960(8) 0.39738(8) 0.39927(4) 0.01795(14) Uani 1 1 d . H24A H 0.4821 0.3199 0.4173 0.022 Uiso 1 1 calc R H24B H 0.4394 0.4662 0.4352 0.022 Uiso 1 1 calc R C25 C 0.28380(8) 0.37710(8) 0.40336(5) 0.01945(14) Uani 1 1 d . H25A H 0.2316 0.4519 0.3818 0.023 Uiso 1 1 calc R H25B H 0.2745 0.3036 0.3710 0.023 Uiso 1 1 calc R C26 C 0.22822(9) 0.35501(9) 0.48642(5) 0.02290(16) Uani 1 1 d . H26A H 0.2863 0.2858 0.5096 0.027 Uiso 1 1 calc R H26B H 0.2299 0.4319 0.5174 0.027 Uiso 1 1 calc R C27 C 0.08696(10) 0.32188(11) 0.49168(6) 0.0303(2) Uani 1 1 d . H27A H 0.0852 0.2434 0.4634 0.046 Uiso 1 1 calc GR H27B H 0.0288 0.3898 0.4687 0.046 Uiso 1 1 calc GR H27C H 0.0559 0.3111 0.5463 0.046 Uiso 1 1 calc GR C28 C 0.62623(7) 0.46638(7) 0.31870(4) 0.01509(13) Uani 1 1 d . C29 C 0.64772(7) 0.59203(7) 0.31340(4) 0.01503(13) Uani 1 1 d . H29 H 0.5742 0.6556 0.3103 0.018 Uiso 1 1 calc R C30 C 0.77584(7) 0.62619(7) 0.31259(4) 0.01536(13) Uani 1 1 d . C31 C 0.88342(8) 0.53236(8) 0.31818(5) 0.01835(14) Uani 1 1 d . H31 H 0.9708 0.5545 0.3178 0.022 Uiso 1 1 calc R C32 C 0.86276(8) 0.40687(8) 0.32429(5) 0.02059(15) Uani 1 1 d . H32 H 0.9361 0.3434 0.3283 0.025 Uiso 1 1 calc R C33 C 0.73505(8) 0.37378(8) 0.32460(5) 0.01869(14) Uani 1 1 d . H33 H 0.7217 0.2877 0.3288 0.022 Uiso 1 1 calc R C34 C 0.79774(7) 0.76017(7) 0.30455(4) 0.01603(13) Uani 1 1 d . C35 C 0.71176(9) 0.96703(8) 0.29735(5) 0.02201(16) Uani 1 1 d . H35 H 0.6378 1.0310 0.2991 0.026 Uiso 1 1 calc R C36 C 0.83852(9) 1.00105(8) 0.28418(5) 0.02317(16) Uani 1 1 d . H36 H 0.8530 1.0862 0.2758 0.028 Uiso 1 1 calc R C37 C 0.94275(8) 0.90455(9) 0.28383(5) 0.02258(16) Uani 1 1 d . H37 H 1.0310 0.9248 0.2762 0.027 Uiso 1 1 calc R C38 C 0.53077(9) 0.23924(8) 0.12961(5) 0.02218(16) Uani 1 1 d . H38A H 0.4602 0.2499 0.0932 0.027 Uiso 1 1 calc R H38B H 0.5253 0.1588 0.1578 0.027 Uiso 1 1 calc R C39 C 0.66616(10) 0.23506(9) 0.08409(6) 0.02624(18) Uani 1 1 d . H39A H 0.6766 0.1672 0.0448 0.031 Uiso 1 1 calc R H39B H 0.7370 0.2159 0.1199 0.031 Uiso 1 1 calc R C40 C 0.68026(10) 0.36074(9) 0.04374(5) 0.02756(18) Uani 1 1 d . H40A H 0.6180 0.3742 0.0025 0.033 Uiso 1 1 calc R H40B H 0.7717 0.3594 0.0190 0.033 Uiso 1 1 calc R C41 C 0.65062(10) 0.46853(8) 0.10242(5) 0.02393(16) Uani 1 1 d . H41A H 0.7211 0.4619 0.1389 0.029 Uiso 1 1 calc R H41B H 0.6510 0.5499 