Crystallography Open Database

Information card for entry 7044813

Preview

Coordinates	7044813.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C99.5 H129.5 Dy5 N67.5 Ni10 O44.5
Calculated formula	C80 H82 Dy5 N56 Ni10 O23
Title of publication	High-nuclear heterometallic oxime clusters assembled from triangular subunits: solvothermal syntheses, crystal structures and magnetic properties.
Authors of publication	Dong, Hui-Ming; Zhang, Zhi-Chao; Li, Hai-Yan; Liu, Zhong-Yi; Yang, En-Cui; Zhao, Xiao-Jun
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2017
Journal volume	47
Journal issue	1
Pages of publication	169 - 179
a	26.4358 ± 0.0015 Å
b	26.7521 ± 0.0016 Å
c	21.9223 ± 0.0013 Å
α	90°
β	100.881 ± 0.001°
γ	90°
Cell volume	15225 ± 1.5 Å³
Cell temperature	173 ± 2 K
Ambient diffraction temperature	173 ± 2 K
Number of distinct elements	6
Space group number	15
Hermann-Mauguin space group symbol	C 1 2/c 1
Hall space group symbol	-C 2yc
Residual factor for all reflections	0.0411
Residual factor for significantly intense reflections	0.0322
Weighted residual factors for significantly intense reflections	0.0839
Weighted residual factors for all reflections included in the refinement	0.0874
Goodness-of-fit parameter for all reflections included in the refinement	1.094
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	Yes
Has F_obs	No

Version history

Revision	Date	Message	Files
229378 (current)	2019-11-17	cif/ Updating files of 7044813, 7044814, 7044815, 7044816, 7044817, 7044818 Original log message: Adding full bibliography for 7044813--7044818.cif.	7044813.cif
203404	2017-11-21	cif/ Adding structures of 7044813, 7044814, 7044815, 7044816, 7044817, 7044818 via cif-deposit CGI script.	7044813.cif