Crystallography Open Database

Information card for entry 7015591

Preview

Coordinates	7015591.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	B Bi Pb S4
Calculated formula	B Bi Pb S4
Title of publication	Syntheses, crystal structures and characterizations of two new quaternary thioborates: PbMBS4 (M = Sb, Bi).
Authors of publication	Geng, Lei; Cheng, Wen-Dan; Zhang, Wei-Long; Li, Ye-Yu; Luo, Zhong-Zhen; Zhang, Hao; Lin, Chen-Sheng; He, Zhang-Zhen
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2011
Journal volume	40
Journal issue	17
Pages of publication	4474 - 4479
a	5.971 ± 0.01 Å
b	6.273 ± 0.009 Å
c	9.132 ± 0.015 Å
α	90°
β	107.75 ± 0.02°
γ	90°
Cell volume	325.8 ± 0.9 Å³
Cell temperature	293 ± 2 K
Ambient diffraction temperature	293 ± 2 K
Number of distinct elements	4
Space group number	11
Hermann-Mauguin space group symbol	P 1 21/m 1
Hall space group symbol	-P 2yb
Residual factor for all reflections	0.043
Residual factor for significantly intense reflections	0.0355
Weighted residual factors for significantly intense reflections	0.0755
Weighted residual factors for all reflections included in the refinement	0.0791
Goodness-of-fit parameter for all reflections included in the refinement	1.141
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179859 (current)	2016-03-25	cif/7/01/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/01/55.	7015591.cif
120112	2014-07-12	Adding DOIs to range 7 structures.	7015591.cif
35909	2012-02-26	cif/7/: reorganising range 7 into a prefix-directory tree.	7015591.cif
21198	2011-06-21	../uploads/cif-deposit/cod/cif Adding structures of 7015591, 7015592 via cif-deposit CGI script.	7015591.cif