0.0746 0.029 Uiso 1 1 calc R C42 C 0.51637(8) 0.46557(7) 0.14810(5) 0.01842(14) Uani 1 1 d . H42A H 0.5028 0.5321 0.1884 0.022 Uiso 1 1 calc R H42B H 0.4447 0.4825 0.1127 0.022 Uiso 1 1 calc R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0219(3) 0.0136(2) 0.0202(3) 0.00069(19) -0.0005(2) -0.0039(2) N1 0.0212(3) 0.0177(3) 0.0126(3) 0.0008(2) 0.0002(2) -0.0058(2) N2 0.0173(3) 0.0165(3) 0.0256(3) -0.0015(2) -0.0055(2) -0.0014(2) N3 0.0222(3) 0.0180(3) 0.0199(3) 0.0006(2) -0.0060(3) 0.0042(2) C1 0.0121(3) 0.0145(3) 0.0137(3) 0.0021(2) -0.0022(2) -0.0016(2) C2 0.0125(3) 0.0128(3) 0.0130(3) 0.0017(2) -0.0011(2) -0.0014(2) C3 0.0144(3) 0.0150(3) 0.0155(3) 0.0020(2) 0.0007(2) 0.0002(2) C4 0.0199(3) 0.0200(4) 0.0237(4) 0.0088(3) 0.0064(3) 0.0042(3) C5 0.0186(3) 0.0250(4) 0.0170(3) 0.0041(3) 0.0036(3) 0.0020(3) C6 0.0162(3) 0.0232(4) 0.0239(4) -0.0009(3) 0.0011(3) -0.0012(3) C7 0.0118(3) 0.0138(3) 0.0125(3) 0.0014(2) -0.0009(2) -0.0019(2) C8 0.0162(3) 0.0148(3) 0.0163(3) 0.0001(2) -0.0023(2) -0.0033(2) C9 0.0158(3) 0.0191(3) 0.0164(3) -0.0005(3) -0.0038(2) -0.0048(3) C10 0.0130(3) 0.0193(3) 0.0151(3) 0.0004(2) -0.0026(2) -0.0017(2) C11 0.0123(3) 0.0143(3) 0.0133(3) 0.0003(2) -0.0009(2) -0.0008(2) C12 0.0124(3) 0.0141(3) 0.0136(3) 0.0007(2) -0.0015(2) -0.0019(2) C13 0.0133(3) 0.0152(3) 0.0149(3) 0.0004(2) -0.0004(2) 0.0006(2) C14 0.0243(4) 0.0187(4) 0.0218(4) 0.0022(3) -0.0028(3) 0.0052(3) C15 0.0225(4) 0.0150(3) 0.0262(4) 0.0013(3) 0.0027(3) 0.0008(3) C16 0.0192(3) 0.0172(3) 0.0300(4) -0.0023(3) -0.0025(3) -0.0025(3) C17 0.0261(4) 0.0275(4) 0.0156(3) 0.0033(3) 0.0013(3) -0.0111(3) C18 0.0374(5) 0.0277(4) 0.0159(4) 0.0053(3) -0.0032(3) -0.0069(4) C19 0.0398(5) 0.0331(5) 0.0155(4) 0.0000(3) -0.0047(3) -0.0069(4) C20 0.0319(4) 0.0261(4) 0.0191(4) -0.0037(3) -0.0050(3) -0.0071(3) C21 0.0255(4) 0.0179(3) 0.0161(3) -0.0021(3) -0.0009(3) -0.0018(3) O2 0.0247(3) 0.0140(2) 0.0218(3) 0.0029(2) 0.0001(2) -0.0021(2) N4 0.0191(3) 0.0140(3) 0.0143(3) -0.0002(2) 0.0001(2) -0.0037(2) N5 0.0163(3) 0.0185(3) 0.0229(3) -0.0012(2) -0.0027(2) -0.0017(2) N6 0.0154(3) 0.0242(3) 0.0226(3) -0.0008(3) -0.0008(2) -0.0042(2) C22 0.0141(3) 0.0148(3) 0.0152(3) 0.0008(2) -0.0012(2) -0.0013(2) C23 0.0157(3) 0.0146(3) 0.0136(3) 0.0008(2) -0.0016(2) -0.0015(2) C24 0.0189(3) 0.0215(3) 0.0134(3) 