#------------------------------------------------------------------------------ #$Date: 2016-03-26 03:40:22 +0200 (Sat, 26 Mar 2016) $ #$Revision: 180191 $ #$URL: file:///home/coder/svn-repositories/cod/cif/7/10/87/7108712.cif $ #------------------------------------------------------------------------------ # # This file is available in the Crystallography Open Database (COD), # http://www.crystallography.net/ # # All data on this site have been placed in the public domain by the # contributors. # data_7108712 loop_ _publ_author_name 'Mirela Pascu' 'Albert Ruggi' 'Rosario Scopelliti' 'Kay Severin' _publ_section_title ; Synthesis of borasiloxane-based macrocycles by multicomponent condensation reactions in solution or in a ball mill ; _journal_name_full Chem.Commun. _journal_page_first 45 _journal_paper_doi 10.1039/c2cc37538a _journal_volume 49 _journal_year 2013 _chemical_formula_moiety 'C30 H46 B2 O6 Si2' _chemical_formula_sum 'C30 H46 B2 O6 Si2' _chemical_formula_weight 580.47 _space_group_IT_number 2 _symmetry_cell_setting triclinic _symmetry_space_group_name_Hall '-P 1' _symmetry_space_group_name_H-M 'P -1' _atom_sites_solution_hydrogens geom _atom_sites_solution_primary direct _atom_sites_solution_secondary difmap _audit_creation_method SHELXL-97 _audit_update_record ; 2012-10-30 # Formatted by publCIF ; _cell_angle_alpha 109.911(7) _cell_angle_beta 94.902(8) _cell_angle_gamma 109.903(7) _cell_formula_units_Z 1 _cell_length_a 8.4713(9) _cell_length_b 10.5851(7) _cell_length_c 10.6720(11) _cell_measurement_reflns_used 161 _cell_measurement_temperature 100(2) _cell_measurement_theta_max 22 _cell_measurement_theta_min 3 _cell_volume 823.76(15) _computing_cell_refinement 'Dirax/lsq (Duisenberg & Schreurs, 1989-2000)' _computing_data_collection 'Collect (Bruker AXS BV, 1997-2004)' _computing_data_reduction 'EvalCCD (Duisenberg & Schreurs, 1990-2000)' _computing_molecular_graphics 'Bruker SHELXTL' _computing_publication_material 'Bruker SHELXTL' _computing_structure_refinement 'SHELXL-97 (Sheldrick, 1997)' _computing_structure_solution 'SHELXS-97 (Sheldrick, 1990)' _diffrn_ambient_temperature 100(2) _diffrn_measured_fraction_theta_full 0.993 _diffrn_measured_fraction_theta_max 0.993 _diffrn_measurement_device_type 'Bruker APEX II CCD' _diffrn_measurement_method 'phi and omega scans' _diffrn_radiation_monochromator graphite _diffrn_radiation_source 'fine-focus sealed tube' _diffrn_radiation_type MoK\a _diffrn_radiation_wavelength 0.71073 _diffrn_reflns_av_R_equivalents 0.0353 _diffrn_reflns_av_sigmaI/netI 0.0484 _diffrn_reflns_limit_h_max 11 _diffrn_reflns_limit_h_min -11 _diffrn_reflns_limit_k_max 13 _diffrn_reflns_limit_k_min -13 _diffrn_reflns_limit_l_max 13 _diffrn_reflns_limit_l_min -13 _diffrn_reflns_number 10453 _diffrn_reflns_theta_full 27.50 _diffrn_reflns_theta_max 27.50 _diffrn_reflns_theta_min 3.23 _exptl_absorpt_coefficient_mu 0.146 _exptl_absorpt_correction_T_max 0.7456 _exptl_absorpt_correction_T_min 0.6356 _exptl_absorpt_correction_type multi-scan _exptl_absorpt_process_details 'SADABS 2008, Bruker AXS, 2008' _exptl_crystal_colour colourless _exptl_crystal_density_diffrn 1.170 _exptl_crystal_density_method 'not measured' _exptl_crystal_description prismatic _exptl_crystal_F_000 312 _exptl_crystal_size_max 0.26 _exptl_crystal_size_mid 0.20 _exptl_crystal_size_min 0.09 _refine_diff_density_max 0.577 _refine_diff_density_min -0.357 _refine_diff_density_rms 0.054 _refine_ls_extinction_method none _refine_ls_goodness_of_fit_ref 1.078 _refine_ls_hydrogen_treatment constr _refine_ls_matrix_type full _refine_ls_number_parameters 230 _refine_ls_number_reflns 3753 _refine_ls_number_restraints 330 _refine_ls_restrained_S_all 1.073 _refine_ls_R_factor_all 0.0682 _refine_ls_R_factor_gt 0.0485 _refine_ls_shift/su_max 0.000 _refine_ls_shift/su_mean 0.000 _refine_ls_structure_factor_coef Fsqd _refine_ls_weighting_details 'calc w=1/[\s^2^(Fo^2^)+(0.0444P)^2^+0.4927P] where P=(Fo^2^+2Fc^2^)/3' _refine_ls_weighting_scheme calc _refine_ls_wR_factor_gt 0.1089 _refine_ls_wR_factor_ref 0.1194 _reflns_number_gt 2981 _reflns_number_total 3753 _reflns_threshold_expression >2sigma(I) _iucr_refine_instructions_details ; TITL MP016 in P-1 CELL 0.71073 8.4713 10.5851 10.6720 109.9111 94.9023 109.9031 ZERR 1.00 0.0009 0.0007 0.0011 0.0067 0.0083 0.0066 LATT 1 SFAC C H B O SI UNIT 30 46 2 6 2 REM ---------------------------------------------------------- REM Data collection: Bruker Nonius APEX II CCD REM Absorption correction: SADABS REM Crystal habit: prismatic; Crystal colour: colourless REM ---------------------------------------------------------- L.S. 10 OMIT 0 -1 1 OMIT 0 1 0 OMIT 0 0 1 OMIT 1 0 0 OMIT -1 1 0 OMIT -1 0 1 ACTA CONF SIZE 0.265 0.199 0.093 WPDB -2 BOND $H FMAP 2 PLAN 20 TEMP -173 SIMU 0.005 C9A > C15B ISOR 0.003 C9A > C15B WGHT 0.044400 0.492700 FVAR 1.37133 0.29809 SI1 5 0.380931 0.390183 0.116999 11.00000 0.01436 0.01538 = 0.01426 0.00557 0.00002 0.00245 O1 4 0.314246 0.333325 -0.049276 11.00000 0.02088 0.01879 = 0.01703 0.00671 -0.00011 0.00310 O2 4 0.425568 0.477593 -0.176420 11.00000 0.01776 0.01822 = 0.01927 0.00707 -0.00059 0.00149 B1 3 0.302144 0.364782 -0.162273 11.00000 0.01459 0.01376 = 0.01684 0.00398 0.00354 0.00581 C1 1 0.405700 0.231116 0.146219 11.00000 0.02018 0.01785 = 0.02027 0.00900 0.00168 0.00506 C2 1 0.242107 0.090003 0.077368 11.00000 0.02496 0.01901 = 0.04016 0.01336 0.00220 0.00234 AFIX 33 H2A 2 0.261545 0.009933 0.093050 11.00000 -1.50000 H2B 2 0.214568 0.065689 -0.021221 11.00000 -1.50000 H2C 2 0.145861 0.104380 0.116359 11.00000 -1.50000 AFIX 0 C3 1 0.554215 0.205962 0.081791 11.00000 0.02492 0.02462 = 0.04371 0.01597 0.00886 0.01086 AFIX 33 H3A 2 0.574445 0.126583 0.098331 11.00000 -1.50000 H3B 2 0.659190 0.295731 0.123092 11.00000 -1.50000 H3C 2 0.523398 0.179584 -0.016996 11.00000 -1.50000 AFIX 0 C4 1 0.454163 0.266089 0.300247 11.00000 0.05031 0.03109 = 0.02564 0.01538 0.00147 0.01622 AFIX 33 H4A 2 0.357212 0.274551 0.341401 11.00000 -1.50000 H4B 2 0.555300 0.358564 0.344637 11.00000 -1.50000 H4C 2 0.480800 0.187394 0.312664 11.00000 -1.50000 AFIX 0 C5 1 0.231637 0.472474 0.199984 11.00000 0.01966 0.02500 = 0.02360 0.00883 0.00410 0.00854 C6 1 0.296455 0.546993 0.357017 11.00000 0.03974 0.03890 = 0.02433 0.00828 0.00909 0.02079 AFIX 33 H6A 2 0.223354 0.597289 0.396447 11.00000 -1.50000 H6B 2 0.415717 0.618094 0.380557 11.00000 -1.50000 H6C 2 0.291470 0.472935 0.393809 11.00000 -1.50000 AFIX 0 C7 1 0.230363 0.591188 0.146489 11.00000 0.03771 0.03619 = 0.03899 0.01792 0.01107 0.02397 AFIX 33 H7A 2 0.189065 0.546206 0.046719 11.00000 -1.50000 H7B 2 0.347464 0.666152 0.171030 11.00000 -1.50000 H7C 2 0.153754 0.636273 0.187891 11.00000 -1.50000 AFIX 0 C8 1 0.046245 0.358884 0.163348 11.00000 0.02128 0.03998 = 0.04467 0.01293 0.01080 0.01060 AFIX 33 H8A 2 0.043547 0.285602 0.200643 11.00000 -1.50000 H8B 2 0.005189 0.310893 0.063595 11.00000 -1.50000 H8C 2 -0.028411 0.407605 0.202408 11.00000 -1.50000 AFIX 66 PART 1 C9A 1 0.139825 0.271248 -0.293520 21.00000 