Crystallography Open Database

Information card for entry 7000380

Preview

Coordinates	7000380.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C59.88 H66.75 Al Cl3.75 F36 Ge O10
Calculated formula	C59.88 H66.76 Al Cl3.76 F36 Ge O10
Title of publication	[(OtBu)2C6H3]3Ge+ a free germyl cation with aryl ligands
Authors of publication	Schenk, Christian; Drost, Christian; Schnepf, Andreas
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	5
Pages of publication	773 - 776
a	18.101 ± 0.0009 Å
b	24.3749 ± 0.0008 Å
c	18.2722 ± 0.0008 Å
α	90°
β	106.088 ± 0.004°
γ	90°
Cell volume	7746.2 ± 0.6 Å³
Cell temperature	99 ± 2 K
Ambient diffraction temperature	99 ± 2 K
Number of distinct elements	7
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.0569
Residual factor for significantly intense reflections	0.0438
Weighted residual factors for significantly intense reflections	0.1068
Weighted residual factors for all reflections included in the refinement	0.1138
Goodness-of-fit parameter for all reflections included in the refinement	1.042
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
179681 (current)	2016-03-24	cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/03.	7000380.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7000380.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7000380.cif
1143	2010-05-03	cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition.	7000380.cif