Crystallography Open Database

Information card for entry 7001655

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Structure parameters

Formula	C8 H28 N8 Si
Calculated formula	C8 H28 N8 Si
Title of publication	Syntheses and structures of (N′,N′-dimethylhydrazido)silanes
Authors of publication	Gronde, Ingo; Neumann, Beate; Willner, Alexander; Pape, Tania; Mitzel, Norbert W.
Journal of publication	Dalton Transactions
Year of publication	2009
Journal issue	27
Pages of publication	5300 - 5309
a	17.998 ± 0.005 Å
b	5.0153 ± 0.0013 Å
c	18.163 ± 0.005 Å
α	90°
β	109.464 ± 0.005°
γ	90°
Cell volume	1545.8 ± 0.7 Å³
Cell temperature	153 ± 2 K
Ambient diffraction temperature	153 ± 2 K
Number of distinct elements	4
Space group number	13
Hermann-Mauguin space group symbol	P 1 2/c 1
Hall space group symbol	-P 2yc
Residual factor for all reflections	0.0833
Residual factor for significantly intense reflections	0.0497
Weighted residual factors for significantly intense reflections	0.1137
Weighted residual factors for all reflections included in the refinement	0.1293
Goodness-of-fit parameter for all reflections included in the refinement	0.991
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
301846 (current)	2025-08-21	Add cross-references to PubChem compounds in COD range 7/00/ Each referenced PubChem compound corresponds to the full crystal structure.	7001655.cif
176432	2016-02-14	cif/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries.	7001655.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7001655.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7001655.cif
1143	2010-05-03	cif/7/ Adding CIFs from Dalton-Trans-2009/ deposition.	7001655.cif