#------------------------------------------------------------------------------ #$Date: 2018-02-04 00:26:57 +0200 (Sun, 04 Feb 2018) $ #$Revision: 206122 $ #$URL: file:///home/coder/svn-repositories/cod/cif/4/51/43/4514338.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_4514338 loop_ _publ_author_name 'Korvorapun, Korkit' 'Kaplaneris, Nikolaos' 'Rogge, Torben' 'Warratz, Svenja' 'St\"uckl, A. Claudia' 'Ackermann, Lutz' _publ_section_title ; Sequential meta-/ortho-C--H Functionalizations by One-Pot Ruthenium(II/III) Catalysis ; _journal_issue 2 _journal_name_full 'ACS Catalysis' _journal_page_first 886 _journal_paper_doi 10.1021/acscatal.7b03648 _journal_volume 8 _journal_year 2018 _chemical_absolute_configuration ad _chemical_formula_moiety 'C23 H21 N3 O3' _chemical_formula_sum 'C23 H21 N3 O3' _chemical_formula_weight 387.43 _space_group_crystal_system orthorhombic _space_group_IT_number 19 _space_group_name_Hall 'P 2ac 2ab' _space_group_name_H-M_alt 'P 21 21 21' _symmetry_space_group_name_Hall 'P 2ac 2ab' _symmetry_space_group_name_H-M 'P 21 21 21' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary dual _audit_creation_date 2017-09-05 _audit_creation_method ; Olex2 1.2 (compiled 2017.08.10 svn.r3458 for OlexSys, GUI svn.r5381) ; _cell_angle_alpha 90 _cell_angle_beta 90 _cell_angle_gamma 90 _cell_formula_units_Z 4 _cell_length_a 6.2748(5) _cell_length_b 13.1370(11) _cell_length_c 24.081(2) _cell_measurement_reflns_used 9846 _cell_measurement_temperature 101 _cell_measurement_theta_max 74.56 _cell_measurement_theta_min 3.67 _cell_volume 1985.0(3) _computing_cell_refinement 'SAINT V8.38A (?, 2016)' _computing_data_reduction 'SAINT V8.38A (?, 2016)' _computing_molecular_graphics 'Olex2 (Dolomanov et al., 2009)' _computing_publication_material 'Olex2 (Dolomanov et al., 2009)' _computing_structure_refinement 'XL (Sheldrick, 2008)' _computing_structure_solution 'XT (Sheldrick, 2015)' _diffrn_ambient_temperature 101.23 _diffrn_measured_fraction_theta_full 0.992 _diffrn_measured_fraction_theta_max 0.989 _diffrn_measurement_device_type 'Bruker APEX-II CCD' _diffrn_measurement_method '\f and \w scans' _diffrn_radiation_type CuK\a _diffrn_radiation_wavelength 1.54178 _diffrn_reflns_av_R_equivalents 0.0197 _diffrn_reflns_av_unetI/netI 0.0181 _diffrn_reflns_Laue_measured_fraction_full 0.992 _diffrn_reflns_Laue_measured_fraction_max 0.989 _diffrn_reflns_limit_h_max 7 _diffrn_reflns_limit_h_min -7 _diffrn_reflns_limit_k_max 16 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 29 _diffrn_reflns_limit_l_min -30 _diffrn_reflns_number 16924 _diffrn_reflns_point_group_measured_fraction_full 0.994 _diffrn_reflns_point_group_measured_fraction_max 0.989 _diffrn_reflns_theta_full 67.679 _diffrn_reflns_theta_max 74.554 _diffrn_reflns_theta_min 3.671 _diffrn_standards_number 0 _exptl_absorpt_coefficient_mu 0.708 _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.8061 _exptl_absorpt_correction_type numerical _exptl_absorpt_process_details 'SADABS-2016/2 (Bruker,2016/2) was used for absorption correction. wR2(int) was 0.0777 before and 0.0339 after correction. The Ratio of minimum to maximum transmission is 0.9094. The \l/2 correction factor is Not present.' _exptl_crystal_colour colourless _exptl_crystal_colour_primary colourless _exptl_crystal_density_diffrn 1.296 _exptl_crystal_description plate _exptl_crystal_F_000 816 _exptl_crystal_size_max 0.49 _exptl_crystal_size_mid 0.21 _exptl_crystal_size_min 0.092 _refine_diff_density_max 0.140 _refine_diff_density_min -0.180 _refine_diff_density_rms 0.036 _refine_ls_abs_structure_details ; Flack x determined using 1676 quotients [(I+)-(I-)]/[(I+)+(I-)] (Parsons, Flack and Wagner, Acta Cryst. B69 (2013) 249-259). ; _refine_ls_abs_structure_Flack 0.03(3) _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.077 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 263 _refine_ls_number_reflns 4024 _refine_ls_number_restraints 0 _refine_ls_restrained_S_all 1.077 _refine_ls_R_factor_all 0.0260 _refine_ls_R_factor_gt 0.0259 _refine_ls_shift/su_max 0.001 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'w=1/[\s^2^(Fo^2^)+(0.0334P)^2^+0.3264P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.0658 _refine_ls_wR_factor_ref 0.0659 _reflns_Friedel_coverage 0.727 _reflns_Friedel_fraction_full 0.995 _reflns_Friedel_fraction_max 0.991 _reflns_number_gt 4000 _reflns_number_total 4024 _reflns_threshold_expression 'I > 2\s(I)' _cod_data_source_file cs7b03648_si_002.cif _cod_data_source_block cu_0123_cg_0m _cod_depositor_comments 'Adding full bibliography for 4514336--4514340.cif.' _cod_original_cell_volume 1985.1(3) _cod_database_code 4514338 _shelx_shelxl_version_number 2016/6 _shelx_space_group_comment ; The symmetry employed for this shelxl refinement is uniquely defined by the following loop, which should always be used as a source of symmetry information in preference to the above space-group names. They are only intended as comments. ; _shelx_estimated_absorpt_t_max 0.938 _shelx_estimated_absorpt_t_min 0.723 _olex2_refinement_description ; 1. Fixed Uiso At 1.2 times of: All C(H) groups, All C(H,H) groups At 1.5 times of: All C(H,H,H) groups 2.a Ternary CH refined with riding coordinates: C3(H3), C12(H12) 2.b Secondary CH2 refined with riding coordinates: C2(H2A,H2B), C4(H4A,H4B) 2.c Aromatic/amide H refined with riding coordinates: C6(H6), C7(H7), C8(H8), C9(H9), C10(H10), C15(H15), C17(H17), C18(H18), C19(H19), C21(H21), C22(H22), C23(H23) 2.d Idealised Me refined as rotating group: C13(H13A,H13B,H13C) ; _shelx_res_file ; TITL cu_0123_cg_0m_a.res in P2(1)2(1)2(1) cu_0123_cg_0m.res created by SHELXL-2016/6 at 09:54:12 on 05-Sep-2017 REM Old TITL cu_0123_CG_0m in P2(1)2(1)2(1) REM SHELXT solution in P2(1)2(1)2(1) REM R1 0.104, Rweak 0.028, Alpha 0.000, Orientation as input REM Flack x = 0.065 ( 0.039 ) from Parsons' quotients REM Formula found by SHELXT: C23 N3 O3 CELL 1.54178 6.2748 13.137 24.0811 90 90 90 ZERR 4 0.0005 0.0011 0.002 0 0 0 LATT -1 SYMM 0.5-X,-Y,0.5+Z SYMM -X,0.5+Y,0.5-Z SYMM 0.5+X,0.5-Y,-Z SFAC C H N O UNIT 92 84 12 12 L.S. 4 PLAN 20 SIZE 0.092 0.21 0.49 TEMP -171.92 BOND $H list 4 fmap 2 acta OMIT -2 3 6 OMIT 1 0 5 REM REM REM WGHT 0.033400 0.326400 FVAR 0.92667 O1 4 0.809093 0.413097 0.472990 11.00000 0.03304 0.03683 = 0.02817 -0.00486 -0.01306 0.01113 O2 4 0.381925 0.439870 0.338484 11.00000 0.01478 0.02810 = 0.02425 -0.00045 -0.00205 0.00331 O3 4 0.687376 0.429123 0.291371 11.00000 0.02003 0.02778 = 0.02242 0.00537 0.00432 0.00467 N1 3 0.711187 0.422414 0.383412 11.00000 0.01296 0.01649 = 0.02355 -0.00044 -0.00182 0.00175 N2 3 -0.044878 0.704147 0.342153 11.00000 0.02356 0.02550 = 0.02369 -0.00485 -0.00184 0.00358 N3 3 0.046915 0.873471 0.368799 11.00000 0.02892 0.02050 = 0.02613 0.00266 -0.00044 0.00308 C1 1 0.572321 0.431812 0.338590 11.00000 0.01855 0.01517 = 0.01953 0.00164 0.00001 0.00123 C2 1 0.914266 0.427802 0.304740 11.00000 0.01772 0.02442 = 0.03604 0.00681 0.00733 0.00361 AFIX 23 H2A 2 0.976901 0.496600 0.300844 11.00000 -1.20000 H2B 2 0.991948 0.380266 0.280084 11.00000 -1.20000 AFIX 0 C3 1 0.924103 0.392188 0.364617 11.00000 0.01200 0.01845 = 0.03116 0.00032 0.00091 0.00064 AFIX 13 H3 2 1.034619 0.432025 0.385182 11.00000 -1.20000 AFIX 0 C4 1 0.965404 0.277306 0.372142 11.00000 0.01693 0.01858 = 0.03133 0.00070 -0.00216 0.00450 AFIX 23 H4A 2 1.099142 0.259272 0.352675 11.00000 -1.20000 H4B 2 0.986389 0.263112 0.412145 11.00000 -1.20000 AFIX 0 C5 1 0.788559 0.210120 0.350667 11.00000 0.02093 0.01333 = 0.02535 0.00104 -0.00341 0.00598 C6 1 0.786876 0.174344 0.296031 11.00000 0.03307 0.02038 = 0.02540 0.00133 -0.00118 0.00896 AFIX 43 H6 2 0.900337 0.191814 0.271712 11.00000 -1.20000 AFIX 0 C7 1 0.621382 0.113540 0.276807 11.00000 0.04377 0.02284 = 0.03100 -0.00660 -0.01445 0.01218 AFIX 43 H7 2 0.621932 0.090445 0.239424 11.00000 -1.20000 AFIX 0 C8 1 0.455570 0.086365 0.311788 11.00000 0.02779 0.01909 = 0.05161 -0.00692 -0.01653 0.00527 AFIX 43 H8 2 0.342956 0.044621 0.298496 11.00000 -1.20000 AFIX 0 C9 1 0.454805 0.120402 0.366305 11.00000 0.02082 0.01844 = 0.04750 0.00209 -0.00213 0.00339 AFIX 43 H9 2 0.342246 0.101542 0.390599 11.00000 -1.20000 AFIX 0 C10 1 0.619681 0.182371 0.385351 11.00000 0.02179 0.01749 = 0.02715 0.00050 -0.00242 0.00447 AFIX 43 H10 2 0.617202 0.206179 0.422596 11.00000 -1.20000 AFIX 0 C11 1 0.668860 0.433817 0.440151 11.00000 0.02374 0.01624 = 0.02176 -0.00091 -0.00361 0.00215 C12 1 0.453640 0.476429 0.456864 11.00000 0.02423 0.01961 = 0.01975 0.00099 0.00099 0.00187 AFIX 13 H12 2 0.340474 0.440336 0.435248 11.00000 -1.20000 AFIX 0 C13 1 0.413778 0.458731 0.518792 11.00000 0.04355 0.02979 = 0.02412 0.00741 0.00790 0.00638 AFIX 137 H13A 2 0.518552 0.497071 0.540549 11.00000 -1.50000 H13B 2 0.427374 0.385999 0.527117 11.00000 -1.50000 H13C 2 0.269873 0.481786 0.528380 11.00000 -1.50000 AFIX 0 C14 1 0.445539 0.589494 0.442429 11.00000 0.02134 0.01834 = 0.01483 -0.00238 0.00349 0.00178 C15 1 0.276264 0.628685 0.411964 11.00000 0.01915 0.01795 = 0.01790 -0.00350 0.00171 -0.00086 AFIX 43 H15 2 0.168771 0.584051 0.398589 11.00000 -1.20000 AFIX 0 C16 1 0.261933 0.732896 0.400719 11.00000 0.02073 0.01932 = 0.01517 -0.00139 0.00395 0.00065 C17 1 0.420550 0.798083 0.420587 11.00000 0.02396 0.01780 = 0.01913 -0.00110 0.00389 -0.00032 AFIX 43 H17 2 0.412012 0.869098 0.413481 11.00000 -1.20000 AFIX 0 C18 1 0.590569 0.759081 0.450702 11.00000 0.02257 0.02339 = 0.02168 -0.00544 0.00013 -0.00427 AFIX 43 H18 2 0.698515 0.803511 0.464032 11.00000 -1.20000 AFIX 0 C19 1 0.603601 0.655278 0.461447 11.00000 0.02042 0.02590 = 0.01805 -0.00231 -0.00144 0.00294 AFIX 43 H19 2 0.720943 0.629077 0.481871 11.00000 -1.20000 AFIX 0 C20 1 0.077976 0.772404 0.368537 11.00000 0.02134 0.02076 = 0.01616 -0.00059 0.00387 0.00224 C21 1 -0.212510 0.741440 0.314385 11.00000 0.02361 0.03483 = 0.02455 -0.00466 -0.00340 0.00409 AFIX 43 H21 2 -0.303272 0.695232 0.295371 11.00000 -1.20000 AFIX 0 C22 1 -0.259298 0.844072 0.312162 11.00000 0.02607 0.03662 = 0.02179 0.00453 0.00112 0.00860 AFIX 43 H22 2 -0.378735 0.869465 0.292266 11.00000 -1.20000 AFIX 0 C23 1 -0.121754 0.907687 0.340656 11.00000 0.03288 0.02403 = 0.02952 0.00544 -0.00020 0.00683 AFIX 43 H23 2 -0.148538 0.978856 0.340168 11.00000 -1.20000 AFIX 0 