0.0014(3) -0.0011(2) -0.0026(3) C25 0.0189(3) 0.0241(4) 0.0153(3) 0.0010(3) 0.0000(3) -0.0038(3) C26 0.0234(4) 0.0298(4) 0.0160(3) 0.0010(3) 0.0017(3) -0.0074(3) C27 0.0273(4) 0.0417(5) 0.0237(4) -0.0022(4) 0.0044(3) -0.0146(4) C28 0.0156(3) 0.0170(3) 0.0127(3) 0.0007(2) -0.0021(2) -0.0013(2) C29 0.0145(3) 0.0168(3) 0.0135(3) 0.0004(2) -0.0019(2) -0.0009(2) C30 0.0147(3) 0.0184(3) 0.0129(3) -0.0001(2) -0.0015(2) -0.0016(2) C31 0.0142(3) 0.0230(4) 0.0173(3) -0.0005(3) -0.0019(2) 0.0002(3) C32 0.0171(3) 0.0217(4) 0.0219(4) 0.0003(3) -0.0034(3) 0.0028(3) C33 0.0190(3) 0.0174(3) 0.0192(3) 0.0016(3) -0.0035(3) 0.0005(3) C34 0.0149(3) 0.0200(3) 0.0134(3) -0.0008(2) -0.0016(2) -0.0027(2) C35 0.0205(4) 0.0191(4) 0.0266(4) -0.0017(3) -0.0036(3) -0.0022(3) C36 0.0239(4) 0.0210(4) 0.0256(4) -0.0010(3) -0.0016(3) -0.0071(3) C37 0.0185(3) 0.0262(4) 0.0241(4) -0.0015(3) 0.0004(3) -0.0078(3) C38 0.0280(4) 0.0203(4) 0.0190(4) -0.0058(3) 0.0044(3) -0.0095(3) C39 0.0310(4) 0.0216(4) 0.0244(4) -0.0041(3) 0.0100(3) -0.0043(3) C40 0.0344(5) 0.0266(4) 0.0209(4) -0.0010(3) 0.0094(3) -0.0088(4) C41 0.0292(4) 0.0205(4) 0.0223(4) 0.0016(3) 0.0045(3) -0.0088(3) C42 0.0235(4) 0.0164(3) 0.0151(3) 0.0031(2) -0.0017(3) -0.0017(3) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0061 0.0033 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C1 N1 C17 119.50(7) C1 N1 C21 126.89(7) C21 N1 C17 113.30(7) C16 N2 C13 116.50(7) C14 N3 C13 116.07(7) O1 C1 N1 121.74(7) O1 C1 C2 119.41(7) N1 C1 C2 118.77(6) C1 C2 H2 108.8 C1 C2 C3 110.00(6) C3 C2 H2 108.8 C7 C2 C1 107.55(6) C7 C2 H2 108.8 C7 C2 C3 112.95(6) C2 C3 H3A 109.3 C2 C3 H3B 109.3 H3A C3 H3B 107.9 C4 C3 C2 111.68(6) C4 C3 H3A 109.3 C4 C3 H3B 109.3 C3 C4 H4A 108.8 C3 C4 H4B 108.8 C3 C4 C5 113.94(7) H4A C4 H4B 107.7 C5 C4 H4A 108.8 C5 C4 H4B 108.8 C4 C5 H5A 109.0 C4 C5 H5B 109.0 H5A C5 H5B 107.8 C6 C5 C4 112.75(7) C6 C5 H5A 109.0 C6 C5 H5B 109.0 C5 C6 H6A 109.5 C5 C6 H6B 109.5 C5 C6 H6C 109.5 H6A C6 H6B 109.5 H6A C6 H6C 109.5 H6B C6 H6C 109.5 C8 C7 C2 120.00(6) C12 C7 C2 120.91(6) C12 C7 C8 119.08(7) C7 C8 H8 119.9 C9 C8 C7 120.22(7) C9 C8 H8 119.9 C8 C9 H9 119.7 C10 C9 C8 120.53(7) C10 C9 H9 119.7 C9 C10 H10 120.1 C9 C10 C11 119.87(7) C11 C10 H10 120.1 C10 C11 C12 119.40(7) C10 C11 C13 120.52(6) C12 C11 C13 120.00(6) C7 C12 C11 120.87(7) C7 C12 H12 119.6 C11 C12 