0.01586 0.01447 = 0.02029 0.00487 0.00761 0.00155 C10A 1 0.131385 0.304186 -0.408722 21.00000 0.02027 0.01821 = 0.01509 0.01061 0.00224 0.00429 AFIX 43 H10A 2 0.223545 0.383456 -0.413079 21.00000 -1.20000 AFIX 65 C11A 1 -0.011899 0.221140 -0.517548 21.00000 0.02144 0.01838 = 0.01364 0.01250 0.00435 0.00358 AFIX 43 H11A 2 -0.017666 0.243652 -0.596283 21.00000 -1.20000 AFIX 65 C12A 1 -0.146744 0.105156 -0.511173 21.00000 0.02030 0.01991 = 0.01629 0.00787 0.00141 0.00923 C13A 1 -0.138306 0.072216 -0.395972 21.00000 0.01860 0.01630 = 0.01824 0.00981 0.00433 0.00281 AFIX 43 H13A 2 -0.230468 -0.007054 -0.391616 21.00000 -1.20000 AFIX 65 C14A 1 0.004976 0.155260 -0.287145 21.00000 0.01969 0.01736 = 0.01629 0.00986 0.00231 0.00688 AFIX 43 H14A 2 0.010743 0.132748 -0.208411 21.00000 -1.20000 AFIX 0 O3A 4 -0.430239 -0.079389 -0.631296 21.00000 0.03738 0.04231 = 0.04421 0.01194 0.00040 0.00802 C15A 1 -0.297615 0.016277 -0.629496 21.00000 0.02336 0.02559 = 0.02170 0.00860 0.00187 0.00780 AFIX 43 H15A 2 -0.290482 0.035269 -0.710104 21.00000 -1.20000 AFIX 66 PART 2 C9B 1 0.131922 0.262291 -0.281835 -21.00000 0.01653 0.01452 = 0.01171 0.00571 0.00183 0.00740 C10B 1 0.111182 0.290560 -0.398829 -21.00000 0.02056 0.01733 = 0.01823 0.00885 0.00451 0.00263 AFIX 43 H10B 2 0.198283 0.369741 -0.407880 -21.00000 -1.20000 AFIX 65 C11B 1 -0.036998 0.202977 -0.502579 -21.00000 0.02559 0.02277 = 0.01666 0.01009 0.00159 0.00734 AFIX 43 H11B 2 -0.051172 0.222298 -0.582539 -21.00000 -1.20000 AFIX 65 C12B 1 -0.164440 0.087123 -0.489336 -21.00000 0.01775 0.01747 = 0.02074 0.00511 0.00181 0.00668 C13B 1 -0.143703 0.058852 -0.372343 -21.00000 0.01867 0.01803 = 0.02093 0.01014 0.00316 0.00140 AFIX 43 H13B 2 -0.230805 -0.020329 -0.363293 -21.00000 -1.20000 AFIX 65 C14B 1 0.004477 0.146435 -0.268592 -21.00000 0.01946 0.01669 = 0.01689 0.00864 0.00231 0.00343 AFIX 43 H14B 2 0.018650 0.127113 -0.188632 -21.00000 -1.20000 AFIX 0 O3B 4 -0.354918 -0.000965 -0.709743 -21.00000 0.04138 0.04417 = 0.03366 0.00897 -0.01189 0.01639 C15B 1 -0.323538 -0.010090 -0.600619 -21.00000 0.02189 0.02551 = 0.02753 0.00690 -0.00142 0.00700 AFIX 43 H15B 2 -0.407565 -0.085707 -0.584615 -21.00000 -1.20000 PART 0 HKLF 4 REM MP016 in P-1 REM R1 = 0.0485 for 2981 Fo > 4sig(Fo) and 0.0682 for all 3753 data REM 230 parameters refined using 330 restraints END WGHT 0.0444 0.4927 REM Highest difference peak 0.577, deepest hole -0.357, 1-sigma level 0.054 Q1 1 0.1736 0.2790 -0.2549 11.00000 0.05 0.58 Q2 1 0.2888 0.4231 0.1659 11.00000 0.05 0.38 Q3 1 -0.2056 0.0628 -0.5308 11.00000 0.05 0.28 Q4 1 0.1499 0.4157 0.1820 11.00000 0.05 0.27 Q5 1 0.4683 0.2184 0.1170 11.00000 0.05 0.27 Q6 1 0.0555 0.2155 -0.2564 11.00000 0.05 0.27 Q7 1 0.4202 0.2953 0.1184 11.00000 0.05 0.25 Q8 1 0.3054 0.3926 -0.0604 11.00000 0.05 0.25 Q9 1 0.2069 0.5222 0.1842 11.00000 0.05 0.24 Q10 1 -0.1047 0.1614 -0.5061 11.00000 0.05 0.24 Q11 1 0.3283 0.3367 0.1825 11.00000 0.05 0.23 Q12 1 -0.1002 0.1280 -0.5231 11.00000 0.05 0.23 Q13 1 0.3999 0.4457 -0.1417 11.00000 0.05 0.22 Q14 1 -0.1701 0.0817 -0.4162 11.00000 0.05 0.22 Q15 1 0.0454 0.2673 -0.4265 11.00000 0.05 0.22 Q16 1 0.2952 0.3265 0.1977 11.00000 0.05 0.21 Q17 1 -0.4501 -0.0851 -0.5550 11.00000 0.05 0.21 Q18 1 -0.1586 0.0616 -0.4407 11.00000 0.05 0.21 Q19 1 0.3271 0.1679 0.1231 11.00000 0.05 0.21 Q20 1 0.5081 0.5143 -0.0196 11.00000 0.05 0.20 ; _cod_data_source_file c2cc37538a.txt _cod_data_source_block mp016 _cod_original_cell_volume 823.76(13) _cod_database_code 7108712 #BEGIN Tags