HKLF 4 REM cu_0123_cg_0m_a.res in P2(1)2(1)2(1) REM R1 = 0.0259 for 4000 Fo > 4sig(Fo) and 0.0260 for all 4024 data REM 263 parameters refined using 0 restraints END WGHT 0.0334 0.3261 REM Highest difference peak 0.140, deepest hole -0.180, 1-sigma level 0.036 Q1 1 0.9260 0.3983 0.3339 11.00000 0.05 0.14 Q2 1 0.5540 0.4561 0.4492 11.00000 0.05 0.14 Q3 1 0.9477 0.3351 0.3666 11.00000 0.05 0.13 Q4 1 0.1835 0.7547 0.3769 11.00000 0.05 0.13 Q5 1 0.8760 0.2405 0.3606 11.00000 0.05 0.12 Q6 1 0.4551 0.4717 0.4875 11.00000 0.05 0.12 Q7 1 0.4493 0.5349 0.4502 11.00000 0.05 0.11 Q8 1 -0.3070 0.6542 0.3714 11.00000 0.05 0.11 Q9 1 1.3204 0.2475 0.3608 11.00000 0.05 0.11 Q10 1 1.1969 0.1830 0.3640 11.00000 0.05 0.11 Q11 1 0.2960 0.4041 0.3723 11.00000 0.05 0.11 Q12 1 -0.2933 0.9155 0.2422 11.00000 0.05 0.11 Q13 1 0.3628 0.7622 0.3993 11.00000 0.05 0.11 Q14 1 -0.3036 0.7426 0.3715 11.00000 0.05 0.10 Q15 1 0.8142 0.4100 0.3757 11.00000 0.05 0.10 Q16 1 0.7730 0.1999 0.3234 11.00000 0.05 0.10 Q17 1 0.2788 0.6821 0.4026 11.00000 0.05 0.10 Q18 1 0.4610 0.7823 0.4487 11.00000 0.05 0.10 Q19 1 0.7049 0.4537 0.4088 11.00000 0.05 0.10 Q20 1 -0.5338 0.6851 0.3404 11.00000 0.05 0.09 ; _shelx_res_checksum 6501 _shelx_hkl_file ; -1 0 0 0.47348 0.11852 4 -2 0 0 327.717 9.48732 4 -3 0 0 1.45968 0.28540 4 -4 0 0 20.5481 1.16089 3 4 0 0 22.2673 1.16496 3 -4 0 0 22.3710 1.16640 4 -5 0 0 0.40858 0.37215 4 -5 0 0 -0.2434 0.19880 7 -6 0 0 1576.17 45.1493 3 -6 0 0 1591.31 47.6860 9 6 0 0 1569.09 45.0143 3 7 0 0 0.08583 0.19466 3 -7 0 0 0.12908 0.27428 3 0 -1 0 0.25876 0.04072 7 0 1 0 0.16353 0.04011 7 -1 -1 0 349.811 10.0314 4 -1 1 0 355.198 10.0238 4 -2 -1 0 485.575 13.7870 4 -2 1 0 475.637 13.7659 4 -3 -1 0 9.33935 0.64601 4 -3 1 0 9.37009 0.62161 4 -4 1 0 690.674 19.7636 7 4 -1 0 678.431 19.8052 3 -4 -1 0 691.330 19.8247 4 -4 1 0 678.524 19.7691 4 4 1 0 676.047 19.7399 3 -4 1 0 672.641 19.8075 3 -4 -1 0 674.997 19.8741 3 -5 1 0 133.224 4.61866 7 5 1 0 149.213 5.45364 3 -5 -1 0 130.477 4.67371 4 -5 1 0 129.939 4.54459 2 -6 -1 0 43.0332 1.98241 3 -6 1 0 40.9667 1.98058 3 6 -1 0 40.9085 1.85202 3 -6 1 0 42.0719 2.52242 9 6 1 0 46.3106 2.42892 3 7 -1 0 466.973 13.8285 3 -7 -1 0 462.578 14.1627 9 -7 -1 0 462.207 13.9721 3 -7 1 0 461.513 13.4405 3 0 2 0 123.164 3.54753 7 -1 -2 0 6048.34 176.082 1 1 2 0 6063.29 176.312 1 1 -2 0 6155.60 176.681 1 -1 2 0 6101.96 176.581 1 -2 2 0 198.795 5.86256 7 -2 -2 0 198.659 5.88001 4 -3 2 0 861.668 24.6673 4 -3 -2 0 866.985 24.7371 4 -3 2 0 861.725 24.6866 7 4 -2 0 555.656 16.3134 3 -4 2 0 551.636 16.2434 3 4 2 0 536.082 16.1424 3 -4 2 0 579.269 16.2509 7 -4 -2 0 562.148 16.2968 4 -4 -2 0 541.341 16.3508 3 5 -2 0 359.733 10.9493 3 -5 2 0 352.782 10.9746 2 -5 -2 0 355.595 11.0848 4 -5 2 0 357.568 10.9834 7 -5 -2 0 367.406 11.0653 3 -5 2 0 367.557 11.9695 9 6 2 0 191.462 5.90768 3 -6 2 0 190.357 6.46079 3 7 -2 0 0.81622 0.37859 3 -7 -2 0 1.01783 0.46495 9 0 3 0 0.47222 0.12506 7 1 -3 0 1294.67 36.4788 4 -2 -3 0 43.5688 1.53596 4 -2 3 0 44.2846 1.52942 7 -3 3 0 5033.49 141.629 4 -4 3 0 787.206 23.2082 2 4 3 0 794.441 22.8951 3 4 -3 0 770.177 23.2486 3 -4 -3 0 794.330 23.1116 4 -4 3 0 816.795 23.0096 3 -4 3 0 815.946 23.0447 7 5 -3 0 287.176 8.86066 3 -5 -3 0 286.583 8.99555 4 -5 3 0 274.635 8.68170 3 -5 3 0 286.107 8.86075 7 -5 3 0 283.189 8.93730 2 -5 -3 0 292.594 8.97415 3 -6 3 0 7.38672 0.58972 3 6 -3 0 5.60527 0.70183 3 -6 -3 0 7.51089 0.79241 3 6 3 0 6.70369 0.52680 3 -7 -3 0 110.029 4.34332 9 -7 -3 0 112.553 3.71984 3 7 -3 0 115.993 3.63074 3 -1 4 0 7.84971 0.43411 7 1 -4 0 7.55163 0.37377 4 -1 -4 0 7.82967 0.37140 4 -2 -4 0 36.1218 1.31215 4 -2 4 0 34.6426 1.30013 7 -3 4 0 722.895 20.8461 7 -3 -4 0 728.068 20.9050 4 -4 -4 0 38.6732 1.83636 3 -4 4 0 41.7998 1.73735 7 -4 4 0 38.3225 1.61384 3 -4 -4 0 41.8643 1.80440 4 -4 4 0 40.0880 1.88362 2 4 -4 0 39.3107 1.76166 3 -5 4 0 23.3360 1.28785 7 5 -4 0 21.4260 1.27962 3 -5 4 0 20.5216 1.07719 3 5 4 0 20.2773 1.02533 3 -5 4 0 21.9335 1.38362 2 -5 -4 0 20.3654 1.28484 4 -5 -4 0 22.0205 1.34204 3 -6 -4 0 0.88957 0.35499 3 -6 4 0 0.44506 0.31900 2 6 -4 0 0.13567 0.29674 3 7 -4 0 116.255 3.66178 3 7 4 0 115.412 3.75232 11 -7 -4 0 111.368 4.40350 9 -7 -4 0 116.503 3.75613 3 0 5 0 0.02805 0.13335 7 1 -5 0 3029.03 85.1766 4 -2 5 0 75.5991 2.46096 7 2 -5 0 76.0800 2.83349 4 -2 -5 0 73.2692 2.43632 4 -3 -5 0 578.331 16.8011 4 -4 5 0 565.122 16.7637 2 -4 -5 0 577.022 16.5995 4 4 5 0 509.591 17.2681 6 -4 -5 0 579.787 16.6838 3 4 -5 0 561.655 16.5699 3 -4 5 0 576.679 16.4871 7 -5 -5 0 58.6859 2.56767 4 -5 5 0 59.3137 2.46677 7 -5 -5 0 62.9149 2.58420 3 -5 5 0 63.0289 2.65258 2 5 -5 0 61.9309 2.49925 3 -6 -5 0 358.499 10.9535 3 -6 5 0 357.822 10.9313 2 6 -5 0 364.063 10.8472 3 7 -5 0 71.5696 2.37068 3 -7 -5 0 69.4520 3.04632 9 -7 -5 0 70.2533 2.44438 3 7 5 0 71.4678 2.45809 11 -3 -6 0 170.684 5.27651 4 -3 6 0 163.196 5.21365 7 4 -6 0 122.279 4.19269 3 -4 -6 0 124.568 4.26876 4 -4 6 0 118.869 4.40315 2 4 6 0 127.217 4.48744 6 -4 6 0 119.093 4.23870 11 -4 -6 0 122.705 4.27160 3 -4 6 0 121.344 4.11829 7 -5 -6 0 4.66961 0.69052 3 5 -6 0 3.81673 0.60746 3 -5 6 0 4.23718 0.69737 7 -5 -6 0 4.72977 0.70504 4 -5 6 0 3.56005 0.71073 2 -6 6 0 19.0576 1.17788 2 6 -6 0 18.6208 1.06620 3 6 6 0 17.5128 1.11039 11 -6 -6 0 18.5136 1.12406 3 7 -6 0 371.568 10.9068 3 -7 -6 0 378.231 11.7760 9 7 6 0 381.811 11.0040 11 -7 -6 0 375.653 10.9823 3 0 7 0 0.43720 0.19686 7 -1 7 0 1566.49 45.8369 7 1 -7 0 1649.67 45.7033 4 -1 -7 0 1642.71 45.6421 4 -2 7 0 0.34445 0.21258 7 2 7 0 0.36886 0.31406 5 -3 -7 0 76.6566 2.70260 4 3 7 0 78.4296 3.17891 6 -3 7 0 77.6693 2.69748 7 -3 7 0 72.5617 2.83984 11 -3 7 0 74.7477 3.01268 2 3 7 0 73.1299 2.77547 8 -4 7 0 636.604 18.9518 2 4 7 0 647.507 19.0500 6 -4 7 0 615.266 18.6496 11 4 -7 0 654.909 18.7693 3 -4 -7 0 631.477 18.6523 4 -4 7 0 622.495 18.5671 7 5 7 0 221.708 7.15389 6 -5 7 0 229.273 7.56810 2 5 7 0 218.836 7.15086 11 6 -7 0 6.46668 0.59245 3 6 7 0 5.00512 0.62020 11 -6 -7 0 5.19092 0.58819 3 -6 7 0 4.92475 0.65163 2 7 7 0 257.480 7.25551 11 -7 -7 0 232.610 7.73315 9 -7 -7 0 247.139 7.19665 3 0 8 0 785.304 22.4781 7 -1 -8 0 1213.94 34.0436 4 -1 8 0 1180.01 34.2989 7 1 8 0 1166.29 34.5220 8 1 8 0 1246.95 35.0173 6 1 -8 0 1237.75 34.1241 4 -1 8 0 1192.37 34.7624 5 1 8 0 1205.80 34.8888 5 -2 8 0 261.365 8.37419 2 -2 8 0 274.875 8.01127 7 2 8 0 269.538 8.19049 8 2 8 0 271.544 8.60493 5 -2 -8 0 268.422 7.85741 4 2 8 0 255.127 8.57693 6 -2 8 0 255.922 8.08971 8 -3 8 0 183.681 5.82751 7 3 8 0 189.605 6.42203 6 3 8 0 186.054 5.95995 11 3 8 0 183.591 5.94715 8 -3 8 0 175.356 5.93314 11 -3 -8 0 189.139 5.79680 4 -3 8 0 185.543 6.23099 2 -3 8 0 179.363 5.80359 8 4 -8 0 421.531 12.8742 3 -4 8 0 428.528 13.2914 2 4 8 0 446.061 13.4335 6 -4 -8 0 433.275 12.9692 4 4 8 0 431.333 13.0309 11 -4 8 0 438.176 12.9603 7 -4 -8 0 427.879 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161.157 4.99784 4 -3 7 4 155.438 5.23044 11 -3 7 4 156.657 5.32650 2 -3 -7 4 163.298 5.15255 4 3 7 4 153.673 5.25031 11 3 -7 -4 161.061 5.28885 3 -3 7 -4 164.601 5.05439 7 3 7 4 162.085 5.60816 6 -4 -7 -4 913.446 26.4664 4 -4 7 4 921.593 26.4016 7 -4 7 4 889.285 26.5796 11 -4 -7 -4 897.091 26.3896 3 4 -7 4 910.406 26.2969 3 -4 7 4 933.692 26.7432 2 -4 -7 4 955.935 27.1319 4 -4 -7 4 913.686 27.1899 3 4 -7 -4 930.462 27.1258 3 -4 7 -4 936.861 26.9592 7 4 7 4 936.208 27.1581 11 -4 7 -4 941.788 27.4113 2 4 7 4 931.968 27.3329 6 -5 -7 -4 310.118 9.59350 3 -5 7 4 306.464 9.80056 2 5 7 -4 324.129 9.92243 6 5 -7 4 313.301 9.50432 3 5 -7 -4 324.591 9.93908 3 5 7 4 345.223 10.3649 11 -5 7 -4 314.839 10.2686 2 -5 -7 4 313.036 10.0078 3 6 7 -4 274.362 8.33695 11 -6 -7 -4 270.728 8.64154 3 -6 7 4 270.666 8.30086 2 6 -7 4 275.781 8.19376 3 6 -7 -4 300.915 9.49565 3 -6 7 -4 281.312 8.79852 2 -6 -7 4 287.891 9.65171 3 6 7 4 279.706 8.70768 11 7 7 -4 67.3907 2.06139 11 -7 -7 -4 53.6753 2.39713 9 -7 -7 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115.299 3.84136 3 -4 -2 -9 113.899 4.12869 4 -4 2 9 117.760 4.27635 11 4 -2 -9 111.831 4.02884 3 -4 -2 9 111.880 3.92273 4 -4 2 -9 112.653 4.05782 2 -4 -2 9 109.709 3.71698 7 -4 2 -9 110.014 3.80915 3 4 2 9 110.504 3.80933 11 -4 2 -9 118.220 5.07175 9 5 2 -9 68.4299 2.68210 3 -5 -2 -9 72.7986 3.95039 9 -5 2 9 69.1534 2.69160 3 -5 -2 -9 65.2524 2.94057 4 -5 -2 -9 70.0179 2.73689 3 -5 2 9 67.5547 2.66853 7 5 2 9 69.4732 2.58272 11 -5 -2 9 65.6212 2.57377 7 -5 2 -9 70.5464 3.72650 9 -5 2 -9 65.8022 2.68336 7 -5 2 -9 65.9298 2.58378 3 -5 -2 9 71.1617 2.89060 3 5 -2 -9 68.1706 2.82950 3 -6 2 9 2.72102 0.42524 3 -6 -2 -9 2.45835 0.79800 9 6 2 -9 2.54413 0.40564 3 -6 -2 -9 2.72274 0.49908 3 -6 -2 9 2.26352 0.53124 3 -6 2 -9 2.50401 0.42885 3 6 2 9 2.83218 0.43493 11 6 -2 -9 2.79524 0.57320 3 -6 2 -9 2.63922 0.75323 9 -7 -2 -9 29.8611 1.70730 9 -7 -2 -9 30.5557 1.23089 3 -7 2 -9 28.0361 1.40083 9 7 -2 -9 30.4953 1.20801 3 -7 -2 9 30.7127 1.23053 3 0 3 9 7.15563 0.44856 7 0 -3 9 7.54428 0.47819 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403.089 12.8943 2 -3 4 -9 418.616 12.6681 3 -3 -4 9 419.356 12.4354 7 -3 -4 9 441.179 12.7337 4 3 -4 -9 423.307 12.8574 3 -3 4 -9 438.600 12.4863 7 3 4 9 433.123 12.9021 11 -4 4 9 13.5070 0.91197 3 -4 -4 -9 14.8104 0.99672 3 -4 4 9 15.1282 1.08559 7 4 4 -9 13.3705 0.92360 3 -4 4 9 15.7181 1.08714 2 -4 4 -9 16.4946 1.58191 9 -4 -4 9 15.0973 1.01410 4 4 4 9 15.8923 1.00887 11 -4 4 -9 15.3532 0.90755 7 -4 -4 9 14.5941 0.85224 7 -4 4 -9 14.3851 0.88874 3 4 -4 -9 12.8634 1.16717 3 -5 -4 -9 262.792 8.68451 4 5 4 -9 266.835 8.05517 3 -5 -4 -9 277.817 8.42268 3 -5 4 9 265.563 8.39825 7 -5 -4 9 281.516 8.79725 3 5 4 9 279.158 8.50034 11 -5 4 -9 280.682 9.73466 9 -5 4 -9 259.146 8.45028 7 5 -4 -9 282.957 8.74032 3 -5 4 -9 264.082 8.23368 3 -5 -4 9 272.010 8.75892 4 -6 -4 -9 41.8012 1.79885 3 -6 -4 -9 41.7139 2.62927 9 -6 4 -9 41.3308 2.28238 9 6 -4 -9 42.5355 1.87881 3 -6 -4 9 42.3604 1.92948 3 6 4 9 42.6475 1.72871 11 -7 -4 -9 70.0164 2.19455 3 -7 -4 -9 59.2856 2.65065 9 -7 -4 9 69.2385 2.28858 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19.6161 2 3 8 9 679.597 19.9303 6 -4 8 9 1.93135 0.57980 11 -4 -8 -9 1.02055 0.34517 3 -4 8 9 1.24726 0.59978 2 4 8 9 1.37669 0.43664 11 -4 8 -9 1.79884 0.56325 2 4 -8 -9 2.21199 0.50953 3 -5 -8 -9 64.7106 2.37175 3 5 8 -9 64.6836 2.73800 6 5 