H12 119.6 N2 C13 N3 125.84(7) N2 C13 C11 117.18(6) N3 C13 C11 116.95(7) N3 C14 H14 118.6 N3 C14 C15 122.84(8) C15 C14 H14 118.6 C14 C15 H15 121.8 C14 C15 C16 116.30(8) C16 C15 H15 121.8 N2 C16 C15 122.44(8) N2 C16 H16 118.8 C15 C16 H16 118.8 N1 C17 H17A 109.6 N1 C17 H17B 109.6 N1 C17 C18 110.21(7) H17A C17 H17B 108.1 C18 C17 H17A 109.6 C18 C17 H17B 109.6 C17 C18 H18A 109.6 C17 C18 H18B 109.6 C17 C18 C19 110.35(8) H18A C18 H18B 108.1 C19 C18 H18A 109.6 C19 C18 H18B 109.6 C18 C19 H19A 109.5 C18 C19 H19B 109.5 C18 C19 C20 110.57(8) H19A C19 H19B 108.1 C20 C19 H19A 109.5 C20 C19 H19B 109.5 C19 C20 H20A 109.4 C19 C20 H20B 109.4 H20A C20 H20B 108.0 C21 C20 C19 111.20(8) C21 C20 H20A 109.4 C21 C20 H20B 109.4 N1 C21 C20 110.04(7) N1 C21 H21A 109.7 N1 C21 H21B 109.7 C20 C21 H21A 109.7 C20 C21 H21B 109.7 H21A C21 H21B 108.2 C22 N4 C38 119.83(7) C22 N4 C42 126.91(7) C38 N4 C42 113.22(6) C35 N5 C34 116.54(7) C37 N6 C34 116.43(7) O2 C22 N4 121.70(7) O2 C22 C23 120.65(7) N4 C22 C23 117.53(6) C22 C23 H23 108.6 C22 C23 C24 111.23(6) C24 C23 H23 108.6 C28 C23 C22 108.21(6) C28 C23 H23 108.6 C28 C23 C24 111.52(6) C23 C24 H24A 108.8 C23 C24 H24B 108.8 H24A C24 H24B 107.7 C25 C24 C23 113.74(6) C25 C24 H24A 108.8 C25 C24 H24B 108.8 C24 C25 H25A 109.2 C24 C25 H25B 109.2 H25A C25 H25B 107.9 C26 C25 C24 111.93(7) C26 C25 H25A 109.2 C26 C25 H25B 109.2 C25 C26 H26A 108.9 C25 C26 H26B 108.9 H26A C26 H26B 107.7 C27 C26 C25 113.21(7) C27 C26 H26A 108.9 C27 C26 H26B 108.9 C26 C27 H27A 109.5 C26 C27 H27B 109.5 C26 C27 H27C 109.5 H27A C27 H27B 109.5 H27A C27 H27C 109.5 H27B C27 H27C 109.5 C29 C28 C23 120.59(7) C29 C28 C33 118.90(7) C33 C28 C23 120.51(7) C28 C29 H29 119.5 C28 C29 C30 121.07(7) C30 C29 H29 119.5 C29 C30 C34 120.51(7) C31 C30 C29 119.23(7) C31 C30 C34 120.26(7) C30 C31 H31 120.0 C32 C31 C30 120.09(7) C32 C31 H31 120.0 C31 C32 H32 119.9 C31 C32 C33 120.26(7) C33 C32 H32 119.9 C28 C33 H33 119.8 C32 C33 C28 120.45(7) C32 C33 H33 119.8 N5 C34 N6 125.55(7) N5 C34 C30 117.52(7) N6 C34 C30 116.93(7) N5 C35 H35 118.8 N5 C35 C36 122.31(8) C36 C35 H35 118.8 C35 C36 H36 121.7 C37 C36 C35 116.53(8) C37 C36 H36 121.7 N6 C37 C36 122.62(8) N6 C37 H37 118.7 C36 C37 H37 118.7 N4 C38 H38A 109.6 N4 C38 H38B 109.6 N4 C38 C39 110.39(7) H38A C38 H38B 108.1 C39 C38 H38A 109.6 C39 C38 H38B 109.6 C38 C39 H39A 109.5 