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Information card for entry 7000399
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| Coordinates | 7000399.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | aqua(N,N'-bis(o-fluorophenyl)diaza-18-crown- 6)lead(ii)diperchlorate |
|---|---|
| Chemical name | aqua{N,N'-bis(o-fluorophenyl)diaza-18-crown-6}lead(II)diperchlorate |
| Formula | C24 H34 Cl2 F2 N2 O13 Pb |
| Calculated formula | C24 H34 Cl2 F2 N2 O13 Pb |
| Title of publication | Lariat ethers with fluoroaryl side-arms: a study of CF⋯metal cation interaction in the complexes of N-(o-fluoroaryl)azacrown ethers |
| Authors of publication | Sazonov, Petr K.; Minacheva, Lidiya Kh.; Churakov, Andrei V.; Sergienko, Vladimir S.; Artamkina, Galina A.; Oprunenko, Yuri F.; Beletskaya, Irina P. |
| Journal of publication | Dalton Transactions |
| Year of publication | 2009 |
| Journal issue | 5 |
| Pages of publication | 843 - 850 |
| a | 19.423 ± 0.005 Å |
| b | 12.719 ± 0.003 Å |
| c | 13.109 ± 0.003 Å |
| α | 90° |
| β | 94.711 ± 0.003° |
| γ | 90° |
| Cell volume | 3227.5 ± 1.3 Å3 |
| Cell temperature | 303 ± 2 K |
| Ambient diffraction temperature | 303 ± 2 K |
| Number of distinct elements | 7 |
| Space group number | 15 |
| Hermann-Mauguin space group symbol | C 1 2/c 1 |
| Hall space group symbol | -C 2yc |
| Residual factor for all reflections | 0.0893 |
| Residual factor for significantly intense reflections | 0.0679 |
| Weighted residual factors for significantly intense reflections | 0.1773 |
| Weighted residual factors for all reflections included in the refinement | 0.1967 |
| Goodness-of-fit parameter for all reflections included in the refinement | 1.009 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 179681 (current) | 2016-03-24 | cif/7/00/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/00/03. |
7000399.cif |
| 120443 | 2014-07-15 | Adding 17924 DOIs guessed from source file names. | 7000399.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7000399.cif |
| 1143 | 2010-05-03 | cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition. |
7000399.cif |
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