8 -9 64.0195 2.37421 11 -5 8 9 64.5467 2.54284 2 -5 8 -9 68.1484 2.72369 2 -5 -8 9 67.3961 2.62557 3 5 -8 -9 66.0480 2.52668 3 5 8 9 67.2324 2.57594 11 -5 8 -9 67.9978 2.35421 8 -6 -8 -9 64.1226 2.78671 9 6 8 -9 59.2438 2.04527 11 -6 -8 -9 63.0336 2.08763 3 6 8 9 64.5452 2.22110 11 -6 -8 9 64.1376 2.24863 3 0 9 -9 361.882 11.0090 8 0 9 9 354.219 11.1872 2 0 -9 9 358.402 10.6935 4 0 9 -9 360.091 11.3803 6 0 9 9 368.175 11.4871 6 0 9 9 356.358 11.1955 5 0 9 9 359.971 11.0623 11 0 9 -9 363.349 11.2816 5 0 9 9 365.107 10.9570 8 0 9 9 362.176 10.9299 7 -1 9 9 69.2566 3.09748 11 1 9 -9 63.5955 2.73888 5 1 -9 9 56.0897 2.90110 4 -1 9 9 62.5364 2.41860 8 -1 9 9 61.9051 2.61472 5 1 9 -9 61.1907 2.50057 8 -1 9 9 64.3340 2.62626 7 -1 -9 -9 60.0758 2.16692 4 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142.227 4.60751 11 -5 9 -9 144.667 4.72338 2 5 -9 -9 139.475 4.47110 3 -5 -9 9 136.085 4.55790 3 -6 -9 -9 2.10451 0.41641 9 6 9 9 1.92215 0.27180 11 -6 9 -9 2.28708 0.32178 5 0 10 9 186.696 6.16480 8 0 10 -9 193.857 6.25641 8 0 10 -9 192.813 6.54809 5 0 10 -9 192.857 6.61016 6 0 10 9 187.082 6.69564 6 0 10 9 191.457 6.47634 2 0 10 9 186.232 6.42385 5 0 -10 9 194.907 5.92175 4 0 10 9 186.642 6.30205 11 0 10 9 188.726 6.18743 7 -1 10 9 364.430 11.3773 2 -1 10 9 355.747 10.9783 7 -1 -10 -9 342.895 10.5352 4 -1 10 9 358.148 10.8976 8 1 10 -9 362.026 11.0497 8 -1 10 9 366.715 11.2122 11 1 10 -9 362.362 11.3861 5 -1 10 9 378.743 11.2602 5 -1 10 -9 370.735 11.4796 5 1 10 9 349.436 11.1442 11 -1 -10 9 359.635 10.7806 4 1 10 9 365.126 11.2983 2 -1 10 -9 369.943 11.1792 8 -1 10 -9 343.840 10.9544 2 1 10 9 381.836 11.6913 6 -1 10 -9 369.553 11.3645 6 2 10 -9 385.615 12.1107 8 -2 10 9 413.450 12.5946 2 -2 10 9 405.840 12.2446 5 -2 10 9 399.978 12.1697 7 -2 10 9 410.710 12.4471 11 -2 -10 -9 394.378 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2.77306 2 -4 4 -10 64.9469 3.46482 9 -4 -4 10 61.8962 2.30421 7 -4 4 -10 66.3722 2.39737 7 -4 4 -10 65.0694 2.43482 3 -4 -4 10 65.3149 2.63212 4 -5 -4 -10 182.018 7.40480 9 -5 -4 -10 186.881 6.02079 3 -5 4 -10 181.393 5.82544 3 -5 -4 10 184.090 6.25276 3 -5 4 -10 186.585 7.15243 9 5 4 10 185.982 5.97261 11 5 -4 -10 188.729 6.21982 3 -6 -4 -10 36.8473 1.62303 3 -6 -4 -10 36.4594 2.38961 9 -6 4 -10 32.9527 2.43240 9 6 -4 -10 34.2756 1.61753 3 -6 -4 10 35.3420 1.68283 3 6 4 10 34.9297 1.47435 11 -7 -4 -10 25.4900 1.00534 3 -7 -4 -10 22.3192 1.33325 9 7 -4 -10 22.1951 0.93945 3 -7 -4 10 22.0986 0.93775 3 0 5 10 68.8455 2.38963 7 0 -5 10 71.3167 2.39490 4 1 -5 10 899.241 26.0813 4 -1 5 10 922.114 26.0470 7 1 5 10 918.213 26.1202 7 -1 -5 10 905.150 26.0718 4 -2 5 10 628.748 17.6803 7 -2 5 10 601.415 18.1204 2 -2 -5 -10 614.645 17.7195 4 -2 5 10 590.749 17.9534 11 -2 5 -10 595.170 17.8357 9 -2 -5 10 583.456 16.5433 4 -2 5 -10 514.027 16.8449 2 2 5 10 579.168 16.6328 11 -3 -5 -10 44.1594 2.00080 4 -3 5 10 45.6071 2.16485 11 -3 -5 -10 45.1342 1.89683 3 -3 5 10 48.3750 1.91763 7 -3 5 10 46.1374 2.11152 2 3 -5 -10 44.3868 1.99875 3 -3 5 -10 49.8155 2.76363 9 -3 5 -10 46.4678 2.11540 2 -3 -5 10 44.4338 1.90770 4 3 5 10 45.2115 1.91824 11 -3 5 -10 40.8643 1.69795 3 -4 -5 -10 361.061 11.2370 4 -4 -5 -10 365.907 11.0171 3 -4 5 10 361.506 11.0020 7 -4 5 10 362.154 11.1824 2 -4 5 10 363.911 11.4006 11 4 5 10 374.896 11.2957 11 -4 -5 10 367.977 11.3862 4 4 -5 -10 374.480 11.4955 3 -4 5 -10 373.622 12.5695 9 -4 5 -10 373.620 11.5534 2 -5 5 10 0.17459 0.28317 2 -5 -5 -10 0.52761 0.34236 3 5 5 10 1.06346 0.35178 11 -5 5 -10 0.60353 0.41075 9 5 -5 -10 0.07893 0.34367 3 -5 -5 10 -0.3493 0.31052 3 6 5 -10 44.0851 2.34575 6 -6 -5 -10 50.1417 2.76211 9 -6 -5 -10 50.5197 1.94155 3 -6 -5 10 51.5669 2.11426 3 -6 5 -10 47.9431 2.30666 9 6 5 10 49.2688 1.88169 11 6 -5 -10 51.2784 2.05177 3 -7 -5 -10 4.04692 0.53009 9 0 6 10 138.446 4.54032 7 0 -6 10 149.040 4.51849 4 1 -6 10 1410.25 39.4094 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87.4010 3.23002 2 -5 -6 10 88.6432 3.38842 3 5 -6 -10 85.7146 3.28649 3 5 6 10 89.3539 3.20966 11 -5 6 -10 83.6029 3.87669 9 -5 6 -10 90.6460 3.41885 2 -6 -6 -10 106.094 4.27447 9 -6 -6 -10 107.003 3.31561 3 6 6 -10 81.8542 3.48406 6 6 6 10 109.154 3.68798 11 -6 -6 10 112.342 3.87131 3 6 -6 -10 122.984 3.85275 3 0 7 10 125.768 4.10969 7 0 7 10 123.355 4.55730 6 0 7 10 122.832 4.25152 11 0 -7 10 130.091 4.03543 4 0 7 -10 121.551 4.36683 5 -1 7 10 944.392 27.9451 11 -1 7 10 1014.37 27.7508 7 1 -7 10 944.324 27.6784 4 1 7 -10 957.565 28.0464 5 -1 7 10 963.322 28.0665 2 1 7 10 953.962 28.3918 2 1 7 10 998.116 28.7221 6 1 7 10 978.320 28.2453 7 1 7 10 951.849 28.2955 11 -1 -7 10 1022.81 28.1229 4 2 7 -10 41.4242 1.85741 8 -2 -7 -10 45.3089 1.82011 4 -2 7 10 46.0099 2.09708 11 2 7 -10 37.1229 2.16417 5 -2 7 10 45.0941 2.10767 2 2 7 10 44.6632 1.97307 11 -2 -7 10 45.0633 1.84814 4 2 7 10 44.7882 1.99773 2 -2 7 -10 44.1750 2.02007 2 2 7 10 47.1566 2.19921 6 -3 7 10 6.93766 0.92550 11 -3 -7 -10 7.62575 0.75152 4 -3 7 10 10.1611 0.97129 2 -3 -7 -10 7.64939 0.67026 3 -3 7 10 9.09238 0.74565 7 3 7 10 8.23912 0.78649 6 3 -7 -10 9.95247 0.98070 3 3 7 10 7.90630 0.79564 11 -3 -7 10 7.62113 0.73333 4 -3 7 -10 9.06656 0.98086 2 -3 7 -10 8.41737 1.15731 9 -4 7 10 197.573 6.61874 11 -4 7 10 191.685 6.28114 7 -4 -7 -10 193.456 6.15527 3 -4 7 10 192.960 6.47162 2 -4 -7 -10 187.429 6.37105 4 4 -7 -10 192.666 6.41004 3 4 7 10 195.819 6.29770 2 -4 -7 10 196.962 6.41852 4 4 7 10 195.291 6.36604 11 -4 7 -10 197.909 6.57410 2 -5 -7 -10 21.8773 1.17380 3 -5 7 10 24.0412 1.26726 2 -5 -7 -10 21.4920 1.89873 9 5 -7 -10 23.9223 1.31264 3 -5 -7 10 21.9369 1.33465 3 -5 7 -10 24.6145 1.45000 2 5 7 10 23.0447 1.26004 11 -6 -7 -10 200.875 5.99977 3 6 7 -10 197.560 5.95578 11 -6 -7 -10 194.743 6.86458 9 6 7 10 198.122 6.00084 11 6 -7 -10 200.030 6.05545 3 -6 -7 10 195.750 6.11585 3 0 8 -10 31.2112 1.66844 5 0 8 10 31.1976 1.68479 2 0 8 10 30.9131 1.81034 6 0 8 10 32.6298 1.50181 7 0 -8 10 32.4556 1.39218 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317.736 11.8907 5 1 10 -11 352.945 10.7385 8 1 10 -11 351.929 11.2621 6 -1 10 11 362.027 10.9650 11 -1 10 11 356.336 10.7471 7 -1 10 11 362.505 11.1326 2 -1 -10 -11 337.116 10.3388 4 1 10 11 360.075 11.6968 6 -1 10 -11 371.045 11.3738 6 1 10 11 368.012 11.4223 2 -1 10 -11 379.175 11.5624 5 1 10 11 360.740 11.2949 11 -1 -10 11 360.748 10.9617 4 -2 10 11 339.808 10.5996 2 -2 -10 -11 302.123 10.2186 4 -2 10 11 325.588 10.1911 7 -2 10 11 340.854 10.4733 11 2 10 -11 349.471 10.4847 5 2 10 -11 334.091 10.1156 8 -2 -10 11 336.096 10.1984 4 2 10 11 335.723 10.7853 6 -2 10 -11 347.678 10.7425 5 2 10 11 341.728 10.4641 11 2 10 11 337.637 10.5070 2 -2 10 -11 327.618 10.2905 2 -3 10 11 101.028 3.84964 2 -3 10 11 101.197 3.79401 11 3 10 -11 94.7723 3.30567 8 -3 -10 -11 97.8730 4.10975 9 3 10 11 98.3358 3.58089 11 -3 10 -11 96.5511 3.54904 2 -3 10 -11 97.5456 3.80624 5 3 10 11 96.6518 3.51463 2 -4 10 11 49.1866 2.14500 2 4 10 -11 48.3269 2.33020 6 -4 10 11 48.3375 2.13764 11 -4 -10 -11 48.4359 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0.23527 3 -3 0 12 0.60720 0.22020 7 -4 0 -12 34.4212 2.47425 9 4 0 -12 33.1686 1.73060 3 -4 0 -12 32.0088 1.77297 4 -4 0 -12 32.2316 1.57835 3 -4 0 12 32.1231 1.44038 7 5 0 -12 58.6254 2.48192 3 -5 0 -12 54.7485 3.34595 9 -5 0 12 59.8824 2.50132 3 -5 0 -12 54.5677 2.29231 3 -6 0 -12 7.51459 1.09199 9 -6 0 12 7.73616 0.69183 3 6 0 -12 7.96069 0.71982 3 -6 0 -12 7.38630 0.65572 3 -7 0 -12 5.85817 0.61278 9 -7 0 -12 7.55655 0.45514 3 0 1 12 115.496 3.43557 7 0 -1 12 107.883 3.59389 4 0 1 12 115.205 3.59035 4 -1 1 12 2085.94 59.0389 4 1 -1 12 2090.84 59.1257 4 -1 -1 12 2145.33 60.3497 7 -2 1 12 1909.04 54.6178 7 -2 1 12 1950.93 54.7904 4 -2 -1 -12 1939.87 54.9530 4 -2 1 -12 1973.57 56.3326 4 -2 -1 12 1984.47 55.9173 7 -2 -1 12 1990.25 56.2298 4 -3 -1 -12 1.94020 0.73774 9 -3 1 12 2.16655 0.49267 11 -3 -1 -12 1.85536 0.41646 3 -3 1 12 1.26143 0.27177 4 -3 -1 -12 1.94759 0.42948 4 3 1 -12 2.61695 0.49782 3 -3 1 -12 1.85857 0.37066 3 3 -1 -12 3.15728 0.58895 3 -3 -1 12 2.26362 0.31893 7 -3 1 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139.322 4.54032 4 -2 2 12 137.622 4.28774 7 -2 2 12 136.595 4.35829 4 -2 2 -12 136.068 4.43439 4 -2 -2 12 133.381 4.34157 4 -2 -2 12 133.518 3.98486 7 -3 -2 -12 503.939 15.9544 9 -3 -2 -12 473.320 14.5105 3 -3 2 12 490.189 14.3643 7 -3 -2 -12 503.826 14.7454 4 3 2 -12 489.475 14.6254 3 -3 -2 12 493.417 14.3722 4 3 -2 -12 482.637 14.4999 3 -3 2 -12 505.120 15.7179 9 -3 2 -12 471.685 14.4899 4 -3 2 -12 472.859 14.2521 3 -3 -2 12 482.487 13.9812 7 -4 -2 -12 373.515 11.8341 4 4 2 -12 361.090 11.2554 3 -4 2 12 380.549 11.4494 3 -4 -2 -12 375.275 12.7489 9 -4 -2 -12 366.725 11.2016 3 -4 2 12 368.763 11.5303 11 -4 2 12 360.686 11.0690 7 -4 2 -12 372.029 10.9140 7 -4 2 -12 369.530 10.9583 3 -4 2 -12 368.956 12.5247 9 -4 -2 12 358.521 11.1524 4 -4 -2 12 351.405 10.7419 7 4 -2 -12 358.182 11.2322 3 4 2 12 365.312 10.8693 11 -5 -2 -12 780.520 22.9279 3 -5 -2 -12 801.876 24.6889 9 -5 2 12 792.394 22.8885 3 5 2 -12 771.415 22.8867 3 -5 -2 12 770.667 22.9426 3 -5 2 -12 774.588 22.5831 3 5 -2 -12 791.387 22.9293 3 5 2 12 779.461 22.4851 11 -5 2 -12 777.114 24.2330 9 -6 2 12 74.0792 2.49050 3 -6 -2 -12 79.5603 2.79782 3 -6 -2 -12 78.8392 3.75495 9 6 2 -12 76.9773 2.69548 3 -6 -2 12 81.1724 2.97962 3 -6 2 -12 78.9335 2.87976 3 6 -2 -12 80.1457 2.94853 3 -6 2 -12 78.1457 3.63812 9 -7 -2 -12 4.44242 0.56369 9 -7 -2 -12 4.59707 0.36364 3 7 -2 -12 4.45866 0.33360 3 -7 -2 12 4.05198 0.30898 3 0 -3 12 250.897 7.40626 4 0 3 12 241.344 7.27479 7 -1 3 12 522.289 15.1783 7 1 -3 12 531.025 15.3396 4 -1 3 -12 543.816 15.5013 4 -1 -3 12 520.900 15.4539 4 -2 3 12 206.256 6.83995 11 -2 -3 -12 221.836 6.73584 4 -2 3 -12 211.119 6.63157 4 -2 3 -12 213.961 6.13775 7 -2 3 -12 210.042 7.60199 9 -3 3 12 697.809 24.2619 2 3 3 -12 812.225 23.5930 3 -3 3 12 826.536 23.4337 7 -3 -3 -12 831.997 23.7648 4 -3 -3 -12 833.541 23.5695 3 -3 -3 -12 871.801 25.0997 9 -3 3 -12 830.579 23.2151 7 -3 3 -12 800.673 23.4017 3 -3 -3 12 821.445 23.5767 4 -3 3 -12 837.526 24.9552 9 3 -3 -12 788.547 23.6793 3 3 3 12 798.354 23.4881 11 -3 -3 12 803.121 23.0983 7 -4 -3 -12 62.2959 2.72686 4 -4 -3 -12 64.2694 3.63240 9 4 3 -12 61.5976 2.47838 3 -4 3 12 61.2293 2.42471 3 -4 3 12 60.7359 2.40224 7 -4 -3 -12 