C38 C39 H39B 109.5 C38 C39 C40 110.66(8) H39A C39 H39B 108.1 C40 C39 H39A 109.5 C40 C39 H39B 109.5 C39 C40 H40A 109.6 C39 C40 H40B 109.6 C39 C40 C41 110.35(7) H40A C40 H40B 108.1 C41 C40 H40A 109.6 C41 C40 H40B 109.6 C40 C41 H41A 109.4 C40 C41 H41B 109.4 H41A C41 H41B 108.0 C42 C41 C40 111.29(7) C42 C41 H41A 109.4 C42 C41 H41B 109.4 N4 C42 C41 110.24(7) N4 C42 H42A 109.6 N4 C42 H42B 109.6 C41 C42 H42A 109.6 C41 C42 H42B 109.6 H42A C42 H42B 108.1 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C1 1.2355(9) N1 C1 1.3513(10) N1 C17 1.4651(10) N1 C21 1.4627(10) N2 C13 1.3399(10) N2 C16 1.3364(11) N3 C13 1.3420(10) N3 C14 1.3402(11) C1 C2 1.5304(10) C2 H2 1.0000 C2 C3 1.5348(10) C2 C7 1.5221(10) C3 H3A 0.9900 C3 H3B 0.9900 C3 C4 1.5233(11) C4 H4A 0.9900 C4 H4B 0.9900 C4 C5 1.5284(11) C5 H5A 0.9900 C5 H5B 0.9900 C5 C6 1.5198(12) C6 H6A 0.9800 C6 H6B 0.9800 C6 H6C 0.9800 C7 C8 1.3975(10) C7 C12 1.3944(10) C8 H8 0.9500 C8 C9 1.3913(11) C9 H9 0.9500 C9 C10 1.3896(11) C10 H10 0.9500 C10 C11 1.3963(10) C11 C12 1.3993(10) C11 C13 1.4850(10) C12 H12 0.9500 C14 H14 0.9500 C14 C15 1.3800(13) C15 H15 0.9500 C15 C16 1.3876(12) C16 H16 0.9500 C17 H17A 0.9900 C17 H17B 0.9900 C17 C18 1.5238(13) C18 H18A 0.9900 C18 H18B 0.9900 C18 C19 1.5261(14) C19 H19A 0.9900 C19 H19B 0.9900 C19 C20 1.5285(14) C20 H20A 0.9900 C20 H20B 0.9900 C20 C21 1.5262(12) C21 H21A 0.9900 C21 H21B 0.9900 O2 C22 1.2388(9) N4 C22 1.3516(10) N4 C38 1.4572(10) N4 C42 1.4573(10) N5 C34 1.3437(10) N5 C35 1.3390(11) N6 C34 1.3443(10) N6 C37 1.3365(11) C22 C23 1.5300(10) C23 H23 1.0000 C23 C24 1.5343(11) C23 C28 1.5221(10) C24 H24A 0.9900 C24 H24B 0.9900 C24 C25 1.5251(11) C25 H25A 0.9900 C25 H25B 0.9900 C25 C26 1.5240(11) C26 H26A 0.9900 C26 H26B 0.9900 C26 C27 1.5219(13) C27 H27A 0.9800 C27 H27B 0.9800 C27 H27C 0.9800 C28 C29 1.3922(10) C28 C33 1.3992(11) C29 H29 0.9500 C29 C30 1.3999(10) C30 C31 1.3978(11) C30 C34 1.4839(11) C31 H31 0.9500 C31 C32 1.3889(12) C32 H32 0.9500 C32 C33 1.3922(12) C33 H33 0.9500 C35 H35 0.9500 C35 C36 1.3869(12) C36 H36 0.9500 C36 C37 1.3832(13) C37 H37 0.9500 C38 H38A 0.9900 C38 H38B 0.9900 C38 C39 1.5249(13) C39 H39A 0.9900 C39 H39B 0.9900 C39 C40 1.5262(13) C40 H40A 0.9900 C40 H40B 0.9900 C40 C41 1.5289(13) C41 H41A 0.9900 C41 H41B 0.9900 C41 C42 1.5243(12) C42 H42A 0.9900 C42 H42B 0.9900