Crystallography Open Database

Information card for entry 7024276

Preview

Coordinates	7024276.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C29 H41 Ge N5
Calculated formula	C29 H41 Ge N5
SMILES	[Ge]1(N(c2c(cccc2C(C)C)C(C)C)C(=CC(=[N]1c1c(cccc1C(C)C)C(C)C)C)C)N=N#N
Title of publication	Reactivity of germanium(II) hydride with nitrous oxide, trimethylsilyl azide, ketones, and alkynes and the reaction of a methyl analogue with trimethylsilyl diazomethane.
Authors of publication	Jana, Anukul; Roesky, Herbert W.; Schulzke, Carola
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2010
Journal volume	39
Journal issue	1
Pages of publication	132 - 138
a	16.697 ± 0.003 Å
b	17.006 ± 0.003 Å
c	17.763 ± 0.004 Å
α	101.17 ± 0.03°
β	116.15 ± 0.03°
γ	100.6 ± 0.03°
Cell volume	4229 ± 2 Å³
Cell temperature	133 ± 2 K
Ambient diffraction temperature	133 ± 2 K
Number of distinct elements	4
Space group number	2
Hermann-Mauguin space group symbol	P -1
Hall space group symbol	-P 1
Residual factor for all reflections	0.09
Residual factor for significantly intense reflections	0.0449
Weighted residual factors for significantly intense reflections	0.0905
Weighted residual factors for all reflections included in the refinement	0.1019
Goodness-of-fit parameter for all reflections included in the refinement	0.999
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
179947 (current)	2016-03-25	cif/7/02/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/02/42.	7024276.cif
92343	2014-01-12	cif/ Adding structures of 7024276, 7024277, 7024278, 7024279, 7024280 via cif-deposit CGI script.	7024276.cif