that were not found in dictionaries: _iucr_refine_reflections_details ; -1 0 0 119.052 5.769 1 -2 0 0 103.423 6.331 1 -2 0 0 111.827 7.401 1 2 0 0 103.276 6.600 1 2 0 0 103.092 6.871 1 -3 0 0 1127.77 33.40 1 -3 0 0 1079.89 32.29 1 3 0 0 1113.14 33.01 1 3 0 0 1082.26 32.58 1 3 0 0 1129.07 30.48 3 -4 0 0 316.492 16.457 1 -4 0 0 292.567 12.684 2 4 0 0 305.048 15.954 1 4 0 0 306.989 16.087 1 4 0 0 312.537 13.952 3 -5 0 0 478.059 22.585 1 -5 0 0 497.328 18.791 2 5 0 0 478.071 19.726 3 5 0 0 403.559 21.379 1 5 0 0 487.575 21.749 4 5 0 0 456.391 21.924 1 -6 0 0 6.28338 6.33345 1 -6 0 0 -0.6520 3.1272 2 6 0 0 1.40722 3.86652 3 6 0 0 7.93945 5.92109 4 6 0 0 2.12093 6.51066 1 -7 0 0 307.131 21.688 1 7 0 0 305.942 19.704 4 7 0 0 305.371 21.308 1 -8 0 0 76.0368 12.1087 1 8 0 0 51.4539 9.9202 4 8 0 0 65.2441 10.9651 1 9 0 0 -10.242 7.069 4 10 0 0 -2.8544 8.7545 1 10 0 0 8.74527 8.21625 5 10 -1 0 53.6280 13.1602 1 9 -1 0 27.3592 7.1042 4 9 -1 0 15.3047 7.4211 1 -9 1 0 27.9975 9.1929 1 8 -1 0 16.0511 6.3396 4 8 -1 0 23.1654 9.1622 1 -8 1 0 17.5080 8.6738 1 7 -1 0 25.0691 6.4474 4 7 -1 0 20.4570 6.8761 1 -7 1 0 32.2802 8.0571 1 -7 1 0 18.8720 3.8914 2 6 -1 0 469.223 19.266 3 6 -1 0 463.414 21.270 4 6 -1 0 465.763 24.721 1 -6 1 0 470.423 17.371 2 -6 1 0 490.123 25.799 1 5 -1 0 288.000 18.005 1 5 -1 0 333.601 18.467 1 -5 1 0 299.199 12.038 2 -5 1 0 318.097 18.310 1 4 -1 0 107.615 9.307 1 4 -1 0 113.947 9.974 1 -4 1 0 116.204 9.855 1 3 -1 0 57.7648 6.7945 1 3 -1 0 69.2999 6.6146 1 -3 1 0 71.2340 6.9794 1 -3 1 0 67.5356 6.7973 1 2 -1 0 321.699 13.033 1 2 -1 0 363.224 13.530 1 -2 1 0 335.038 12.944 1 -2 1 0 345.513 13.629 1 1 -1 0 509.733 12.637 2 0 -1 0 0.12457 1.19310 6 0 -1 0 -1.7219 1.2458 2 0 1 0 -3.7670 2.1477 4 0 1 0 -7.1994 3.2371 6 0 1 0 -0.1382 0.4257 1 -1 -1 0 359.452 10.987 1 -1 -1 0 448.120 13.487 2 -1 -1 0 394.528 11.255 1 -1 -1 0 400.587 13.617 3 1 1 0 361.564 10.971 1 1 1 0 380.265 13.389 3 1 1 0 362.474 11.941 5 1 1 0 397.350 11.520 1 -2 -1 0 1354.87 35.08 1 -2 -1 0 1347.95 35.73 2 -2 -1 0 1349.52 35.40 1 2 1 0 1411.07 37.06 3 2 1 0 1402.42 35.46 1 2 1 0 1442.20 35.94 1 -3 -1 0 1687.65 45.28 1 -3 -1 0 1718.50 44.98 2 -3 -1 0 1733.93 46.16 1 3 1 0 1695.03 45.60 1 3 1 0 1773.79 46.60 3 3 1 0 1739.74 46.22 1 -4 -1 0 31.8386 5.8590 1 -4 -1 0 26.1404 4.9679 2 4 1 0 22.6094 5.8436 1 4 1 0 19.6171 5.9823 4 4 1 0 28.3765 5.6526 1 4 1 0 23.5148 5.2233 3 -5 -1 0 -2.9549 4.7544 1 -5 -1 0 5.59387 4.00803 2 5 1 0 1.18399 4.46696 1 5 1 0 -0.1873 4.0114 3 5 1 0 11.5803 5.1290 4 5 1 0 -12.346 5.897 1 -6 -1 0 270.754 17.735 1 6 1 0 244.133 17.806 4 6 1 0 229.790 16.386 1 6 1 0 206.716 15.809 1 -7 -1 0 341.841 22.703 1 7 1 0 346.896 22.812 4 7 1 0 344.150 22.121 1 -8 -1 0 6.63455 7.30947 1 8 1 0 17.1008 6.4940 5 8 1 0 25.4851 7.5398 4 8 1 0 23.7370 9.1924 1 9 1 0 42.4855 11.8525 1 9 1 0 37.7737 9.7850 4 9 1 0 24.5718 9.4959 5 10 -2 0 33.0063 11.5194 1 -10 2 0 27.1560 11.5633 1 9 -2 0 22.0681 6.1211 4 9 -2 0 25.4010 10.0851 1 -9 2 0 12.5872 8.7660 1 8 -2 0 143.335 12.070 4 8 -2 0 109.507 14.676 1 -8 2 0 137.501 16.543 1 7 -2 0 131.829 10.646 4 7 -2 0 129.517 13.943 1 -7 2 0 159.640 15.812 1 6 -2 0 93.6993 8.0810 4 6 -2 0 91.6135 11.5037 1 -6 2 0 96.5269 12.4022 1 -6 2 0 90.2979 5.4426 2 5 -2 0 961.442 35.354 1 -5 2 0 968.558 36.655 1 4 -2 0 70.4981 7.8840 1 4 -2 0 63.4076 7.7244 1 -4 2 0 92.7441 9.1772 1 -4 2 0 70.5565 7.9899 1 3 -2 0 1833.73 48.78 1 3 -2 0 1754.15 48.35 1 -3 2 0 1742.57 48.06 1 -3 2 0 1778.49 49.13 1 -3 2 0 1895.94 40.83 2 2 -2 0 4808.40 108.13 1 2 -2 0 4690.85 107.48 1 -2 2 0 4761.75 107.53 1 -2 2 0 4758.38 108.33 1 1 -2 0 4474.38 100.23 6 -1 2 0 4387.08 100.21 6 0 -2 0 106.907 6.963 2 0 -2 0 114.578 3.881 1 0 -2 0 107.027 7.041 6 0 -2 0 123.945 4.062 1 0 2 0 110.936 7.187 2 0 2 0 120.230 6.702 4 0 2 0 119.548 4.009 1 0 2 0 108.372 7.036 6 -1 -2 0 243.101 7.864 1 -1 -2 0 244.359 7.720 1 -1 -2 0 256.859 11.717 6 -1 -2 0 258.432 10.399 5 -1 -2 0 236.335 11.775 2 -1 -2 0 258.690 12.718 3 1 2 0 241.359 7.730 1 1 2 0 248.000 12.408 4 1 2 0 248.774 10.685 5 -2 -2 0 4671.89 105.54 1 -2 -2 0 4725.63 110.73 3 -2 -2 0 4866.31 110.11 2 -2 -2 0 4745.40 105.65 1 2 2 0 4690.26 113.93 4 2 2 0 4665.13 104.84 5 2 2 0 4699.20 105.94 1 2 2 0 4890.92 111.55 3 -3 -2 0 1624.09 43.40 1 -3 -2 0 1731.95 47.58 2 -3 -2 0 1690.93 44.16 1 3 2 0 1658.35 43.78 1 3 2 0 1621.58 49.49 4 3 2 0 1576.18 44.04 5 3 2 0 1560.70 43.78 1 3 2 0 1720.48 48.78 3 -4 -2 0 83.8198 8.9582 2 -4 -2 0 71.1480 7.5228 1 4 2 0 62.3079 9.1854 4 4 2 0 71.6251 7.8349 1 4 2 0 78.5057 8.6692 5 4 2 0 78.6510 7.7420 1 -5 -2 0 116.279 10.526 1 5 2 0 161.593 14.840 4 5 2 0 136.615 11.697 5 5 2 0 147.657 11.606 1 5 2 0 128.479 11.176 1 -6 -2 0 -2.2848 3.8896 1 6 2 0 1.93122 6.14836 5 6 2 0 -1.3285 4.1973 1 6 2 0 3.35129 6.61949 4 -7 -2 0 22.3605 7.2932 1 7 2 0 21.8500 6.8124 5 7 2 0 27.7887 9.4746 4 7 2 0 19.4512 6.9459 1 8 2 0 100.174 12.811 5 8 2 0 117.729 14.203 1 8 2 0 104.130 15.062 4 9 2 0 15.0765 9.2602 4 9 2 0 -7.0176 7.8506 5 9 2 0 1.08453 6.94320 1 10 -3 0 28.2634 11.4383 1 -10 3 0 17.9761 10.3398 1 9 -3 0 50.9132 11.6306 1 -9 3 0 40.0943 12.0047 1 8 -3 0 -15.062 8.625 1 8 -3 0 -3.6434 3.5330 4 -8 3 0 6.28054 8.45935 1 7 -3 0 322.120 22.569 1 7 -3 0 331.323 15.246 4 -7 3 0 331.796 23.833 1 6 -3 0 2072.78 64.52 1 -6 3 0 2105.50 66.53 1 5 -3 0 76.7044 10.0298 1 -5 3 0 53.7276 9.7150 1 4 -3 0 658.764 26.176 1 -4 3 0 664.937 26.033 1 -4 3 0 678.147 27.455 1 -4 3 0 697.947 18.586 2 3 -3 0 1316.80 37.81 1 3 -3 0 1232.78 37.37 1 -3 3 0 1251.58 37.24 1 -3 3 0 1265.18 38.38 1 -3 3 0 1302.50 32.35 2 -3 3 0 1253.23 38.55 6 -2 3 0 9999.99 221.42 6 1 -3 0 230.421 8.934 1 1 -3 0 221.920 9.772 4 1 -3 0 219.501 12.035 6 1 -3 0 208.720 8.704 1 1 -3 0 212.494 10.949 2 -1 3 0 223.708 10.169 4 -1 3 0 223.577 12.454 6 -1 3 0 217.433 8.764 1 -1 3 0 195.990 11.059 2 -1 3 0 233.549 9.421 1 0 -3 0 868.195 27.697 2 0 -3 0 937.322 21.449 1 0 -3 0 928.638 21.374 1 0 -3 0 888.926 28.206 6 0 3 0 904.596 27.955 4 0 3 0 870.828 28.494 6 0 3 0 876.929 21.380 1 0 3 0 908.828 28.126 2 -1 -3 0 -0.5263 6.0082 1 -1 -3 0 -8.9561 14.0869 6 -1 -3 0 0.35743 2.72065 5 -1 -3 0 0.28075 4.56056 3 1 3 0 5.16790 8.06321 4 1 3 0 -0.7023 4.4955 1 1 3 0 2.74200 3.56891 5 -2 -3 0 141.538 11.655 3 -2 -3 0 121.980 8.548 5 -2 -3 0 113.754 9.639 2 -2 -3 0 115.500 6.258 1 -2 -3 0 120.166 9.770 6 -2 -3 0 134.504 6.738 1 2 3 0 121.261 10.946 4 2 3 0 128.972 9.006 5 2 3 0 135.566 6.693 1 -3 -3 0 301.446 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6 -4 4 0 472.000 16.507 2 -4 4 0 502.182 23.565 1 3 -4 0 1131.71 34.31 1 3 -4 0 1089.93 33.79 1 3 -4 0 1136.70 31.15 2 3 -4 0 1028.43 27.67 4 -3 4 0 1047.49 33.45 1 -3 4 0 1115.12 36.98 6 -3 4 0 1045.92 34.69 1 -3 4 0 1080.89 31.17 2 2 -4 0 111.418 7.759 1 2 -4 0 114.582 6.890 4 2 -4 0 112.394 9.796 6 2 -4 0 120.244 8.628 2 2 -4 0 109.575 7.744 1 -2 4 0 101.001 9.939 6 -2 4 0 102.141 7.473 1 -2 4 0 103.898 8.061 1 -2 4 0 112.209 8.798 2 1 -4 0 2.03830 1.94202 1 1 -4 0 5.11519 4.22024 2 1 -4 0 4.08021 1.98952 1 -1 4 0 1.47470 2.07124 1 -1 4 0 9.63410 