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Information card for entry 7052393
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| Coordinates | 7052393.cif |
|---|---|
| Original paper (by DOI) | HTML |
| Common name | Bis(rubidium-(4,7,13,1621,24-Hexaoxa-1,10- diazabicyclo(8.8.8)hexacosane))-nonagermanid - ammonia(1/4) |
|---|---|
| Chemical name | Bis[rubidium-(4,7,13,1621,24-Hexaoxa-1,10-diazabicyclo[8.8.8]hexacosane)]- nonagermanid - ammonia(1/4) |
| Formula | C36 H84 Ge5 N8 O12 Rb2 |
| Calculated formula | C36 H84 Ge5 N8 O12 Rb2 |
| Title of publication | Ge52? Zintl anions: synthesis and crystal structures of [K([2.2.2]-crypt)]2Ge5?4NH3 and [Rb([2.2.2]-crypt)]2Ge5?4NH3 |
| Authors of publication | Suchentrunk, Christof; Korber, Nikolaus |
| Journal of publication | New Journal of Chemistry |
| Year of publication | 2006 |
| Journal volume | 30 |
| Journal issue | 12 |
| Pages of publication | 1737 |
| a | 11.3169 ± 0.0015 Å |
| b | 12.3333 ± 0.0015 Å |
| c | 20.915 ± 0.003 Å |
| α | 89.183 ± 0.013° |
| β | 83.6 ± 0.02° |
| γ | 78.266 ± 0.015° |
| Cell volume | 2840.3 ± 0.7 Å3 |
| Cell temperature | 123 ± 2 K |
| Ambient diffraction temperature | 123 ± 2 K |
| Number of distinct elements | 6 |
| Space group number | 2 |
| Hermann-Mauguin space group symbol | P -1 |
| Hall space group symbol | -P 1 |
| Residual factor for all reflections | 0.0671 |
| Residual factor for significantly intense reflections | 0.042 |
| Weighted residual factors for significantly intense reflections | 0.0946 |
| Weighted residual factors for all reflections included in the refinement | 0.1013 |
| Goodness-of-fit parameter for all reflections included in the refinement | 0.883 |
| Diffraction radiation wavelength | 0.71073 Å |
| Diffraction radiation type | MoKα |
| Has coordinates | Yes |
| Has disorder | No |
| Has Fobs | No |
| Revision | Date | Message | Files |
|---|---|---|---|
| 180077 (current) | 2016-03-26 | cif/7/05/ (antanas@kurmis) Replacing _[local]_cod_* tags with their equivalents from the COD CIF dictionary in multiple entries in subrange 7/05/23. |
7052393.cif |
| 120112 | 2014-07-12 | Adding DOIs to range 7 structures. | 7052393.cif |
| 35909 | 2012-02-26 | cif/7/: reorganising range 7 into a prefix-directory tree. | 7052393.cif |
| 1504 | 2010-09-08 | cif/7/ Adding data extracted from RSC 2005 and 2006 year publications. |
7052393.cif |
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Users of the data should acknowledge the original authors of the
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