Crystallography Open Database

Information card for entry 7012489

Preview

Coordinates	7012489.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C23 H41 N3 Pb Si2
Calculated formula	C23 H41 N3 Pb Si2
SMILES	[Pb]12[n]3c(cccc3C=C(N2[Si](C)(C)C)C(C)(C)C)C=C(N1[Si](C)(C)C)C(C)(C)C
Title of publication	Synthesis and structural characterisation of low-valent Group 14 metal complexes containing tridentate 2,6-pyridyl-bridged bis(1-azaallyl) ligands
Authors of publication	Leung, Wing-Por; Hou, Henry L.; Cheng, Hui; Yang, Qing-Chuan; Li, Hung-Wing; Mak, Thomas C. W.
Journal of publication	Dalton Transactions
Year of publication	2003
Journal issue	8
Pages of publication	1505
a	9.751 ± 0.002 Å
b	12.115 ± 0.002 Å
c	12.609 ± 0.003 Å
α	103.36 ± 0.03°
β	100.73 ± 0.03°
γ	100.66 ± 0.03°
Cell volume	1382.8 ± 0.6 Å³
Cell temperature	294 ± 2 K
Ambient diffraction temperature	294 ± 2 K
Number of distinct elements	5
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.0794
Residual factor for significantly intense reflections	0.0734
Weighted residual factors for significantly intense reflections	0.2011
Weighted residual factors for all reflections included in the refinement	0.2156
Goodness-of-fit parameter for all reflections included in the refinement	0.971
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179828 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/24.	7012489.cif
120443	2014-07-15	Adding 17924 DOIs guessed from source file names.	7012489.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7012489.cif
5312	2011-01-03	cif/ Adding files, updated with the 'cif_fix_enum' program and the cif_core.dic dictionary. The enumerator values were fixed, mostly incorrect case, but also some values that had extra underscores, dashes or spaces. Unfortunately, 22 had non-ASCII characters with the 8-th bit set, and these got incorrectly interpreted as latin1 characters and converted to their UTF8 equivalents by Perl. To fix the structures, however, they need to be redeposited from the original files with the new CIFParser/cif_filter version.	7012489.cif
3896	2010-12-08	cif/7/ Adding CIFs with data from Dalton-Trans-2004-2000/.	7012489.cif