62.6206 2.50624 3 -4 3 12 62.1003 2.77792 11 4 -3 -12 61.0480 2.65504 3 4 3 12 58.9808 2.34575 11 -4 3 -12 60.0373 2.34973 3 -4 3 -12 64.3847 3.53893 9 -4 -3 12 62.4598 2.58762 4 -4 3 -12 62.0813 2.37788 7 5 3 -12 160.341 5.12940 3 -5 3 12 155.863 4.89095 3 -5 -3 -12 144.337 7.48650 9 5 3 12 162.772 5.05657 11 -5 3 -12 162.411 5.17811 3 -5 3 -12 142.748 7.50435 9 -6 -3 -12 7.41345 0.66673 3 -6 -3 -12 5.95272 0.98881 9 -6 3 -12 6.14832 0.44033 3 -6 3 -12 7.00525 1.03327 9 -6 -3 12 6.62083 0.71974 3 6 -3 -12 5.42104 0.65453 3 -7 -3 -12 24.1242 0.91996 3 -7 -3 -12 23.1620 1.26536 9 7 -3 -12 22.5915 0.86759 3 -7 -3 12 22.5539 0.85885 3 0 4 12 328.938 9.56963 7 0 -4 12 321.036 9.63860 4 -1 4 12 294.723 8.86972 7 1 -4 12 304.942 9.07818 4 -1 -4 12 305.685 9.02374 4 1 4 12 293.347 8.91542 7 -2 -4 -12 78.2583 3.00810 3 -2 -4 -12 83.7428 2.98249 4 -2 4 12 82.5722 2.81951 7 -2 -4 12 79.0097 2.79565 4 2 4 12 80.5919 2.83252 11 2 -4 -12 75.9668 2.90861 3 -2 4 -12 70.9247 4.68176 9 -2 4 -12 81.2864 2.95129 2 -3 -4 -12 140.005 4.76131 4 -3 4 12 135.624 4.73512 2 -3 4 12 139.355 4.88635 11 -3 4 12 136.205 4.49899 7 3 4 -12 137.051 4.54502 3 -3 -4 -12 134.989 4.56233 3 -3 4 -12 141.896 4.81132 2 -3 -4 12 139.906 4.65932 4 -3 4 -12 135.711 4.42396 3 3 -4 -12 137.232 4.77696 3 -3 4 -12 137.350 5.72955 9 3 4 12 135.948 4.55660 11 -4 -4 -12 104.853 3.70348 3 -4 4 12 100.761 3.67365 2 4 4 -12 100.131 3.54565 3 -4 -4 -12 101.293 3.92613 4 -4 4 12 106.080 4.03392 11 -4 4 12 102.729 3.63956 7 -4 -4 -12 106.568 4.96863 9 -4 4 -12 104.517 4.82343 9 4 -4 -12 102.528 3.87138 3 -4 -4 12 102.663 3.80236 4 4 4 12 101.885 3.61276 11 -4 4 -12 103.392 3.48228 3 -5 -4 -12 152.203 5.04590 3 5 4 -12 146.710 4.67974 3 -5 -4 -12 154.935 6.40051 9 -5 -4 12 161.107 5.43959 3 -5 4 -12 153.104 6.24402 9 5 4 12 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4.16448 9 3 5 12 84.2092 3.07346 11 -3 5 -12 79.4615 2.82285 3 -3 -5 12 86.4638 3.12824 4 -3 5 -12 85.7659 3.26980 2 -4 -5 -12 333.596 10.0068 3 -4 5 12 319.667 10.0661 2 -4 -5 -12 329.626 11.4835 9 -4 -5 -12 320.921 10.2657 4 -4 5 12 318.638 9.98201 7 -4 5 12 334.678 10.3976 11 -4 5 -12 337.272 10.4178 2 -4 5 -12 325.660 9.80518 3 4 5 12 330.395 10.1456 11 -4 -5 12 327.544 10.3210 4 -4 5 -12 343.096 11.6083 9 4 -5 -12 332.046 10.3907 3 -5 -5 -12 163.682 6.65695 9 -5 -5 -12 165.804 5.39107 3 -5 -5 12 169.699 5.70804 3 5 5 12 164.843 5.37209 11 5 -5 -12 169.316 5.65172 3 -5 5 -12 165.732 6.47783 9 -6 -5 -12 28.6704 1.26284 3 6 5 -12 24.6084 1.17876 6 -6 -5 -12 27.6410 1.83994 9 6 -5 -12 29.0492 1.37940 3 -6 -5 12 30.1091 1.42215 3 6 5 12 28.7951 1.47921 2 0 6 12 34.5634 1.64930 2 0 6 12 31.9228 1.58315 11 0 6 12 33.7907 1.44952 7 0 -6 12 30.8300 1.40877 4 -1 6 12 69.5724 2.78312 2 1 -6 12 67.1921 2.51529 4 -1 6 12 65.6106 2.67669 11 -1 6 12 70.3823 2.50369 7 -1 -6 12 69.9549 2.52812 4 1 6 12 64.6998 2.61565 11 1 6 12 71.7337 2.59331 7 1 6 12 72.2672 2.74174 2 -2 -6 -12 76.7388 2.84565 3 -2 -6 -12 83.1675 2.96253 4 -2 6 12 79.6030 3.17964 2 -2 6 12 80.5274 3.15680 11 2 6 12 79.5896 2.93619 11 -2 6 -12 82.0001 3.91650 9 -2 -6 12 76.5336 2.84733 4 -2 6 -12 74.4340 2.96703 2 2 -6 -12 77.7290 2.96735 3 -3 -6 -12 42.1247 2.17623 3 -3 6 12 46.8231 2.17465 2 -3 6 12 43.1877 2.17051 11 -3 -6 -12 43.1820 2.03840 4 -3 6 12 44.4974 1.90704 7 3 -6 -12 43.0632 2.15496 3 3 6 12 44.8393 1.98019 11 -3 6 -12 44.9083 2.13157 2 -3 -6 12 44.1410 1.97426 4 -3 6 -12 47.0626 2.88392 9 -4 -6 -12 47.1135 1.99039 3 -4 6 12 44.3349 2.01046 7 -4 6 12 46.5732 2.11955 2 -4 -6 -12 46.1105 2.91990 9 -4 -6 -12 45.1455 2.18607 4 -4 6 12 45.5995 2.29076 11 -4 -6 12 45.3955 2.09687 4 -4 6 -12 44.7882 2.19027 2 -4 6 -12 46.7260 2.85444 9 4 6 12 44.8545 1.99298 11 4 -6 -12 45.3204 2.13388 3 -5 -6 -12 52.6457 2.99648 9 -5 -6 -12 51.0339 2.04643 3 -5 6 12 46.4957 2.00712 2 -5 6 -12 50.3091 2.73398 9 -5 -6 12 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4 -1 8 -12 419.742 12.2643 5 -1 8 -12 392.247 12.0109 2 1 8 12 341.518 13.0211 6 1 8 12 403.415 12.6447 11 -2 8 12 1762.39 49.1840 2 -2 -8 -12 1697.51 48.6859 4 -2 8 12 1738.63 49.0775 11 -2 8 12 1678.43 48.7206 7 2 8 -12 1659.02 48.6477 8 -2 -8 12 1750.56 49.0881 4 2 8 12 1650.66 49.5103 6 2 8 12 1738.03 49.3308 2 2 8 12 1742.83 49.2388 11 -2 8 -12 1720.32 49.1871 2 -3 -8 -12 255.511 8.07143 3 -3 8 12 265.447 8.59012 11 -3 -8 -12 263.809 8.36236 4 -3 -8 -12 266.351 9.28611 9 -3 8 12 255.752 8.25190 7 -3 8 12 277.351 8.66199 2 3 -8 -12 262.018 8.31116 3 3 8 12 268.830 8.37535 11 -3 -8 12 265.342 8.38704 4 -3 8 -12 267.049 8.41426 2 3 8 12 259.954 8.35219 2 4 8 -12 116.431 3.79567 11 -4 -8 -12 117.462 4.98349 3 -4 8 12 115.183 4.20375 2 -4 -8 -12 117.469 5.03402 9 -4 8 12 118.349 4.33485 11 -4 8 -12 113.732 4.09556 2 4 8 12 111.648 3.92168 2 4 -8 -12 109.198 3.96086 3 4 8 12 118.368 4.01356 11 -5 -8 -12 18.8666 1.51803 9 5 8 -12 19.6168 1.25975 6 5 8 -12 19.1298 0.91481 11 -5 -8 -12 18.9852 0.96770 3 -5 8 12 20.0732 1.00031 2 -5 -8 12 19.7210 1.15522 3 5 -8 -12 21.0490 1.09376 3 5 8 12 20.5119 1.08016 11 -6 -8 -12 172.803 5.59614 9 -6 -8 -12 178.016 5.26774 3 6 -8 -12 207.219 6.18758 3 -6 -8 12 190.194 5.88444 3 0 9 12 1019.79 29.8596 2 0 -9 12 1018.44 29.4049 4 0 9 -12 1018.78 29.8137 5 0 9 12 1002.91 29.5449 7 0 9 12 1047.34 29.7283 11 -1 9 12 64.9518 2.54204 7 -1 9 12 64.2733 2.73265 11 1 9 -12 60.6628 2.54855 8 -1 -9 -12 63.0170 2.34025 4 -1 9 12 63.5572 2.84507 2 1 -9 12 62.9227 2.50053 4 1 9 -12 62.7222 2.68131 5 -1 9 -12 67.6347 3.83577 6 1 9 12 62.6218 2.72870 2 -1 9 -12 61.2946 2.73395 5 1 9 12 60.4948 2.60613 11 -1 -9 12 60.0938 2.37264 4 -2 9 12 351.845 10.6804 11 -2 -9 -12 336.484 10.2620 4 2 9 -12 333.850 10.4980 5 -2 9 12 345.780 10.7662 2 2 9 -12 330.362 10.2458 8 -2 9 12 329.835 10.3375 7 2 9 12 345.966 10.6046 2 2 9 12 340.469 10.4963 11 -2 9 -12 327.388 10.4137 2 -2 -9 12 340.482 10.3398 4 -2 9 -12 343.830 10.7461 5 -3 9 12 80.7928 3.40874 2 -3 9 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118.485 4.06887 10 2 -4 -20 117.595 4.24800 3 2 4 20 115.610 3.96672 10 -2 -4 20 119.388 4.05500 10 -2 -4 20 108.784 4.97347 4 -2 4 -20 122.062 3.94760 3 3 4 -20 155.417 4.91769 3 -3 -4 -20 148.757 5.84627 9 -3 4 20 155.073 5.28391 11 -3 -4 -20 159.517 5.12995 3 3 -4 20 154.887 5.06760 10 3 -4 -20 162.728 5.48176 3 -3 4 -20 157.489 5.01652 3 4 -4 20 52.8153 2.03809 10 -4 -4 -20 54.6211 2.12468 3 4 -4 -20 55.8581 2.32859 3 5 -4 20 2.60572 0.32478 10 -5 -4 -20 1.61109 0.52911 9 5 4 20 1.90097 0.33933 2 -5 -4 20 2.61187 0.40349 3 5 -4 -20 2.55516 0.42001 3 0 -5 20 155.187 5.13256 10 0 5 20 156.289 5.21473 11 0 5 20 160.930 5.33656 2 0 -5 -20 151.742 5.17990 3 0 5 -20 148.404 4.90027 3 -1 5 20 60.3670 2.57821 2 1 5 -20 62.4255 2.31391 3 1 -5 20 63.3756 2.50943 10 1 -5 20 61.7393 2.73084 4 -1 -5 -20 63.2925 2.52259 3 -1 5 20 62.4213 2.61394 11 1 -5 -20 65.6669 2.68437 3 -1 5 -20 64.7279 2.38955 3 -1 -5 20 64.0193 2.76955 4 1 5 20 66.0732 2.58887 11 1 5 20 64.2159 2.72561 2 1 5 20 64.8701 2.58046 10 -1 -5 20 73.2515 2.64951 10 -2 5 20 19.2185 1.31184 11 -2 -5 -20 18.9735 1.41148 3 -2 5 20 18.6276 1.11975 2 -2 5 -20 20.9385 1.01869 3 -2 -5 20 20.7942 1.13084 10 2 5 20 18.8138 1.08593 11 2 -5 -20 21.7043 1.47825 3 -3 -5 -20 26.4573 1.38086 3 -3 5 20 26.9959 1.51796 11 -3 -5 -20 27.6339 1.80095 9 3 -5 20 28.2220 1.38649 10 3 -5 -20 29.1825 1.58157 3 -4 -5 -20 40.1570 2.12081 9 4 -5 20 42.3079 1.82245 10 -4 -5 -20 45.4653 2.02983 3 4 5 20 42.6117 1.83133 2 4 -5 -20 43.0652 1.92335 3 -5 -5 -20 21.3019 1.14513 9 -5 -5 -20 24.1637 0.99710 3 5 -5 20 22.9586 0.87593 10 -5 -5 20 22.3418 1.01625 3 5 -5 -20 23.2374 1.03176 3 5 5 20 20.1593 1.24792 2 0 6 20 0.76405 0.39806 11 0 -6 20 0.94507 0.41938 10 0 -6 -20 0.93004 0.37141 3 0 6 20 1.12531 0.42886 2 1 -6 20 56.9936 2.42342 10 1 6 -20 56.8535 2.09436 8 -1 6 20 46.5954 3.10490 11 -1 -6 20 64.4527 3.15255 10 1 6 20 61.0829 2.67105 2 1 6 20 56.9862 2.47082 11 -2 6 20 71.3837 2.89559 11 -2 6 20 68.6850 2.75341 2 -2 -6 -20 74.6419 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263.399 8.06879 2 -1 10 20 265.904 8.05859 11 1 10 -20 251.217 7.96806 6 -1 10 -20 266.791 8.07181 8 1 10 20 266.872 8.25434 2 1 10 20 265.639 8.15161 11 -2 10 20 76.2323 2.73172 2 2 -10 20 79.5219 2.61370 10 2 10 -20 79.0832 2.87775 6 -2 10 20 77.6837 2.81279 11 2 10 20 79.3350 2.76223 11 2 10 20 78.8576 2.86031 2 -2 10 -20 83.9199 2.82183 8 3 10 -20 83.3370 3.00771 6 3 -10 20 92.5048 2.81253 10 3 10 20 75.3314 3.02110 11 3 10 20 89.0421 2.74974 2 0 11 20 0.42681 0.31109 2 0 11 20 0.05229 0.28941 11 -1 11 20 92.8029 3.04821 11 1 -11 20 80.0136 2.84504 10 -1 11 20 89.8599 3.03982 2 -1 11 -20 96.3956 3.11617 8 1 11 20 96.0102 3.26097 2 1 11 20 92.9038 3.17099 11 -2 11 20 11.3818 0.63594 2 2 -11 20 10.0512 0.52076 10 2 11 -20 10.0224 0.61883 6 2 11 20 11.6724 0.80227 2 2 11 20 11.1362 0.62286 11 0 12 20 161.034 4.87220 11 0 12 20 156.533 4.89662 2 -1 12 20 17.5152 0.82851 11 -1 12 20 16.8005 0.80960 2 1 12 20 16.0552 0.76165 11 -1 12 -20 17.5789 0.73369 8 1 12 20 16.7306 0.81548 2 0 0 21 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10 0 3 21 130.400 4.54807 2 0 3 -21 131.022 4.47307 3 0 -3 -21 132.768 4.59112 3 -1 3 21 85.1032 3.27486 10 -1 -3 -21 82.2298 3.16367 3 -1 3 21 79.6844 3.07816 2 1 -3 21 85.9490 3.15881 10 1 3 -21 85.2724 3.13651 3 -1 3 21 82.9807 3.12979 11 1 3 21 86.3921 3.18635 10 1 3 21 82.9847 3.21121 2 1 -3 -21 85.6233 3.28099 3 -1 -3 21 85.0682 3.19500 10 -1 3 -21 83.7691 3.10302 3 -2 -3 -21 141.341 5.41547 9 -2 -3 -21 136.040 4.68068 3 2 -3 21 139.352 4.66403 10 2 3 -21 132.839 4.76853 3 2 -3 -21 148.302 5.01820 3 2 3 21 141.356 5.01963 10 -2 3 -21 140.020 4.74731 3 -3 -3 -21 323.893 11.0144 9 3 -3 21 335.714 10.0773 10 3 3 -21 329.531 10.0256 3 -3 3 21 334.373 10.2077 11 -3 -3 -21 339.637 10.1377 3 3 3 21 322.447 9.93803 10 3 -3 -21 349.772 10.4503 3 -3 3 -21 339.723 11.6246 9 -3 3 -21 331.645 10.0368 3 4 3 -21 95.1590 3.08559 3 -4 -3 -21 97.5055 4.02866 9 -4 -3 -21 97.7558 3.33856 3 4 -3 -21 100.888 3.52827 3 -4 3 -21 93.7748 4.27809 9 -4 3 -21 99.2624 3.14532 3 -5 -3 -21 139.389 4.27177 3 -5 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185.790 5.79741 3 3 -4 -21 194.088 6.26846 3 4 -4 21 155.839 4.93591 10 -4 -4 -21 156.270 5.63089 9 -4 -4 -21 161.361 5.41366 3 4 -4 -21 167.769 5.66303 3 -5 -4 -21 7.03189 0.61387 9 -5 -4 -21 8.55878 0.55389 3 5 -4 -21 8.57877 0.58324 3 5 4 21 7.20441 0.76251 2 0 5 21 187.506 6.19237 2 0 -5 -21 185.949 6.10751 3 0 -5 21 186.137 6.04397 10 -1 5 21 352.669 11.1165 11 1 5 -21 339.783 10.6987 3 -1 5 21 350.294 11.1107 2 1 -5 21 382.653 11.3330 10 -1 -5 -21 396.323 11.8516 3 1 5 21 350.660 10.9002 11 -1 -5 21 375.135 11.3784 10 -1 5 -21 359.857 10.6689 3 2 -5 21 124.252 4.16246 10 -2 -5 -21 124.795 4.17741 3 -2 5 21 117.615 4.09311 2 -2 5 21 115.764 4.24468 11 2 -5 -21 122.385 4.16388 3 2 5 21 97.1854 3.89478 11 2 5 21 119.506 4.14161 2 -2 -5 21 121.330 3.92980 10 3 -5 21 47.7583 1.95604 10 -3 -5 -21 47.5609 1.96731 3 -3 5 21 47.7819 2.08542 11 -3 -5 -21 46.3035 2.28949 9 3 5 21 48.6347 2.10737 2 3 -5 -21 47.6064 2.13174 3 -4 -5 -21 13.8593 0.82915 3 -4 -5 -21 12.1837 1.05864 9 4 -5 21 14.4657 0.79493 10 4 5 21 13.2203 0.87082 2 4 -5 -21 13.1750 0.88129 3 -5 -5 -21 26.8213 1.04936 3 -5 -5 21 24.7912 1.02560 3 5 5 21 25.9207 1.02287 2 5 -5 -21 25.7267 1.03326 3 0 6 21 271.480 8.45880 2 0 -6 -21 265.544 8.29103 3 0 -6 21 264.644 8.21612 10 0 6 21 259.009 8.29593 11 1 -6 21 351.719 10.4244 10 -1 -6 -21 342.065 10.4236 3 -1 6 21 335.057 10.5361 2 -1 6 21 343.196 10.5609 11 1 6 21 335.608 10.3449 11 -1 -6 21 337.433 10.2875 10 1 -6 -21 343.358 10.4630 3 1 6 21 347.309 10.5866 2 2 -6 21 16.4063 1.03653 10 -2 6 21 16.6814 1.07865 2 -2 6 21 15.0467 1.11692 11 -2 -6 -21 18.0985 1.07019 3 2 6 21 16.3705 1.14628 2 2 6 21 17.0569 0.99293 11 2 -6 -21 16.5638 1.13454 3 -2 -6 21 17.8460 0.96249 10 3 -6 21 108.902 3.62600 10 -3 -6 -21 106.562 3.61342 3 -3 6 21 105.434 3.77090 11 3 6 21 112.434 3.89546 2 3 -6 -21 110.366 3.88047 3 4 -6 21 12.3026 0.73283 10 -4 -6 -21 15.0149 0.79794 3 4 -6 -21 14.4173 0.86213 3 4 6 21 13.3013 0.83132 2 0 7 21 18.5893 1.19549 11 0 7 21 17.3054 1.25039 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116.110 4.27468 3 -2 8 21 87.8522 3.16775 2 2 -8 21 88.2408 3.09671 10 -2 8 21 98.4961 3.58208 11 -2 -8 -21 87.0400 3.04342 3 2 8 21 86.4139 3.02321 11 2 -8 -21 86.6074 3.08251 3 2 8 21 90.9407 3.26291 2 -3 8 21 275.722 8.42356 11 3 -8 21 278.794 8.27591 10 3 8 21 283.795 8.02845 2 3 8 21 222.175 7.87185 11 3 -8 -21 280.216 7.90227 3 4 8 -21 7.34953 0.58949 6 4 -8 21 9.28087 0.50742 10 4 8 21 8.86364 0.52344 2 -4 -8 21 8.15212 0.51883 3 0 9 21 11.8539 0.94889 2 0 9 -21 11.0168 0.74796 8 0 -9 21 10.8573 0.70135 10 0 -9 -21 9.06234 0.69603 3 1 -9 21 76.0983 2.59778 10 -1 -9 -21 72.8366 3.00926 3 -1 9 21 75.2856 2.85570 11 -1 9 21 76.2243 2.82591 2 1 9 -21 70.9887 2.76090 6 1 9 21 77.2597 2.91039 2 1 -9 -21 74.6148 2.64962 3 -1 9 -21 77.7121 2.75152 8 1 9 21 75.2721 2.76428 11 -2 -9 -21 62.9090 2.09423 3 2 -9 21 59.3371 2.16307 10 -2 9 21 62.1510 2.35338 11 -2 9 21 57.9017 2.21961 2 2 -9 -21 58.9815 2.08085 3 2 9 21 57.2734 2.10080 11 2 9 21 58.4906 2.28132 2 3 9 -21 22.1763 1.18632 6 -3 9 21 23.9922 1.10322 11 3 -9 21 23.0115 0.99639 10 3 9 21 23.3456 1.08852 2 0 10 -21 250.342 7.47574 8 0 10 21 253.796 7.69026 11 0 10 21 249.783 7.76164 2 -1 10 21 83.2816 2.82906 11 1 -10 21 74.9447 2.71455 10 1 10 -21 75.4942 2.64050 6 -1 10 21 80.7644 2.82688 2 1 10 21 84.6367 2.97258 2 1 10 21 80.7592 2.84092 11 -1 10 -21 82.2759 2.80098 8 -2 10 21 105.948 3.42282 11 -2 10 21 101.894 3.31086 2 2 10 -21 100.060 3.41507 6 2 10 21 103.898 3.35783 11 -2 10 -21 109.252 3.44536 8 2 10 21 106.072 3.52184 2 0 11 21 584.798 16.7109 2 0 11 21 566.597 17.0962 11 -1 11 21 283.444 8.49176 11 -1 11 21 276.217 8.42846 2 1 11 21 250.077 7.46942 11 1 11 21 248.170 7.56707 2 -1 11 -21 257.536 7.42412 8 -2 11 21 51.3214 1.81619 11 0 0 22 49.4354 2.15521 10 0 0 22 44.9018 1.89776 2 0 0 -22 46.8987 2.12314 3 1 0 -22 18.9016 1.26129 3 -1 0 22 19.5334 1.28963 10 1 0 22 19.9429 1.23929 10 -1 0 -22 21.4911 1.27546 3 -2 0 -22 174.660 6.72347 9 -3 0 -22 12.3445 1.37760 9 -3 0 -22 11.8025 0.92555 3 3 0 22 12.4194 0.85865 10 3 0 -22 12.2943 1.01369 3 -4 0 -22 110.035 4.99057 9 -4 0 22 113.125 3.74327 3 -4 0 -22 122.003 3.87061 3 4 0 22 114.920 3.64660 10 4 0 -22 122.737 4.08892 3 5 0 -22 3.46706 0.33982 3 -5 0 -22 3.94704 0.35959 3 -5 0 -22 4.30807 0.61522 9 0 -1 -22 17.9661 1.20260 3 0 1 22 16.4997 1.18297 10 0 -1 22 16.4628 1.15717 10 0 1 -22 16.5618 1.14666 3 0 1 22 17.5042 1.05187 2 -1 -1 -22 74.9019 2.90344 3 1 1 -22 77.4407 2.97449 3 1 -1 22 71.0491 2.87334 10 -1 1 22 74.6966 2.97352 10 -1 -1 22 74.8866 2.97171 10 1 1 22 78.1968 2.96651 10 -1 1 -22 74.4504 2.90985 3 -2 -1 -22 307.638 10.4522 9 -2 -1 22 341.474 10.8141 10 2 1 22 327.119 10.4880 10 -3 -1 -22 381.376 11.3697 3 -3 -1 -22 381.694 12.4683 9 3 -1 22 370.016 11.2782 10 3 1 -22 377.002 11.4474 3 3 1 22 373.602 11.4024 10 -3 1 -22 387.543 11.5022 3 3 -1 -22 385.016 11.7127 3 -3 1 -22 390.239 12.8129 9 -4 -1 -22 533.385 15.2271 3 4 1 -22 538.557 15.2445 3 4 -1 22 522.584 15.0652 10 -4 -1 -22 511.421 16.1822 9 -4 1 22 497.885 14.9233 3 -4 1 -22 541.603 16.1007 3 4 -1 -22 530.803 15.9339 3 -4 1 -22 554.978 17.0941 9 -5 -1 -22 8.40173 0.79166 9 5 -1 -22 9.00388 0.55314 3 0 2 22 615.000 18.3025 2 0 2 -22 633.492 18.3711 3 0 -2 -22 634.242 18.4522 3 0 -2 22 629.419 18.4139 10 0 2 22 602.459 18.4150 10 -1 2 22 534.364 15.5470 10 -1 -2 -22 498.923 16.5829 4 1 -2 22 515.894 15.3985 10 1 2 -22 514.062 15.3962 3 -1 -2 -22 520.631 15.4128 3 -1 -2 22 530.564 15.5066 10 1 2 22 510.623 15.4364 10 1 -2 -22 520.263 15.5527 3 -1 2 -22 514.301 15.4010 3 -2 -2 -22 247.438 7.60478 3 2 -2 22 240.128 7.54531 10 -2 -2 -22 238.452 8.35039 9 2 2 -22 238.705 7.57694 3 -2 2 22 233.045 7.44450 11 2 -2 -22 234.117 7.59308 3 -2 2 -22 237.502 7.37815 3 2 2 22 235.618 7.37747 10 -2 -2 22 235.139 7.48064 10 -3 -2 -22 2.95348 0.55479 3 3 2 -22 2.65297 0.52506 3 3 -2 22 2.79033 0.53316 10 -3 -2 -22 2.13901 0.67832 9 -3 2 -22 1.75815 0.41527 3 3 -2 -22 3.31594 0.59276 3 -3 2 -22 2.07542 0.77292 9 3 2 22 2.90304 0.47260 10 4 2 -22 34.5365 1.42282 3 4 -2 22 35.5952 1.43516 10 -4 -2 -22 37.2010 1.59875 3 -4 -2 -22 36.8041 2.09292 9 4 -2 -22 39.2570 1.78492 3 -4 2 -22 35.5229 1.44273 3 -5 -2 -22 10.1271 0.80482 9 5 -2 -22 11.1099 0.81268 3 -5 -2 22 11.3351 0.53826 3 0 3 22 1.65124 0.40586 2 0 3 22 1.09978 0.50536 10 0 3 -22 2.08377 0.48221 3 0 -3 -22 1.25223 0.44737 3 0 -3 22 1.44408 0.55178 10 -1 3 22 133.655 4.67466 2 -1 3 22 137.506 4.66056 11 1 3 -22 142.755 4.75943 3 -1 3 22 144.068 4.91067 10 -1 -3 -22 139.465 4.77809 3 1 -3 22 143.347 4.78107 10 -1 3 -22 141.580 4.69829 3 1 3 22 140.974 4.85596 2 1 3 22 132.141 4.73373 10 1 -3 -22 142.887 4.89007 3 -1 -3 22 145.562 4.82081 10 -2 -3 -22 79.3477 3.56022 9 -2 -3 -22 84.7462 3.13531 3 -2 3 22 81.1860 3.05953 11 2 3 -22 88.4093 3.08041 3 2 -3 22 82.6576 3.08693 10 -2 3 -22 85.8309 3.06917 3 2 -3 -22 85.1862 3.29818 3 2 3 22 83.8341 3.05719 10 -2 -3 22 88.2775 3.19784 10 3 3 -22 152.603 4.86470 3 3 -3 22 151.695 4.94109 10 -3 -3 -22 153.633 5.00794 3 -3 -3 -22 149.671 5.65772 9 -3 3 -22 156.169 4.85950 3 3 -3 -22 154.093 5.18567 3 3 3 22 148.930 4.75369 10 -4 -3 -22 34.1804 1.47190 3 4 -3 22 33.7239 1.37123 10 -4 -3 -22 32.7664 1.85973 9 4 -3 -22 37.8293 1.68505 3 -5 -3 -22 35.0769 1.22341 3 -5 -3 -22 28.4513 1.52545 9 -5 -3 22 33.7245 1.23102 3 5 3 22 36.2591 1.33840 2 5 -3 -22 35.1970 1.31926 3 0 -4 22 5.88873 1.31070 10 0 4 22 5.02677 0.74572 2 0 4 22 5.20944 0.90150 10 0 4 22 4.69846 0.64203 11 1 -4 22 50.1942 2.25931 10 1 4 -22 48.6990 1.98045 3 -1 4 22 49.3758 2.09472 2 -1 4 22 48.2264 2.09740 11 -1 -4 -22 49.3545 2.14002 3 1 4 22 48.7911 2.15414 2 1 4 22 48.9113 2.06597 10 -1 4 -22 47.0100 1.92519 3 1 -4 -22 46.8330 2.14812 3 -1 -4 22 48.1417 2.07815 10 2 -4 22 44.9591 1.94083 10 2 4 -22 43.4133 1.76106 3 -2 -4 -22 43.6804 1.94752 3 -2 4 22 42.3779 1.91470 11 -2 -4 22 44.4205 1.87887 10 -2 4 -22 44.2563 1.72857 3 2 4 22 43.1315 1.98266 2 2 4 22 40.1588 1.75069 10 2 -4 -22 42.4223 2.00744 3 -3 -4 -22 238.850 7.32851 3 -3 -4 -22 232.537 7.86995 9 -3 4 22 226.515 7.33693 11 3 -4 22 244.759 7.30254 10 3 -4 -22 238.939 7.54500 3 -3 4 -22 236.493 7.03750 3 -4 -4 -22 0.25347 0.38866 9 4 -4 22 0.33189 0.24421 10 -4 -4 -22 0.00414 0.24377 3 4 -4 -22 -0.1060 0.24175 3 4 4 22 0.47783 0.26748 2 0 -5 -22 1.63674 0.46847 3 0 5 22 1.14891 0.41822 2 0 -5 22 2.16685 0.50601 10 -1 5 22 227.604 7.32327 11 -1 -5 -22 236.843 7.33715 3 -1 5 22 227.859 7.32091 2 1 -5 22 234.371 7.30335 10 1 5 22 228.499 7.24562 11 1 5 22 241.776 7.53715 2 -1 -5 22 231.613 7.33514 10 1 -5 -22 236.421 7.49527 3 -2 5 22 42.6223 1.93735 11 -2 -5 -22 44.6944 1.91522 3 2 -5 22 43.2738 1.88335 10 2 -5 -22 44.1108 2.02188 3 2 5 22 44.1804 2.00495 2 -2 -5 22 44.0328 1.81485 10 3 -5 22 242.123 7.47877 10 -3 5 22 242.155 8.06975 11 -3 -5 -22 248.702 7.52787 3 3 -5 -22 249.590 7.76916 3 3 5 22 246.572 7.72644 2 4 -5 22 3.95390 0.43959 10 -4 -5 -22 4.28063 0.48727 3 4 5 22 4.78722 0.53290 2 4 -5 -22 4.43521 0.53184 3 0 6 22 91.9726 3.36357 11 0 6 22 91.8494 3.49220 2 0 -6 -22 96.5189 3.42786 3 0 -6 22 95.7953 3.36055 10 -1 6 22 39.7292 1.86004 11 1 -6 22 43.1368 1.83915 10 -1 -6 -22 42.0993 1.85071 3 -1 6 22 40.9303 1.89075 2 -1 -6 22 42.8210 1.83054 10 1 6 22 42.0087 1.83737 11 1 -6 -22 43.0693 1.95395 3 1 6 22 46.0242 2.05891 2 -2 6 22 94.8277 3.41897 11 -2 6 22 92.8232 3.27312 2 -2 -6 -22 92.5010 3.29126 3 2 -6 22 96.4597 3.31928 10 -2 -6 22 96.0788 3.22314 10 2 -6 -22 96.7892 3.48896 3 2 6 22 97.5861 3.53293 2 3 -6 22 51.1143 2.25940 10 -3 6 22 47.4060 1.98862 11 -3 -6 -22 49.5282 1.91792 3 3 -6 -22 50.5082 2.12332 3 3 6 22 58.0885 2.87580 2 -4 -6 -22 1.29387 0.40609 3 4 -6 22 1.77578 0.32846 10 4 6 22 1.26599 0.30631 2 4 -6 -22 1.44090 0.32374 3 0 7 22 14.4547 1.00577 11 0 -7 22 14.6401 0.95307 10 0 -7 -22 15.1789 1.00668 3 0 7 22 15.1243 1.10170 2 1 -7 22 58.0855 2.25979 10 -1 7 22 57.1105 2.35784 2 -1 7 22 57.4391 2.34444 11 -1 -7 -22 58.7528 2.26351 3 1 -7 -22 57.8029 2.33432 3 1 7 22 59.9811 2.48066 2 -1 -7 22 59.6934 2.47802 10 -2 7 22 15.9039 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8 22 66.4224 2.37775 2 3 -8 -22 66.6208 2.26276 3 0 -9 22 78.9977 2.56206 10 0 9 22 75.5708 2.74990 11 0 -9 -22 76.0785 2.60308 3 0 9 -22 75.7363 2.55628 8 0 9 22 77.8030 2.85579 2 1 -9 22 10.1519 0.64883 10 -1 -9 -22 9.71854 0.62615 3 1 9 -22 9.15111 0.67302 6 -1 9 22 10.1439 0.76254 11 -1 9 22 8.86976 0.73829 2 -1 9 -22 9.41679 0.69809 8 1 9 22 9.66523 0.79266 2 1 -9 -22 9.78302 0.65321 3 1 9 22 9.99720 0.70453 11 2 -9 22 33.2418 1.32782 10 -2 -9 -22 34.0607 1.50298 3 2 9 -22 32.7437 1.51673 6 -2 9 22 32.9822 1.32059 2 -2 9 22 34.0772 1.43514 11 -2 9 -22 37.0198 1.46702 8 2 9 22 33.9377 1.51018 2 2 9 22 34.7681 1.30908 11 3 -9 22 13.6954 0.65279 10 -3 9 22 13.1822 0.68736 11 3 9 -22 12.8216 0.74072 6 -3 9 -22 14.8262 0.73252 8 3 9 22 14.0405 0.73182 2 0 10 -22 53.1486 1.75922 8 0 10 22 52.5735 1.94178 11 0 10 22 51.6153 2.01237 2 -1 10 22 29.0053 1.27902 2 -1 10 22 28.1367 1.26227 11 1 -10 22 30.6277 1.09275 10 1 10 22 27.6745 1.29883 2 -1 10 -22 31.4328 1.51983 8 1 10 22 27.9521 1.17361 11 -2 10 22 20.3437 1.03997 2 2 -10 22 26.0891 0.94640 10 -2 10 22 25.5854 1.05078 11 -2 10 -22 27.1283 1.07765 8 2 10 22 25.6657 1.13377 2 0 11 22 3.63852 0.42657 2 0 11 22 4.06198 0.38621 11 -1 11 22 6.88032 0.47289 11 -1 11 22 6.88425 0.46197 2 1 11 22 5.94129 0.48420 2 0 0 23 0.89066 0.48954 10 0 0 -23 -0.2426 0.30522 3 -2 0 23 254.051 7.96913 10 2 0 23 245.796 7.82309 10 -2 0 -23 251.417 7.84979 3 2 0 -23 253.784 7.98161 3 -3 0 -23 45.6188 2.65767 9 3 0 23 49.5167 1.96592 10 3 0 -23 52.2845 2.15541 3 -3 0 -23 52.6522 2.07129 3 -4 0 23 24.9233 1.10870 3 4 0 -23 26.2900 1.22163 3 -4 0 -23 24.9906 1.66889 9 -4 0 -23 26.6555 1.17909 3 0 1 -23 253.234 8.04502 3 0 -1 -23 258.286 8.08859 3 0 -1 23 258.138 8.07857 10 0 1 23 255.078 8.07698 10 0 1 23 249.608 7.85452 2 1 1 23 48.4873 2.04667 2 -2 -1 -23 71.2718 2.72646 3 2 1 -23 70.7607 2.77073 3 2 -1 23 66.8714 2.66542 10 2 1 23 69.0463 2.62386 10 2 -1 -23 68.6359 2.77799 3 -2 1 -23 68.8094 2.63236 3 -2 -1 23 65.2661 2.68423 10 3 1 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58.5633 2.40143 3 -3 2 -23 58.3517 2.17573 3 -4 -2 -23 9.82772 0.71287 3 4 -2 23 9.61074 0.59504 10 -4 -2 -23 9.26705 0.90424 9 4 -2 -23 9.35404 0.72816 3 -4 2 -23 9.57415 0.55708 3 0 -3 -23 24.9194 1.43593 3 0 -3 23 24.1689 1.37638 10 0 3 23 23.4322 1.38833 10 0 3 23 24.8961 1.33993 2 0 3 -23 23.6136 1.29402 3 -1 -3 -23 6.56344 0.78306 3 1 -3 23 7.61402 0.96091 10 -1 3 23 8.38919 0.68939 2 1 3 -23 7.74768 0.73462 3 1 -3 -23 7.16608 0.83000 3 -1 3 -23 6.75407 0.68633 3 1 3 23 7.74470 0.75838 2 1 3 23 7.63824 0.94138 10 -1 -3 23 8.07366 0.78819 10 2 -3 23 92.4313 3.30215 10 -2 -3 -23 90.3516 3.32553 3 -2 3 23 91.1375 3.21630 11 2 3 -23 91.2970 3.21324 3 -2 -3 23 89.6575 3.29391 10 2 3 23 91.8041 3.37608 2 2 3 23 91.9969 3.22461 10 2 -3 -23 95.6641 3.48812 3 -2 3 -23 91.3284 3.19322 3 3 -3 23 392.677 11.5236 10 3 3 -23 375.049 11.3415 3 -3 -3 -23 380.159 12.1557 9 -3 -3 -23 402.614 11.6091 3 -3 3 -23 391.920 11.5510 3 3 -3 -23 397.419 11.9156 3 -4 -3 -23 66.8817 2.34072 3 4 -3 23 66.9518 2.23508 10 -4 -3 -23 63.8716 2.66822 9 4 3 23 69.1378 2.49607 2 4 -3 -23 70.4472 2.52477 3 0 -4 -23 1145.49 32.7849 3 0 4 -23 1130.42 32.4917 3 0 4 23 1129.32 32.7289 2 0 -4 23 1137.29 32.7191 10 1 4 -23 101.397 3.43935 3 -1 -4 -23 100.747 3.64574 3 1 -4 23 104.044 3.65267 10 -1 4 23 99.6072 3.55000 11 -1 4 23 103.639 3.59760 2 -1 4 -23 99.8574 3.36103 3 1 4 23 97.4904 3.51481 10 1 4 23 98.3273 3.61375 2 1 -4 -23 100.486 3.66219 3 -1 -4 23 100.960 3.55802 10 2 -4 23 0.68472 0.40926 10 -2 4 23 0.99186 0.33721 11 -2 -4 -23 1.33626 0.40150 3 -2 -4 23 0.88665 0.41795 10 2 -4 -23 0.61660 0.39606 3 2 4 23 0.78786 0.35702 2 -2 4 -23 0.70350 0.30029 3 3 -4 23 17.0347 0.97817 10 -3 -4 -23 17.4047 1.02916 3 3 -4 -23 16.1041 1.08876 3 3 4 23 17.9767 1.06463 2 -4 -4 -23 39.6882 1.54727 3 4 -4 23 39.8816 1.47394 10 4 4 23 40.8964 1.63230 2 4 -4 -23 40.7942 1.64451 3 0 -5 -23 18.7006 1.18534 3 0 -5 23 19.8488 1.15998 10 0 5 23 17.6156 1.14650 2 0 5 23 18.0721 1.05169 11 1 -5 23 51.1854 2.11258 10 -1 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26.0123 1.16674 10 3 -6 -23 25.5392 1.23758 3 3 6 23 25.7031 1.26926 2 -4 -6 -23 18.8482 0.81667 3 4 -6 23 18.4978 0.79054 10 4 -6 -23 18.2074 0.84373 3 4 6 23 19.7621 0.89010 2 -4 -6 23 18.2868 0.85702 3 0 7 23 17.6594 1.02013 11 0 7 -23 17.9888 0.93853 8 0 -7 23 16.7644 1.00141 10 0 7 23 17.6809 1.13041 2 1 -7 23 63.9156 2.34416 10 -1 -7 -23 62.0435 2.33441 3 -1 7 23 62.2536 2.37633 11 -1 7 23 60.2053 2.37472 2 1 -7 -23 60.5135 2.34022 3 1 7 23 61.3069 2.22248 11 1 7 23 62.7587 2.46620 2 -1 -7 23 60.2195 2.19350 10 -2 7 23 2.29298 0.37190 2 -2 7 23 1.85475 0.39670 11 -2 -7 -23 2.76170 0.44040 3 2 -7 23 2.15191 0.44794 10 2 -7 -23 1.81906 0.40840 3 2 7 23 2.03497 0.41796 2 3 -7 23 10.7216 0.66158 10 -3 -7 -23 10.8307 0.78949 3 3 7 23 10.7272 0.73005 2 3 -7 -23 10.7767 1.00842 3 0 -8 23 668.795 19.0374 10 0 8 -23 664.966 18.9668 8 0 8 23 668.463 19.2889 2 0 8 23 656.065 19.1274 11 0 -8 -23 645.062 19.0893 3 -1 -8 -23 91.4754 3.04307 3 1 -8 23 92.3825 3.06263 10 1 8 -23 85.1129 3.48624 6 -1 8 23 92.8501 3.15139 11 -1 8 23 93.6510 3.17271 2 -1 -8 23 86.8211 2.93486 10 1 8 23 94.7531 3.24910 2 1 8 23 85.8023 3.07045 11 1 -8 -23 94.0936 3.07686 3 -2 8 23 90.3930 2.92038 2 -2 -8 -23 93.0504 2.97477 3 2 -8 23 93.5824 3.03403 10 -2 8 23 89.2158 3.06464 11 2 -8 -23 86.3071 3.01265 3 2 8 23 93.9012 3.15081 2 3 -8 23 29.9589 1.19246 10 3 -8 -23 28.0537 1.08331 3 3 8 23 30.0555 1.22501 2 0 -9 23 2.03441 0.30598 10 0 9 23 2.74553 0.44720 11 0 9 23 1.41679 0.34992 2 -1 9 23 52.0511 1.99321 11 -1 9 23 52.1747 1.94301 2 -1 9 -23 51.5416 2.04396 8 1 9 23 53.3106 2.02216 2 1 9 23 50.7987 1.81757 11 1 -9 -23 51.2670 1.91618 3 2 -9 23 64.2217 2.05577 10 -2 9 23 62.1709 2.10777 11 2 9 -23 56.4900 2.12727 6 -2 9 -23 61.8962 2.17515 8 2 9 23 63.1864 2.22227 2 0 10 23 14.1756 0.81280 2 0 10 23 15.2221 0.71576 11 -1 10 23 123.734 3.76225 11 -1 10 23 119.270 3.75747 2 1 10 23 123.025 3.89458 2 0 0 24 133.385 4.63857 10 0 0 -24 135.622 4.63943 3 -1 0 -24 427.703 12.6589 3 -1 0 24 426.704 12.7322 10 1 0 -24 430.709 12.7192 3 1 0 24 405.004 12.6192 10 1 0 24 410.571 12.4515 2 -2 0 -24 288.388 8.86236 3 2 0 -24 289.045 8.96050 3 2 0 24 289.216 8.85628 10 -3 0 -24 1.32487 0.35080 3 3 0 -24 1.49093 0.44593 3 3 0 24 1.34047 0.38718 10 -4 0 -24 63.3539 2.16275 3 4 0 -24 63.0834 2.18566 3 0 1 -24 76.4467 2.95644 3 0 -1 24 76.6538 2.99984 10 0 1 24 80.3510 3.03556 10 0 1 24 77.8341 2.79475 2 0 -1 -24 77.2197 3.00454 3 -1 1 24 26.7358 1.48029 10 1 -1 24 25.5022 1.41525 10 -1 -1 -24 26.9742 1.44930 3 1 1 -24 25.8040 1.43439 3 1 -1 24 25.8829 1.24977 2 1 1 24 24.6115 1.30202 2 -1 -1 24 28.0885 1.47701 10 1 -1 -24 28.2676 1.50309 3 -1 1 -24 26.5833 1.41827 3 1 1 24 25.8920 1.41994 10 2 1 -24 35.2130 1.66649 3 -2 -1 -24 34.0193 1.63136 3 2 -1 24 34.4852 1.61722 10 2 1 24 33.2060 1.57028 10 -2 1 -24 34.9160 1.59978 3 2 -1 -24 34.1917 1.70300 3 3 -1 24 18.6545 1.20028 10 -3 1 24 15.2797 0.74961 3 -3 -1 -24 17.4206 0.99771 3 3 1 -24 13.1594 1.28607 3 3 1 24 16.8454 0.91154 10 -3 1 -24 18.6534 1.01440 3 3 -1 -24 17.8164 1.09146 3 4 1 -24 35.1412 1.37786 3 -4 -1 -24 36.0827 1.40985 3 4 -1 -24 36.3099 1.45031 3 -4 -1 24 32.7320 1.24927 3 -4 1 -24 37.8340 1.62663 3 0 -2 24 0.85338 0.45764 10 0 -2 -24 0.01298 0.31818 3 0 2 24 -0.2032 0.41650 10 0 2 24 0.03413 0.26983 2 0 2 -24 0.23949 0.30492 3 1 -2 24 28.2149 1.47040 10 -1 2 24 28.6997 1.53524 10 -1 -2 -24 27.7666 1.48114 3 1 2 -24 26.7230 1.40916 3 -1 -2 24 31.1929 1.55213 10 -1 2 -24 29.1224 1.44573 3 1 2 24 27.5780 1.45655 10 1 2 24 28.0934 1.42561 2 1 -2 -24 28.3401 1.54901 3 2 -2 24 388.211 11.6334 10 2 2 -24 385.822 11.6002 3 -2 -2 -24 388.951 11.6593 3 2 -2 -24 383.859 11.6134 3 -2 -2 24 380.540 11.4922 10 -2 2 -24 386.139 11.3937 3 2 2 24 374.845 11.4750 2 2 2 24 384.183 11.4016 10 3 -2 24 4.58904 0.78993 10 -3 -2 -24 4.06753 0.55838 3 3 2 -24 3.30302 0.46651 3 -3 2 -24 4.28462 0.50126 3 3 -2 -24 4.39524 0.60527 3 3 2 24 4.09070 0.44852 10 -4 -2 -24 72.3311 2.42786 3 4 -2 24 70.3606 2.28002 10 4 -2 -24 72.4164 2.50902 3 4 2 24 72.1162 2.50245 2 0 -3 24 31.8125 1.58673 10 0 3 24 31.9431 1.61123 10 0 3 24 32.5114 1.55219 2 0 -3 -24 30.6606 1.60654 3 0 3 -24 30.9760 1.47495 3 -1 -3 -24 41.4344 1.93118 3 1 3 -24 44.4390 1.83533 3 1 -3 24 43.9726 1.92799 10 1 3 24 45.5451 1.95875 2 1 -3 -24 43.6527 2.01873 3 -1 3 -24 45.9206 1.85657 3 -1 -3 24 45.1154 1.95974 10 1 3 24 42.4116 1.91087 10 2 -3 24 132.172 4.43734 10 -2 -3 -24 136.030 4.47740 3 2 3 -24 130.919 4.29487 3 2 3 24 131.405 4.41884 2 2 -3 -24 133.742 4.52125 3 2 3 24 127.253 4.25257 10 -2 3 -24 128.135 4.20613 3 -2 -3 24 134.012 4.37150 10 3 -3 24 100.493 3.36849 10 -3 3 -24 100.369 3.22117 3 3 3 24 105.761 3.55492 2 -4 -3 -24 13.0318 0.73126 3 4 -3 24 13.1870 0.63168 10 -4 -3 24 12.3191 0.75086 3 4 3 24 14.8022 0.78606 2 4 -3 -24 13.7470 0.79253 3 0 -4 -24 3.10809 0.57931 3 0 4 -24 4.09243 0.50240 3 0 4 24 3.42187 0.54809 2 0 -4 24 3.93795 0.64245 10 1 4 -24 177.522 5.83306 3 -1 4 24 184.023 5.80035 2 -1 -4 -24 180.922 5.85908 3 1 -4 24 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3.39872 0.46319 3 3 -5 -24 3.30790 0.48541 3 3 5 24 3.75409 0.50505 2 4 -5 24 5.04161 0.34237 10 -4 -5 -24 4.45915 0.39402 3 -4 -5 24 4.66633 0.40049 3 4 -5 -24 5.12049 0.42410 3 4 5 24 6.27002 0.45000 2 0 6 -24 62.4336 2.22609 8 0 6 24 64.5913 2.29944 11 0 -6 24 64.0649 2.40589 10 0 6 24 66.3582 3.28911 2 0 -6 -24 65.9453 2.48906 3 1 -6 24 32.2877 1.46820 10 -1 6 24 32.9615 1.42177 11 -1 6 24 32.2370 1.44278 2 1 6 24 34.9884 1.64199 2 -1 -6 24 31.8921 1.41374 10 -2 6 24 26.7165 1.20068 11 2 -6 24 26.5339 1.25858 10 -2 -6 -24 28.7533 1.29867 3 2 -6 -24 28.9010 1.38544 3 2 6 24 28.4004 1.39395 2 3 -6 24 18.0700 0.88718 10 -3 -6 -24 18.2360 0.89519 3 3 6 24 19.4037 0.99701 2 3 -6 -24 19.0663 0.96729 3 0 7 -24 40.8256 1.59415 8 0 -7 -24 41.4204 1.69268 3 0 7 24 37.7972 1.60384 11 0 7 24 39.8133 1.73410 2 0 -7 24 41.0466 1.62098 10 -1 7 24 21.4758 1.06922 11 1 -7 24 23.7283 1.13455 10 -1 7 24 22.6339 1.10443 2 -1 -7 -24 23.0410 1.12444 3 -1 -7 24 23.5890 1.03822 10 1 -7 -24 22.8158 1.15074 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0.90284 3 3 0 25 98.9729 3.27881 10 -3 0 -25 103.134 3.38198 3 3 0 -25 102.228 3.42401 3 -4 0 -25 0.22811 0.18295 3 4 0 -25 0.07353 0.17105 3 0 -1 -25 2.36529 0.52874 3 0 1 25 2.01220 0.55351 10 0 -1 25 3.05948 0.63779 10 0 1 -25 2.64166 0.51461 3 1 -1 25 92.6891 3.24339 10 -1 -1 -25 89.5866 3.22910 3 1 1 -25 92.1193 3.21876 3 -1 1 25 88.7416 3.26700 10 1 -1 25 75.2533 3.09984 2 1 1 25 90.6672 3.29636 10 1 1 25 92.4348 3.18888 2 -1 -1 25 86.6138 3.30492 10 1 -1 -25 94.0503 3.37307 3 -1 1 -25 90.0730 3.24952 3 2 -1 25 118.713 4.00942 10 -2 -1 -25 120.069 4.04044 3 2 1 -25 118.224 4.02619 3 -2 1 -25 120.296 4.05564 3 2 1 25 119.852 4.04872 10 2 1 25 125.624 4.23471 2 2 -1 -25 122.835 4.19482 3 3 -1 25 32.2235 1.34768 10 3 1 -25 31.1505 1.36126 3 -3 -1 -25 32.7932 1.40777 3 -3 1 -25 30.3283 1.29267 3 3 -1 -25 31.5463 1.42606 3 3 1 25 29.2322 1.21034 10 -4 -1 -25 154.327 4.69000 3 4 -1 -25 159.190 4.83413 3 4 1 25 160.956 4.88548 2 0 2 25 18.2576 1.15004 2 0 2 -25 16.2424 1.04283 3 0 2 25 17.9475 1.13813 10 0 -2 -25 17.2178 1.13331 3 0 -2 25 17.0169 1.11525 10 -1 -2 -25 102.561 3.60294 3 1 2 -25 100.277 3.50557 3 1 -2 25 99.3477 3.56132 10 -1 -2 25 99.4984 3.55304 10 1 -2 -25 102.622 3.62604 3 1 2 25 98.1879 3.44366 2 1 2 25 96.9111 3.50694 10 -1 2 -25 101.949 3.46233 3 2 2 -25 185.466 6.19867 3 2 -2 25 186.350 5.90730 10 -2 -2 -25 186.953 5.93389 3 -2 2 -25 182.200 5.82680 3 2 2 25 193.473 6.07382 2 2 -2 -25 183.082 5.99293 3 3 -2 25 37.8716 1.50045 10 -3 -2 -25 36.3495 1.54011 3 3 2 -25 36.8975 1.39066 3 3 -2 -25 38.9216 1.67278 3 -3 2 -25 38.1141 1.44148 3 3 2 25 39.3657 1.61076 2 -4 -2 -25 127.625 3.94312 3 4 -2 -25 130.177 4.00674 3 4 2 25 129.710 4.02388 2 0 -3 25 0.42295 0.37369 10 0 -3 -25 0.63590 0.38431 3 0 3 -25 1.04527 0.31663 3 -1 -3 -25 28.0706 1.42725 3 1 3 -25 25.8476 1.24715 3 1 -3 25 27.2032 1.39156 10 1 -3 -25 28.7369 1.47497 3 -1 3 -25 26.4272 1.24020 3 1 3 25 27.3591 1.35429 2 -1 -3 25 26.1341 1.36470 10 1 3 25 27.0371 1.35389 10 2 3 -25 129.679 4.18144 3 -2 -3 -25 137.217 4.45615 3 2 -3 25 136.068 4.42276 10 2 -3 -25 138.119 4.56181 3 -2 3 -25 135.491 4.23670 3 2 3 25 133.271 4.31332 10 3 -3 25 46.8542 1.79748 10 -3 -3 -25 49.2738 1.85801 3 3 -3 -25 49.7820 1.95285 3 3 3 25 48.1213 1.89497 2 -4 -3 -25 3.37348 0.36040 3 4 3 25 3.28644 0.36815 2 4 -3 -25 3.19206 0.36730 3 0 4 25 34.3930 1.55818 2 0 -4 25 36.1781 1.65429 10 0 -4 -25 37.6240 1.71440 3 0 4 -25 36.5769 1.38321 3 1 -4 25 118.702 4.03188 10 -1 -4 -25 119.771 4.07261 3 1 4 25 120.610 4.15912 2 -1 4 -25 108.672 3.66118 3 1 -4 -25 119.132 4.04566 3 -1 -4 25 118.061 3.92147 10 -2 -4 -25 34.9735 2.04431 3 2 4 25 29.3270 1.40395 2 3 -4 25 24.9780 1.11859 10 -3 -4 -25 25.6134 1.15681 3 3 4 25 25.6226 1.20280 2 3 -4 -25 26.8553 1.23977 3 0 5 25 202.575 6.37933 2 0 -5 -25 206.685 6.46366 3 0 -5 25 204.514 6.39230 10 1 -5 25 159.658 5.11931 10 -1 -5 25 152.772 4.90890 10 1 5 25 156.635 5.03223 2 -2 -5 -25 16.5924 0.93728 3 2 -5 25 13.8905 0.86583 10 2 5 25 14.3671 0.91339 2 2 -5 -25 15.0864 0.96434 3 3 -5 25 28.6909 1.21240 10 -3 -5 -25 31.8038 1.26654 3 3 5 25 30.3541 1.29852 2 3 -5 -25 30.3058 1.29296 3 0 6 25 176.605 5.73570 2 0 -6 25 187.532 5.72392 10 0 -6 -25 186.006 5.78866 3 1 -6 25 44.6209 1.78258 10 -1 6 25 44.1559 1.74385 2 -1 -6 -25 45.7651 1.81325 3 -1 -6 25 42.4548 1.67589 10 1 6 25 45.0649 1.84331 2 1 -6 -25 46.5097 1.85190 3 -2 -6 -25 24.9138 1.13229 3 2 -6 25 24.2789 1.12466 10 2 -6 -25 23.3259 1.14130 3 2 6 25 23.6602 1.16130 2 3 -6 25 130.638 4.05492 10 -3 -6 -25 134.037 4.06796 3 3 6 25 133.947 4.18031 2 3 -6 -25 134.034 4.14595 3 0 7 25 5.64983 0.55184 2 0 -7 25 5.80946 0.49224 10 0 -7 -25 5.80659 0.54913 3 -1 -7 -25 88.7678 2.87329 3 -1 7 25 84.9715 2.76279 2 1 -7 25 92.3343 2.87231 10 -1 7 25 74.3055 2.90524 11 -1 -7 25 84.3341 2.73217 10 1 7 25 86.6746 2.97513 2 1 -7 -25 88.2841 2.92883 3 -1 7 -25 86.3348 2.78456 8 -2 -7 -25 0.43559 0.20710 3 2 -7 25 0.12974 0.22983 10 2 -7 -25 0.73957 0.26543 3 2 7 25 0.89775 0.27392 2 0 -8 -25 124.077 3.79182 3 0 8 25 120.748 3.86163 2 0 -8 25 120.864 3.70025 10 1 -8 25 26.6966 1.06541 10 -1 8 -25 23.7288 1.02088 8 1 -8 -25 27.2554 1.20235 3 2 -8 25 14.1159 0.65379 10 2 8 25 14.7622 0.74068 2 0 9 25 0.74715 0.29559 2 0 0 26 0.46281 0.36270 10 0 0 -26 0.55379 0.35178 3 1 0 26 63.6296 2.47963 2 1 0 -26 73.5030 2.69665 3 1 0 26 73.9279 2.69067 10 -1 0 -26 71.7715 2.66247 3 -1 0 26 72.2050 2.71187 10 2 0 -26 1.29206 0.43057 3 2 0 26 1.30064 0.38203 10 2 0 26 0.92401 0.28055 2 3 0 -26 32.4759 1.32331 3 3 0 26 31.3355 1.21945 10 -3 0 -26 31.9382 1.29894 3 3 0 26 31.9730 1.35381 2 0 1 26 147.353 4.89047 10 0 1 -26 146.343 4.81264 3 0 -1 26 148.862 4.88884 10 0 -1 -26 144.773 4.86634 3 -1 -1 -26 19.0887 1.12669 3 1 1 -26 19.4204 1.10580 3 1 -1 26 18.0132 1.10993 10 -1 -1 26 18.2503 1.13587 10 -1 1 -26 19.0451 1.08778 3 1 1 26 21.2392 1.01906 2 1 -1 -26 20.2723 1.19189 3 1 1 26 18.5454 1.10670 10 2 -1 26 85.4247 2.81497 2 2 -1 26 83.5447 2.95604 10 2 1 -26 85.2684 2.94739 3 2 1 26 81.0218 2.88428 10 -2 1 -26 84.5770 2.90042 3 2 1 26 87.3869 2.90472 2 3 -1 26 11.6126 0.71501 10 3 -1 26 12.9996 0.67058 2 -3 -1 -26 12.2884 0.73351 3 3 1 26 12.7942 0.73096 2 -3 1 -26 12.4612 0.67848 3 3 -1 -26 13.2778 0.78999 3 0 -2 -26 31.7354 1.52301 3 0 2 26 28.3288 1.45925 10 0 2 -26 31.0679 1.42062 3 0 -2 26 30.6753 1.48636 10 -1 -2 -26 30.2048 1.47159 3 1 -2 26 29.8798 1.45484 10 1 2 26 29.1990 1.41933 10 1 2 26 30.4864 1.35165 2 -1 -2 26 30.6391 1.46553 10 1 -2 -26 30.0863 1.50256 3 2 -2 26 17.8097 0.98502 10 2 2 -26 17.7969 0.91227 3 -2 -2 -26 17.0861 1.02159 3 2 2 26 16.4198 0.92514 2 -2 2 -26 17.4769 0.87790 3 2 2 26 15.9085 0.87481 10 2 -2 -26 16.9570 1.07421 3 3 -2 26 150.424 4.58306 10 3 -2 26 144.740 4.49503 2 -3 -2 -26 151.993 4.65875 3 3 -2 -26 150.943 4.79414 3 3 2 26 154.560 4.75325 2 0 3 26 15.3830 0.82410 2 0 -3 26 17.5589 1.03038 10 0 -3 -26 16.5844 1.03666 3 0 3 -26 14.3119 0.83982 3 -1 -3 -26 117.257 3.92558 3 1 3 -26 112.003 3.64913 3 1 -3 26 117.131 3.90033 10 1 3 26 108.635 3.73139 2 1 -3 -26 117.175 3.92101 3 -1 3 -26 114.858 3.61501 3 -2 -3 -26 83.7150 2.95518 3 2 -3 26 85.7958 2.93923 10 -2 3 -26 82.8032 2.59479 3 2 3 26 80.7564 2.86839 2 2 -3 -26 85.7308 2.98735 3 -3 -3 -26 7.28020 0.56698 3 3 -3 26 7.07239 0.52183 10 3 -3 -26 7.83890 0.61181 3 3 3 26 8.04975 0.58372 2 0 4 26 5.24709 0.49524 2 0 -4 26 4.22976 0.82560 10 0 -4 -26 3.73856 0.72594 3 -1 -4 -26 56.9266 2.28269 3 1 -4 26 63.7222 2.50684 10 1 4 26 54.8256 2.07639 2 1 -4 -26 55.0059 2.17654 3 -1 -4 26 53.5738 2.07530 10 -2 -4 -26 46.9494 1.83180 3 2 -4 26 45.5812 1.78855 10 2 -4 -26 47.7172 1.89674 3 2 4 26 45.6547 1.81089 2 3 -4 26 4.69862 0.57890 10 -3 -4 -26 4.01336 0.47934 3 3 -4 -26 4.62042 0.49667 3 3 4 26 5.24624 0.47119 2 0 -5 26 3.01161 0.53449 10 0 -5 -26 4.31248 0.56787 3 -1 -5 -26 27.0620 1.28536 3 1 -5 26 27.8681 1.27714 10 1 5 26 26.6449 1.23824 2 -1 -5 26 26.4701 1.18142 10 1 -5 -26 26.9550 1.30757 3 2 -5 26 24.9291 1.11958 10 -2 -5 -26 24.1307 1.12386 3 2 5 26 25.1076 1.14738 2 2 -5 -26 23.9727 1.16128 3 3 -5 26 31.5042 1.19970 10 -3 -5 -26 33.3197 1.23526 3 3 5 26 31.3359 1.23794 2 3 -5 -26 32.9009 1.25121 3 0 6 26 233.963 7.61460 2 0 -6 26 251.628 7.38591 10 0 -6 -26 252.670 7.47001 3 1 -6 26 0.04303 0.26448 10 -1 -6 -26 0.42053 0.24489 3 1 -6 -26 0.05340 0.25254 3 -1 -6 26 0.51662 0.26006 10 -1 6 -26 0.40906 0.17427 8 1 6 26 0.26354 0.23440 2 2 -6 26 37.4746 1.43885 10 -2 -6 -26 38.4582 1.44952 3 2 6 26 31.0279 1.66082 2 2 -6 -26 35.2380 1.40882 3 0 -7 26 6.63466 0.46019 10 0 7 26 6.09419 0.47155 2 0 -7 -26 6.07383 0.50069 3 -1 -7 -26 20.7028 0.92549 3 1 -7 26 20.8061 0.93544 10 1 -7 -26 22.7509 0.98154 3 1 7 26 20.8369 0.97727 2 2 -7 26 86.6929 2.71570 10 -2 -7 -26 85.3543 2.69080 3 2 -7 -26 78.5620 2.76159 3 2 7 26 86.1950 2.67174 2 0 0 -27 1.30067 0.64948 3 0 0 27 -0.1618 0.32493 10 1 0 -27 90.2437 3.10775 3 1 0 27 85.6437 3.07902 10 -1 0 -27 90.0296 3.07771 3 2 0 -27 41.3785 1.64695 3 2 0 27 40.7840 1.46756 2 -2 0 -27 40.6136 1.61151 3 2 0 27 40.8923 1.59835 10 3 0 27 4.35883 0.44231 2 -3 0 -27 4.25924 0.39244 3 3 0 -27 3.83786 0.36968 3 0 -1 -27 1.49262 0.48847 3 0 -1 27 1.01709 0.39256 10 0 1 -27 1.32293 0.38610 3 0 1 27 0.83433 0.38736 10 -1 -1 -27 235.931 7.10679 3 1 1 -27 225.980 7.01517 3 1 -1 27 228.191 7.10842 10 1 -1 -27 236.018 7.16946 3 1 1 27 226.333 7.10247 10 -1 1 -27 231.832 7.04711 3 -1 -1 27 231.218 7.15417 10 2 -1 27 11.1810 0.72262 10 2 1 -27 10.8993 0.70685 3 -2 -1 -27 11.9366 0.76309 3 2 1 27 10.5871 0.67744 10 -2 1 -27 11.0883 0.68379 3 2 1 27 11.5357 0.64660 2 2 -1 -27 12.4686 0.80723 3 -3 -1 -27 29.5875 1.13403 3 3 -1 27 26.1271 1.13560 10 3 1 27 29.8903 1.13660 2 3 -1 -27 30.4564 1.18058 3 0 -2 27 0.19774 0.40139 10 0 2 -27 0.35820 0.26113 3 1 -2 27 70.9323 2.53858 10 1 2 -27 67.2379 2.37049 3 -1 -2 -27 69.9844 2.54674 3 -1 -2 27 68.4488 2.50656 10 1 2 27 67.5012 2.32473 2 1 -2 -27 70.2039 2.56631 3 -1 2 -27 69.2257 2.36151 3 1 2 27 67.1272 2.46236 10 2 -2 27 52.7789 1.91063 10 2 2 -27 46.7158 1.68292 3 -2 -2 -27 53.2419 1.94128 3 -2 2 -27 48.0324 1.69983 3 2 2 27 50.7636 2.16941 2 2 -2 -27 50.4169 1.92990 3 3 -2 27 90.3316 2.81154 10 -3 -2 -27 90.5577 2.90877 3 3 2 27 93.9097 2.95710 2 3 -2 -27 94.0576 3.01144 3 0 -3 -27 24.9111 1.23336 3 0 -3 27 23.1335 1.17539 10 0 3 -27 22.7135 1.06675 3 1 -3 27 5.40713 0.56508 10 -1 -3 -27 5.22596 0.59298 3 -1 3 -27 4.44546 0.55808 3 1 -3 -27 5.60794 0.62280 3 1 3 27 4.78220 0.54741 2 -1 -3 27 4.98465 0.53779 10 2 -3 27 28.8138 1.24562 10 -2 -3 -27 29.3578 1.27896 3 2 -3 -27 28.6681 1.30330 3 2 3 27 28.6834 1.30887 2 -3 -3 -27 16.0991 0.75195 3 3 -3 27 15.4603 0.68689 10 3 3 27 16.3471 0.72527 2 3 -3 -27 15.6388 0.76487 3 0 -4 -27 44.3905 1.81690 3 0 -4 27 44.9827 1.76693 10 -1 -4 -27 6.24931 0.60361 3 1 -4 27 6.08601 0.57254 10 1 4 27 6.68136 0.50913 2 1 -4 -27 5.31273 0.59690 3 -1 -4 27 6.00451 0.52909 10 -2 -4 -27 270.546 7.91433 3 2 -4 27 259.759 7.87280 10 2 -4 -27 267.351 7.85818 3 2 4 27 256.264 7.75208 2 0 -5 -27 5.43258 0.56682 3 0 -5 27 5.60816 0.50486 10 -1 -5 -27 135.354 4.24970 3 1 -5 27 131.796 4.20232 10 1 5 27 125.346 4.01886 2 1 -5 -27 134.125 4.16425 3 2 -5 27 29.8896 1.56577 10 -2 -5 -27 29.3723 1.19183 3 2 -5 -27 28.3946 1.17924 3 2 5 27 27.4762 1.10919 2 0 -6 27 100.943 3.28467 10 0 -6 -27 108.706 3.54339 3 1 -6 27 4.11901 0.42126 10 -1 -6 -27 3.83009 0.41174 3 1 6 27 3.85083 0.37178 2 1 -6 -27 3.80625 0.43387 3 0 0 -28 628.363 18.2020 3 0 0 28 631.086 18.2773 10 1 0 -28 84.1682 2.85875 3 -1 0 -28 85.1133 2.85076 3 1 0 28 84.1182 2.88831 10 2 0 28 105.744 3.52885 10 2 0 -28 118.136 