Crystallography Open Database

Information card for entry 7000392

Preview

Coordinates	7000392.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C39.5 H39 Cl3 Co2 I4 N2 O2 P2
Calculated formula	C39.5 H39 Cl3 Co2 I4 N2 O2 P2
Title of publication	Synthesis and characterization of Co and Ni complexes stabilized by keto- and acetamide-derived P,O-type phosphine ligands
Authors of publication	Agostinho, Magno; Rosa, Vitor; Avilés, Teresa; Welter, Richard; Braunstein, Pierre
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	5
Pages of publication	814 - 822
a	8.052 ± 0.0003 Å
b	15.407 ± 0.0005 Å
c	19.874 ± 0.0007 Å
α	89.393 ± 0.002°
β	82.027 ± 0.002°
γ	76.374 ± 0.0014°
Cell volume	2372.33 ± 0.15 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	8
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.114
Residual factor for significantly intense reflections	0.0593
Weighted residual factors for significantly intense reflections	0.1627
Weighted residual factors for all reflections included in the refinement	0.1971
Goodness-of-fit parameter for all reflections included in the refinement	0.912
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
176453 (current)	2016-02-16	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in range 7.	7000392.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7000392.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7000392.cif
1143	2010-05-03	cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition.	7000392.cif