Crystallography Open Database

Information card for entry 7045917

Preview

Coordinates	7045917.cif
Original paper (by DOI)	HTML

Structure parameters

Formula	C30 H58 Ge3 Si6
Calculated formula	C30 H58 Ge3 Si6
Title of publication	Spirocyclic germanes via transannular insertion reactions of vinyl germylenes into Si-Si bonds.
Authors of publication	Walewska, Małgorzata; Baumgartner, Judith; Marschner, Christoph; Albers, Lena; Müller, Thomas
Journal of publication	Dalton transactions (Cambridge, England : 2003)
Year of publication	2018
Journal volume	47
Journal issue	17
Pages of publication	5985 - 5996
a	10.817 ± 0.003 Å
b	35.902 ± 0.009 Å
c	10.823 ± 0.003 Å
α	90°
β	96.083 ± 0.005°
γ	90°
Cell volume	4179.5 ± 1.9 Å³
Cell temperature	100 ± 2 K
Ambient diffraction temperature	100 ± 2 K
Number of distinct elements	4
Space group number	14
Hermann-Mauguin space group symbol	P 1 21/n 1
Hall space group symbol	-P 2yn
Residual factor for all reflections	0.1116
Residual factor for significantly intense reflections	0.0894
Weighted residual factors for significantly intense reflections	0.1831
Weighted residual factors for all reflections included in the refinement	0.1923
Goodness-of-fit parameter for all reflections included in the refinement	1.182
Diffraction radiation wavelength	0.71073 Å
Diffraction radiation type	MoKα
Has coordinates	Yes
Has disorder	No
Has F_obs	No

Version history

Revision	Date	Message	Files
229556 (current)	2019-11-17	cif/ Updating files of 7045912, 7045913, 7045914, 7045915, 7045916, 7045917 Original log message: Adding full bibliography for 7045912--7045917.cif.	7045917.cif
207087	2018-03-24	cif/ Adding structures of 7045912, 7045913, 7045914, 7045915, 7045916, 7045917 via cif-deposit CGI script.	7045917.cif