data_5000118
_chemical_name_systematic          'Lead molybdate'
_chemical_name_mineral             'Wulfenite'
_publ_author_name                  'ARAKI, T'
_journal_name_full
;
Memoirs of the College of Science, University of Kyoto, Series B
;
_journal_volume                    24
_journal_year                      1957
_journal_page_first                155
_journal_page_last                 160
_cell_length_a                     5.47(1)
_cell_length_b                     5.47(1)
_cell_length_c                     12.18(2)
_cell_angle_alpha                  90
_cell_angle_beta                   90
_cell_angle_gamma                  90
_cell_volume                       364.4
_cell_formula_units_Z              4
_exptl_crystal_density_meas        6.7
_symmetry_space_group_name_H-M     'I 41/a Z'
_symmetry_Int_Tables_number        88
_symmetry_cell_setting             tetragonal
loop_
_symmetry_equiv_pos_as_xyz
  'x,y,z'
  '-x,1/2-y,z'
  '3/4-y,1/4+x,1/4+z'
  '1/4+y,1/4-x,1/4+z'
  '-x,-y,-z'
  'x,1/2+y,-z'
  '1/4+y,3/4-x,3/4-z'
  '3/4-y,3/4+x,3/4-z'
  '1/2+x,1/2+y,1/2+z'
  '1/2-x,-y,1/2+z'
  '1/4-y,3/4+x,3/4+z'
  '3/4+y,3/4-x,3/4+z'
  '1/2-x,1/2-y,1/2-z'
  '1/2+x,y,1/2-z'
  '3/4+y,1/4-x,1/4-z'
  '1/4-y,1/4+x,1/4-z'
loop_
_atom_type_symbol
_atom_type_oxidation_number
  Pb2+   2.000
  Mo6+   6.000
  O2-   -2.000
loop_
_atom_site_label
_atom_site_type_symbol
_atom_site_symmetry_multiplicity
_atom_site_Wyckoff_symbol
_atom_site_fract_x
_atom_site_fract_y
_atom_site_fract_z
_atom_site_occupancy
_atom_site_attached_hydrogens
_atom_site_calc_flag
  Pb1   Pb2+   4 b 0. 0.25 0.625 1.  0 d
  Mo1   Mo6+   4 a 0. 0.25 0.125 1.  0 d
  O1    O2-   16 f 0.247(3) 0.342(5) 0.04(2) 1.  0 d
_refine_ls_R_factor_all            0.2