3.28336 4 -1 4 0 5.20006 4.04678 6 0 -4 0 3.73154 1.21878 1 0 -4 0 3.92487 3.46015 2 0 -4 0 -1.7351 3.1208 6 0 4 0 10.8047 5.7384 6 0 4 0 3.66573 4.67112 4 0 4 0 6.73965 4.21651 2 0 4 0 2.74565 1.36099 1 -1 -4 0 1036.57 36.21 3 -1 -4 0 1049.19 31.76 5 -1 -4 0 1030.27 34.84 6 1 4 0 1006.51 35.15 4 -2 -4 0 24.7298 2.6858 1 -2 -4 0 18.8173 4.1635 5 -2 -4 0 18.9376 2.5341 1 -2 -4 0 22.6213 7.0702 3 2 4 0 21.4823 2.6925 1 2 4 0 10.2484 6.4879 4 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0 1754.10 47.18 2 3 -5 0 3007.44 75.41 2 3 -5 0 3098.96 79.77 4 3 -5 0 3177.07 77.59 1 -3 5 0 3013.97 78.58 1 -3 5 0 3077.15 83.09 6 -3 5 0 3102.44 77.08 2 -3 5 0 2991.42 77.77 1 2 -5 0 49.1219 5.5473 1 2 -5 0 50.2087 5.2497 1 2 -5 0 59.7981 7.1374 2 -2 5 0 48.3693 7.2851 2 -2 5 0 53.6586 6.4687 1 -2 5 0 56.1024 5.4752 1 -2 5 0 57.6677 9.2488 6 -2 5 0 51.2502 6.1886 4 1 -5 0 1130.90 29.73 1 1 -5 0 1134.78 29.40 1 -1 5 0 1099.01 29.96 1 -1 5 0 1119.86 36.10 4 -1 5 0 1102.45 29.56 1 -1 5 0 1087.49 38.89 6 -1 5 0 1129.18 37.56 2 0 -5 0 59.3479 10.0914 3 0 -5 0 64.0668 6.8298 5 0 5 0 71.8058 9.2295 4 0 5 0 76.4694 10.4518 6 -1 -5 0 122.604 12.061 3 1 5 0 145.005 13.430 4 -2 -5 0 55.8121 9.1469 3 2 5 0 52.1694 8.9222 4 -3 -5 0 378.355 13.338 1 -3 -5 0 374.520 23.348 3 -3 -5 0 387.518 13.552 1 3 5 0 374.976 13.208 1 3 5 0 354.727 13.058 1 3 5 0 401.729 21.154 5 3 5 0 401.393 24.718 4 4 5 0 166.806 9.699 1 4 5 0 169.101 18.065 4 4 5 0 176.105 14.697 5 5 5 0 17.2326 7.5128 5 5 5 0 9.33810 4.19870 1 5 5 0 18.7122 10.1822 4 6 5 0 5.50792 4.04788 1 6 5 0 -6.2416 9.6377 4 6 5 0 17.8825 7.4544 5 7 5 0 8.3337 10.5526 4 10 -6 0 141.354 19.011 1 -10 6 0 117.754 18.986 1 -10 6 0 89.8582 15.1128 6 9 -6 0 4.23709 8.80688 1 -9 6 0 21.4133 11.8731 1 -9 6 0 7.22439 7.45469 6 8 -6 0 83.7086 13.8281 1 -8 6 0 81.0092 13.7887 6 -8 6 0 54.5993 13.3167 1 7 -6 0 24.0470 9.0040 1 -7 6 0 19.0392 9.5349 1 6 -6 0 897.254 37.815 1 -6 6 0 910.919 40.196 1 -6 6 0 903.428 40.465 6 5 -6 0 1353.80 46.02 1 -5 6 0 1327.85 47.81 1 -5 6 0 1235.08 38.58 2 -5 6 0 1397.11 50.24 6 4 -6 0 1107.35 40.56 2 4 -6 0 1149.96 38.40 1 -4 6 0 1088.51 39.52 1 -4 6 0 1140.65 43.18 6 -4 6 0 1107.58 38.20 1 -4 6 0 1127.98 36.57 2 3 -6 0 816.790 28.390 1 -3 6 0 819.527 28.327 1 -3 6 0 768.780 33.703 6 -3 6 0 825.926 29.973 1 -3 6 0 752.917 29.232 2 2 -6 0 641.139 21.948 1 -2 6 0 655.047 27.543 2 -2 6 0 659.737 25.381 4 -2 6 0 647.463 22.385 1 -2 6 0 640.160 23.038 1 -2 6 0 667.132 30.486 6 1 -6 0 -2.0114 5.5400 3 1 -6 0 2.17945 1.91825 1 -1 6 0 -6.2829 6.6921 2 -1 6 0 2.07751 7.12232 6 -1 6 0 0.42926 3.66565 4 -1 6 0 0.00246 2.07646 1 0 -6 0 71.7230 10.0147 3 0 6 0 46.0761 10.0723 6 0 6 0 65.1546 8.9288 4 -1 -6 0 -0.1303 6.4248 3 1 6 0 19.6021 6.8585 4 -2 -6 0 647.469 32.646 3 2 6 0 618.035 32.354 4 3 6 0 443.156 28.493 4 4 6 0 3.07219 6.50866 4 5 6 0 5.51568 9.17078 4 5 6 0 14.5861 6.8220 5 6 6 0 6.6296 10.8688 4 6 6 0 34.2425 9.8011 5 10 -7 0 289.101 25.829 1 -10 7 0 250.171 26.563 1 -10 7 0 296.240 27.539 6 9 -7 0 13.6475 10.4045 1 -9 7 0 25.2544 9.2640 6 8 -7 0 9.53080 8.26593 1 -8 7 0 5.75953 8.79470 6 -8 7 0 -1.9323 9.1795 1 7 -7 0 15.3964 8.1556 1 -7 7 0 28.8655 8.7092 6 -7 7 0 30.1419 10.6775 1 6 -7 0 3.57385 4.69060 1 -6 7 0 6.32616 6.33103 6 -6 7 0 11.9998 4.4479 2 -6 7 0 -7.3778 6.3619 1 5 -7 0 -9.8997 5.6092 1 -5 7 0 -0.3069 4.1883 2 -5 7 0 11.1966 8.9257 6 -5 7 0 2.34953 6.24913 1 4 -7 0 6.33689 5.05481 1 -4 7 0 0.12265 3.73129 1 -4 7 0 7.24971 8.07875 6 -4 7 0 -1.2685 6.1897 1 -4 7 0 