3.84427 3 0 -1 -28 78.8829 2.69118 3 0 1 -28 73.7150 2.57382 3 0 -1 28 75.2022 2.68470 10 -1 -1 -28 54.2649 1.99252 3 1 -1 28 51.7820 1.97997 10 1 1 -28 52.7057 1.88930 3 -1 1 -28 54.5257 1.92110 3 1 1 28 51.5116 1.98111 10 1 -1 -28 55.7227 2.03304 3 -2 -1 -28 36.3315 1.37854 3 2 1 -28 34.0932 1.23053 3 -2 1 -28 35.7366 1.26439 3 2 -1 -28 36.1139 1.41342 3 0 -2 28 44.3087 1.75712 10 0 2 -28 44.7154 1.72696 3 0 -2 -28 44.3493 1.77609 3 1 2 -28 210.005 6.52703 3 1 -2 28 229.621 6.81384 10 -1 -2 -28 233.439 6.83731 3 1 -2 -28 228.917 6.89927 3 -1 2 -28 223.928 6.61603 3 -2 -2 -28 98.5597 3.17399 3 2 -2 -28 96.9816 3.15499 3 0 -3 28 37.8895 1.52245 10 0 -3 -28 36.2015 1.52928 3 -1 -3 -28 64.3343 2.26806 3 1 -3 28 62.4802 2.23184 10 1 -3 -28 61.1471 2.20898 3 2 -3 28 17.7059 0.82665 10 2 -3 -28 16.0979 1.08390 3 0 -4 -28 6.10810 0.54383 3 0 -4 28 4.77722 0.48810 10 1 -4 28 33.6530 1.32213 10 -1 -4 -28 31.7490 1.33302 3 1 -4 -28 31.8082 1.32392 3 2 -4 28 56.8857 1.93043 10 -2 -4 -28 58.1858 1.95736 3 2 -4 -28 56.7062 1.95096 3 0 -5 -28 40.7284 1.58388 3 0 -5 28 42.9085 1.51925 10 1 -5 28 28.6341 1.13390 10 -1 -5 -28 29.2040 1.16641 3 1 -5 -28 27.7296 1.14336 3 0 -6 -28 228.042 6.74538 3 -1 0 -29 232.919 6.86264 3 1 0 -29 232.099 6.86727 3 0 1 -29 29.6636 1.12867 3 0 -1 -29 31.6752 1.27899 3 1 -1 29 62.4120 2.18598 10 -1 1 -29 59.5639 2.13909 3 -2 -1 -29 29.3358 1.07045 3 2 -1 -29 31.3118 1.24753 3 0 -2 29 94.1592 3.07846 10 0 -2 -29 94.5666 3.08216 3 0 -3 29 5.10494 0.45226 10 1 -3 29 80.2844 2.60992 10 -1 -3 -29 80.2612 2.62125 3 1 -3 -29 81.2415 2.66028 3 0 -4 29 24.0802 0.98887 10 0 -4 -29 25.6038 1.04476 3 0 -1 -30 11.2978 0.56328 3 0 0 0 0.00 0.00 0 _exptl_absorpt_process_details ) SADABS 2016/2: Krause, L., Herbst-Irmer, R., Sheldrick G.M. & Stalke D., J. Appl. Cryst. 48 (2015) 3-10 ) _exptl_absorpt_correction_type numerical _exptl_absorpt_correction_T_max 1.0000 _exptl_absorpt_correction_T_min 0.8061 _exptl_special_details ) The following wavelength and cell were deduced by SADABS from the direction cosines etc. They are given here for emergency use only: CELL 1.54184 6.269 13.152 24.078 89.980 89.997 89.997 ) ; _shelx_hkl_checksum 15045 _olex2_submission_special_instructions 'No special instructions were received' loop_ _space_group_symop_operation_xyz 'x, y, z' '-x+1/2, -y, z+1/2' '-x, y+1/2, -z+1/2' 'x+1/2, -y+1/2, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_site_symmetry_order _atom_site_calc_flag _atom_site_refinement_flags_posn O1 O 0.80909(19) 0.41310(9) 0.47299(4) 0.0327(3) Uani 1 1 d . O2 O 0.38192(16) 0.43987(8) 0.33848(4) 0.0224(2) Uani 1 1 d . O3 O 0.68738(16) 0.42912(8) 0.29137(4) 0.0234(2) Uani 1 1 d . N1 N 0.71119(18) 0.42241(9) 0.38341(5) 0.0177(2) Uani 1 1 d . N2 N -0.0449(2) 0.70415(9) 0.34215(5) 0.0242(3) Uani 1 1 d . N3 N 0.0469(2) 0.87347(9) 0.36880(5) 0.0252(3) Uani 1 1 d . C1 C 0.5723(2) 0.43181(10) 0.33859(5) 0.0177(3) Uani 1 1 d . C2 C 0.9143(2) 0.42780(12) 0.30474(6) 0.0261(3) Uani 1 1 d . H2A H 0.976901 0.496600 0.300844 0.031 Uiso 1 1 calc R H2B H 0.991948 0.380266 0.280084 0.031 Uiso 1 1 calc R C3 C 0.9241(2) 0.39219(10) 0.36462(6) 0.0205(3) Uani 1 1 d . H3 H 1.034619 0.432025 0.385182 0.025 Uiso 1 1 calc R C4 C 0.9654(2) 0.27731(10) 0.37214(6) 0.0223(3) Uani 1 1 d . H4A H 1.099142 0.259272 0.352675 0.027 Uiso 1 1 calc R H4B H 0.986389 0.263112 0.412145 0.027 Uiso 1 1 calc R C5 C 0.7886(2) 0.21012(10) 0.35067(6) 0.0199(3) Uani 1 1 d . C6 C 0.7869(3) 0.17434(11) 0.29603(6) 0.0263(3) Uani 1 1 d . H6 H 0.900337 0.191814 0.271712 0.032 Uiso 1 1 calc R C7 C 0.6214(3) 0.11354(12) 0.27681(7) 0.0325(4) Uani 1 1 d . H7 H 0.621932 0.090445 0.239424 0.039 Uiso 1 1 calc R C8 C 0.4556(3) 0.08636(12) 0.31179(7) 0.0328(4) Uani 1 1 d . H8 H 0.342956 0.044621 0.298496 0.039 Uiso 1 1 calc R C9 C 0.4548(3) 0.12040(11) 0.36630(7) 0.0289(3) Uani 1 1 d . H9 H 0.342246 0.101542 0.390599 0.035 Uiso 1 1 calc R C10 C 0.6197(2) 0.18237(11) 0.38535(6) 0.0221(3) Uani 1 1 d . H10 H 0.617202 0.206179 0.422596 0.027 Uiso 1 1 calc R C11 C 0.6689(2) 0.43382(10) 0.44015(6) 0.0206(3) Uani 1 1 d . C12 C 0.4536(2) 0.47643(10) 0.45686(6) 0.0212(3) Uani 1 1 d . H12 H 0.340474 0.440336 0.435248 0.025 Uiso 1 1 calc R C13 C 0.4138(3) 0.45873(12) 0.51879(6) 0.0325(4) Uani 1 1 d . H13A H 0.518552 0.497071 0.540549 0.049 Uiso 1 1 calc GR H13B H 0.427374 0.385999 0.527117 0.049 Uiso 1 1 calc GR H13C H 0.269873 0.481786 0.528380 0.049 Uiso 1 1 calc GR C14 C 0.4455(2) 0.58949(10) 0.44243(5) 0.0182(3) Uani 1 1 d . C15 C 0.2763(2) 0.62869(10) 0.41196(5) 0.0183(3) Uani 1 1 d . H15 H 0.168771 0.584051 0.398589 0.022 Uiso 1 1 calc R C16 C 0.2619(2) 0.73290(10) 0.40072(5) 0.0184(3) Uani 1 1 d . C17 C 0.4205(2) 0.79808(10) 0.42059(5) 0.0203(3) Uani 1 1 d . H17 H 0.412012 0.869098 0.413481 0.024 Uiso 1 1 calc R C18 C 0.5906(2) 0.75908(11) 0.45070(6) 0.0225(3) Uani 1 1 d . H18 H 0.698515 0.803511 0.464032 0.027 Uiso 1 1 calc R C19 C 0.6036(2) 0.65528(11) 0.46145(6) 0.0215(3) Uani 1 1 d . H19 H 0.720943 0.629077 0.481871 0.026 Uiso 1 1 calc R C20 C 0.0780(2) 0.77240(10) 0.36854(5) 0.0194(3) Uani 1 1 d . C21 C -0.2125(3) 0.74144(13) 0.31439(6) 0.0277(3) Uani 1 1 d . H21 H -0.303272 0.695232 0.295371 0.033 Uiso 1 1 calc R C22 C -0.2593(3) 0.84407(13) 0.31216(6) 0.0282(3) Uani 1 1 d . H22 H -0.378735 0.869465 0.292266 0.034 Uiso 1 1 calc R C23 C -0.1218(3) 0.90769(12) 0.34066(6) 0.0288(3) Uani 1 1 d . H23 H -0.148538 0.978856 0.340168 0.035 Uiso 1 1 calc R loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 O1 0.0330(6) 0.0368(6) 0.0282(5) -0.0049(5) -0.0131(5) 0.0111(5) O2 0.0148(4) 0.0281(5) 0.0242(5) -0.0004(4) -0.0020(4) 0.0033(4) O3 0.0200(5) 0.0278(5) 0.0224(5) 0.0054(4) 0.0043(4) 0.0047(4) N1 0.0130(5) 0.0165(5) 0.0236(5) -0.0004(4) -0.0018(4) 0.0018(4) N2 0.0236(6) 0.0255(6) 0.0237(6) -0.0049(5) -0.0018(5) 0.0036(5) N3 0.0289(7) 0.0205(6) 0.0261(6) 0.0027(5) -0.0004(5) 0.0031(5) C1 0.0185(7) 0.0152(6) 0.0195(6) 0.0016(5) 0.0000(5) 0.0012(5) C2 0.0177(7) 0.0244(7) 0.0360(8) 0.0068(6) 0.0073(6) 0.0036(6) C3 0.0120(6) 0.0184(6) 0.0312(7) 0.0003(5) 0.0009(5) 0.0006(5) C4 0.0169(6) 0.0186(6) 0.0313(7) 0.0007(5) -0.0022(6) 0.0045(5) C5 0.0209(6) 0.0133(6) 0.0254(7) 0.0010(5) -0.0034(6) 0.0060(5) C6 0.0331(8) 0.0204(7) 0.0254(7) 0.0013(6) -0.0012(6) 0.0090(6) C7 0.0438(9) 0.0228(7) 0.0310(8) -0.0066(6) -0.0145(7) 0.0122(7) C8 0.0278(8) 0.0191(7) 0.0516(10) -0.0069(6) -0.0165(7) 0.0053(6) C9 0.0208(7) 0.0184(6) 0.0475(9) 0.0021(6) -0.0021(7) 0.0034(6) C10 0.0218(7) 0.0175(6) 0.0271(7) 0.0005(5) -0.0024(6) 0.0045(5) C11 0.0237(7) 0.0162(6) 0.0218(6) -0.0009(5) -0.0036(5) 0.0021(5) C12 0.0242(7) 0.0196(6) 0.0198(6) 0.0010(5) 0.0010(6) 0.0019(5) C13 0.0436(9) 0.0298(8) 0.0241(7) 0.0074(6) 0.0079(7) 0.0064(7) C14 0.0213(7) 0.0183(6) 0.0148(5) -0.0024(5) 0.0035(5) 0.0018(5) C15 0.0191(6) 0.0179(6) 0.0179(6) -0.0035(5) 0.0017(5) -0.0009(5) C16 0.0207(7) 0.0193(6) 0.0152(6) -0.0014(5) 0.0039(5) 0.0006(5) C17 0.0240(7) 0.0178(6) 0.0191(6) -0.0011(5) 0.0039(5) -0.0003(6) C18 0.0226(7) 0.0234(7) 0.0217(7) -0.0054(5) 0.0001(6) -0.0043(6) C19 0.0204(6) 0.0259(7) 0.0180(6) -0.0023(5) -0.0014(5) 0.0029(6) C20 0.0213(7) 0.0208(6) 0.0162(6) -0.0006(5) 0.0039(5) 0.0022(5) C21 0.0236(7) 0.0348(8) 0.0245(7) -0.0047(6) -0.0034(6) 0.0041(7) C22 0.0261(8) 0.0366(8) 0.0218(7) 0.0045(6) 0.0011(6) 0.0086(6) C23 0.0329(8) 0.0240(7) 0.0295(7) 0.0054(6) -0.0002(7) 0.0068(6) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0181 0.0091 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' N N 0.0311 0.0180 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0492 0.0322 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle C1 O3 C2 109.68(11) C1 N1 C3 110.80(11) C1 N1 C11 128.92(12) C11 N1 C3 120.23(11) C21 N2 C20 116.29(13) C23 N3 C20 116.49(13) O2 C1 O3 122.29(13) O2 C1 N1 129.25(13) O3 C1 N1 108.45(11) O3 C2 H2A 110.8 O3 C2 H2B 110.8 O3 C2 C3 104.65(11) H2A C2 H2B 108.9 C3 C2 H2A 110.8 C3 C2 H2B 110.8 N1 C3 C2 99.96(11) N1 C3 H3 109.7 N1 C3 C4 112.47(11) C2 C3 H3 109.7 C2 C3 C4 114.86(12) C4 C3 H3 109.7 C3 C4 H4A 108.7 C3 C4 H4B 108.7 H4A C4 H4B 107.6 C5 C4 C3 114.11(11) C5 C4 H4A 108.7 C5 C4 H4B 108.7 C6 C5 C4 121.66(14) C6 C5 C10 117.99(14) C10 C5 C4 120.35(13) C5 C6 H6 119.6 C7 C6 C5 120.85(15) C7 C6 H6 119.6 C6 C7 H7 119.8 C8 C7 C6 120.45(14) C8 C7 H7 119.8 C7 C8 H8 120.2 C7 C8 C9 119.67(15) C9 C8 H8 120.2 C8 C9 H9 120.1 C8 C9 C10 119.81(16) C10 C9 H9 120.1 C5 C10 H10 119.4 C9 C10 C5 121.22(14) C9 C10 H10 119.4 O1 C11 N1 118.31(13) O1 C11 C12 123.74(13) N1 C11 C12 117.87(12) C11 C12 H12 108.6 C11 C12 C13 110.38(12) C11 C12 C14 109.18(11) C13 C12 H12 108.6 C14 C12 H12 108.6 C14 C12 C13 111.37(11) C12 C13 H13A 109.5 C12 C13 H13B 109.5 C12 C13 H13C 109.5 H13A C13 H13B 109.5 H13A C13 H13C 109.5 H13B C13 H13C 109.5 C15 C14 C12 120.41(12) C15 C14 C19 119.20(12) C19 C14 C12 120.34(13) C14 C15 H15 119.5 C14 C15 C16 120.93(13) C16 C15 H15 119.5 C15 C16 C20 119.57(13) C17 C16 C15 119.20(13) C17 C16 C20 121.23(13) C16 C17 H17 120.0 C18 C17 C16 120.01(13) C18 C17 H17 120.0 C17 C18 H18 119.9 C17 C18 C19 120.30(13) C19 C18 H18 119.9 C14 C19 H19 119.8 C18 C19 C14 120.36(13) C18 C19 H19 119.8 N2 C20 C16 117.40(12) N3 C20 N2 125.43(13) N3 C20 C16 117.16(13) N2 C21 H21 118.5 N2 C21 C22 122.92(15) C22 C21 H21 118.5 C21 C22 H22 122.0 C21 C22 C23 115.97(15) C23 C22 H22 122.0 N3 C23 C22 122.89(14) N3 C23 H23 118.6 C22 C23 H23 118.6 loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance O1 C11 1.2140(18) O2 C1 1.1994(17) O3 C1 1.3474(16) O3 C2 1.4597(18) N1 C1 1.3927(17) N1 C3 1.4654(18) N1 C11 1.3999(18) N2 C20 1.3424(19) N2 C21 1.339(2) N3 C20 1.3420(18) N3 C23 1.335(2) C2 H2A 0.9900 C2 H2B 0.9900 C2 C3 1.517(2) C3 H3 1.0000 C3 C4 1.5420(18) C4 H4A 0.9900 C4 H4B 0.9900 C4 C5 1.509(2) C5 C6 1.397(2) C5 C10 1.398(2) C6 H6 0.9500 C6 C7 1.389(2) C7 H7 0.9500 C7 C8 1.385(3) C8 H8 0.9500 C8 C9 1.387(2) C9 H9 0.9500 C9 C10 1.394(2) C10 H10 0.9500 C11 C12 1.516(2) C12 H12 1.0000 C12 C13 1.530(2) C12 C14 1.5263(18) C13 H13A 0.9800 C13 H13B 0.9800 C13 H13C 0.9800 C14 C15 1.390(2) C14 C19 1.393(2) C15 H15 0.9500 C15 C16 1.3984(19) C16 C17 1.397(2) C16 C20 1.484(2) C17 H17 0.9500 C17 C18 1.388(2) C18 H18 0.9500 C18 C19 1.390(2) C19 H19 0.9500 C21 H21 0.9500 C21 C22 1.381(2) C22 H22 0.9500 C22 C23 1.384(2) C23 H23 0.9500