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1 -5 2 2362.71 64.31 6 -2 5 -2 1951.81 51.41 1 -2 5 -2 1935.35 57.68 6 -2 5 -2 2067.86 56.36 2 -2 5 -2 2022.44 52.83 1 2 -5 2 1971.20 54.46 2 2 -5 2 2005.61 51.70 1 2 -5 2 1896.29 50.90 1 -3 5 -2 891.564 31.064 1 -3 5 -2 909.594 32.537 1 -3 5 -2 961.545 35.728 6 -3 5 -2 943.534 31.813 2 3 -5 2 939.030 31.609 1 -4 5 -2 179.600 14.822 1 -4 5 -2 187.240 13.994 1 -4 5 -2 214.932 12.977 2 4 -5 2 192.585 14.103 1 -5 5 -2 40.0149 6.0596 2 -5 5 -2 42.9535 9.7066 1 5 -5 2 55.7819 9.4775 1 -6 5 -2 243.699 20.031 1 -6 5 -2 270.543 14.344 2 6 -5 2 278.789 19.999 1 -7 5 -2 415.339 28.142 1 -7 5 -2 398.072 17.619 2 7 -5 2 383.933 25.618 1 -8 5 -2 140.788 17.063 1 8 -5 2 134.487 16.155 1 -9 5 -2 -9.1083 10.4455 1 9 -5 2 30.1194 11.4938 1 -10 5 -2 25.5537 12.2529 1 10 -5 2 39.3225 12.5043 1 8 4 -2 5.15770 8.76810 4 8 4 -2 4.58403 8.05941 5 8 4 -2 5.98832 6.12457 1 7 4 -2 96.2857 14.0296 5 7 4 -2 102.168 15.373 4 7 4 -2 114.765 12.053 1 6 4 -2 198.840 14.146 1 6 4 -2 220.246 18.602 5 6 4 -2 227.468 20.254 4 5 4 -2 304.552 21.484 4 5 4 -2 288.806 19.717 5 5 4 -2 287.592 15.523 1 -5 -4 2 292.014 15.596 1 4 4 -2 539.933 27.658 4 4 4 -2 524.659 19.534 1 4 4 -2 559.349 25.948 5 4 4 -2 525.069 20.340 1 -4 -4 2 531.666 25.824 3 -4 -4 2 549.519 20.311 1 3 4 -2 641.337 20.325 1 3 4 -2 655.500 26.993 5 3 4 -2 789.158 30.022 2 3 4 -2 673.891 29.743 4 -3 -4 2 648.176 27.510 3 -3 -4 2 631.940 20.377 1 -3 -4 2 670.983 25.709 6 -3 -4 2 662.286 20.590 1 2 4 -2 2094.60 57.13 5 2 4 -2 2128.80 60.58 2 2 4 -2 2165.91 61.86 4 2 4 -2 1995.61 48.05 1 -2 -4 2 2022.06 48.25 1 -2 -4 2 2133.85 48.36 1 -2 -4 2 2154.00 56.37 6 1 4 -2 1174.93 38.45 2 1 4 -2 1138.50 35.46 6 1 4 -2 1172.10 38.37 4 1 4 -2 1214.17 36.57 5 -1 -4 2 1147.56 37.40 4 -1 -4 2 1162.95 35.75 5 -1 -4 2 1204.40 35.44 6 -1 -4 2 1135.10 36.66 2 0 4 -2 669.430 24.397 6 0 4 -2 699.276 25.957 2 0 4 -2 704.930 18.576 1 0 -4 2 673.700 23.889 6 0 -4 2 692.934 24.821 4 0 -4 2 687.027 25.009 2 0 -4 2 672.242 17.991 1 0 -4 2 623.119 17.771 1 0 -4 2 696.720 23.777 5 -1 4 -2 7640.54 173.13 6 -1 4 -2 7675.91 171.45 2 1 -4 2 7556.90 170.17 2 -2 4 -2 65.5927 6.8520 1 -2 4 -2 50.1225 6.8100 2 -2 4 -2 60.0124 6.3677 1 2 -4 2 51.7436 5.8757 1 2 -4 2 53.4793 6.0454 1 -3 4 -2 124.276 11.079 1 -3 4 -2 116.420 9.336 1 -3 4 -2 132.617 9.570 2 3 -4 2 127.118 10.244 1 3 -4 2 127.513 9.791 1 -4 4 -2 5.29433 6.20349 1 4 -4 2 4.62638 5.56250 1 -5 4 -2 684.406 31.169 1 5 -4 2 635.163 29.180 1 -6 4 -2 458.116 26.723 1 6 -4 2 461.760 25.600 1 -7 4 -2 78.1654 13.3038 1 7 -4 2 62.3612 11.8857 1 -8 4 -2 75.1627 13.9724 1 8 -4 2 49.8913 11.9612 1 -9 4 -2 149.722 19.640 1 9 -4 2 157.080 19.073 1 10 -4 2 21.1357 9.2568 1 9 3 -2 17.9320 8.4666 1 9 3 -2 21.9045 9.1508 4 9 3 -2 27.5229 8.9767 5 8 3 -2 187.471 17.278 1 8 3 -2 236.585 20.397 5 8 3 -2 225.502 21.326 4 7 3 -2 26.4975 9.5393 5 7 3 -2 35.7028 8.3386 1 7 3 -2 24.5050 9.0179 4 6 3 -2 55.1152 9.5796 4 6 3 -2 55.8517 10.0604 5 6 3 -2 34.0052 7.0301 1 -6 -3 2 50.5147 7.9796 1 5 3 -2 51.7986 7.5895 1 5 3 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1604.12 42.62 2 0 3 -2 1567.98 37.27 1 0 3 -2 1543.70 40.55 6 0 -3 2 1413.97 36.44 1 0 -3 2 1640.48 40.73 6 0 -3 2 1517.26 36.70 1 0 -3 2 1501.91 41.41 2 0 -3 2 1509.31 39.78 5 -1 3 -2 525.933 17.341 1 -1 3 -2 519.340 19.239 2 -1 3 -2 509.398 16.928 1 1 -3 2 528.999 16.968 1 1 -3 2 479.545 16.458 1 -2 3 -2 -0.3536 4.2560 1 -2 3 -2 5.17541 3.79522 1 2 -3 2 4.83160 3.72265 1 2 -3 2 10.1694 4.3398 1 -3 3 -2 11.7507 5.1209 1 -3 3 -2 11.2234 3.6869 1 3 -3 2 9.54627 4.59643 1 3 -3 2 6.74091 3.39059 1 -4 3 -2 26.7231 7.2380 1 4 -3 2 6.52932 5.36381 1 -5 3 -2 495.288 25.180 1 5 -3 2 489.505 24.317 1 6 -3 2 16.4199 6.2616 1 -7 3 -2 78.0984 12.4348 1 7 -3 2 54.1728 10.9145 1 -8 3 -2 60.4376 11.5176 1 8 -3 2 86.3066 13.1357 1 -9 3 -2 9.54059 7.21060 1 9 -3 2 13.4475 7.7128 1 -10 3 -2 44.0546 11.9595 1 10 -3 2 64.8992 13.1525 1 9 2 -2 120.311 15.193 1 9 2 -2 137.380 15.946 4 9 2 -2 103.751 15.681 5 8 2 -2 283.864 22.357 4 8 2 -2 288.709 21.488 1 8 2 -2 286.167 22.751 5 7 2 -2 720.607 34.872 5 7 2 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1 2 -2 475.004 14.637 1 1 2 -2 480.088 17.015 2 1 2 -2 448.324 16.551 5 1 2 -2 465.518 14.004 6 1 2 -2 451.543 14.138 1 -1 -2 2 470.254 14.064 1 -1 -2 2 487.496 17.123 5 -1 -2 2 453.942 17.036 4 -1 -2 2 448.866 16.654 2 -1 -2 2 478.340 14.486 1 -1 -2 2 451.883 13.763 6 0 2 -2 41.1529 4.1624 1 0 2 -2 40.6176 3.9964 1 0 2 -2 39.6826 4.6219 5 0 -2 2 40.9327 4.1094 1 0 -2 2 41.0250 3.8215 1 0 -2 2 34.9972 4.2821 5 -1 2 -2 396.083 14.334 1 -1 2 -2 388.047 14.403 1 1 -2 2 356.583 13.816 1 1 -2 2 379.482 14.009 1 -2 2 -2 83.2192 7.5424 1 -2 2 -2 95.2407 8.2925 1 2 -2 2 102.933 8.072 1 2 -2 2 86.1201 7.6387 1 -3 2 -2 744.273 26.658 1 -3 2 -2 759.031 27.505 1 3 -2 2 770.013 27.172 1 3 -2 2 739.365 26.699 1 -4 2 -2 44.7040 7.8840 1 4 -2 2 36.7334 7.3832 1 4 -2 2 48.5171 8.1010 1 -5 2 -2 89.7232 10.3484 1 5 -2 2 84.1980 10.0721 1 -6 2 -2 9.31736 7.70597 1 6 -2 2 12.4589 7.1125 1 -7 2 -2 28.6050 9.1570 1 7 -2 2 30.8207 9.1116 1 -8 2 -2 9.14770 6.82176 1 8 -2 2 3.29794 5.80280 1 -9 2 -2 56.9545 12.1071 1 9 -2 2 45.5544 11.5970 1 9 -2 2 50.7442 9.8563 4 -10 2 -2 7.39013 9.13816 1 10 -2 2 -0.2320 8.5912 1 9 1 -2 194.347 19.697 1 9 1 -2 216.031 18.927 4 9 1 -2 220.402 20.913 5 8 1 -2 282.708 21.721 1 8 1 -2 263.920 19.933 4 -8 -1 2 257.981 21.096 1 7 1 -2 632.873 29.429 4 7 1 -2 598.452 29.827 1 -7 -1 2 587.563 30.112 1 6 1 -2 1907.64 58.28 4 6 1 -2 1866.71 58.36 1 -6 -1 2 1864.06 59.05 1 -6 -1 2 1952.54 51.42 2 5 1 -2 1519.96 49.96 1 5 1 -2 1690.82 50.71 1 5 1 -2 1748.26 51.01 4 -5 -1 2 1735.18 51.65 1 -5 -1 2 1660.75 44.78 2 4 1 -2 234.780 11.401 2 4 1 -2 213.675 13.377 1 4 1 -2 242.829 13.480 4 4 1 -2 237.419 13.619 1 -4 -1 2 243.949 11.415 2 -4 -1 2 217.069 13.365 1 3 1 -2 145.822 9.650 1 3 1 -2 149.900 9.495 4 3 1 -2 147.187 9.863 1 3 1 -2 157.245 8.598 2 -3 -1 2 145.639 9.255 1 -3 -1 2 153.109 9.484 4 -3 -1 2 157.393 8.375 2 -3 -1 2 157.136 7.904 3 -3 -1 2 158.635 10.031 1 2 1 -2 185.352 9.504 1 2 1 -2 178.036 8.712 2 2 1 -2 172.575 9.466 1 -2 -1 2 177.551 9.296 4 -2 -1 2 171.339 8.829 1 -2 -1 2 178.020 9.373 1 1 1 -2 554.395 17.039 5 1 1 -2 562.084 17.016 1 1 1 -2 571.509 17.476 1 -1 -1 2 568.768 17.300 1 -1 -1 2 542.542 16.666 1 -1 1 -2 110.003 7.224 1 -1 1 -2 110.302 7.067 1 1 -1 2 109.162 6.941 1 1 -1 2 96.0766 6.7415 1 -2 1 -2 1104.06 32.12 1 -2 1 -2 1096.03 32.43 1 2 -1 2 1102.47 32.25 1 2 -1 2 1039.18 31.61 1 -3 1 -2 2011.81 54.83 1 -3 1 -2 2041.91 54.41 1 3 -1 2 1974.92 54.26 1 3 -1 2 1945.42 54.02 1 -4 1 -2 444.377 21.187 1 4 -1 2 439.195 20.759 1 4 -1 2 388.922 19.871 1 -5 1 -2 18.8103 7.2608 1 5 -1 2 17.6200 6.9449 1 -6 1 -2 38.1266 9.3271 1 -7 1 -2 223.137 19.430 1 7 -1 2 265.401 20.574 1 -8 1 -2 13.8653 8.0098 1 8 -1 2 13.3770 8.6415 1 -9 1 -2 2.87581 8.28797 1 9 -1 2 18.8610 10.1235 1 9 -1 2 24.4119 7.7213 4 10 0 -2 28.3044 9.3298 1 9 0 -2 78.2731 11.3520 4 9 0 -2 83.2499 13.9571 1 8 0 -2 36.6629 7.6968 4 8 0 -2 31.2663 9.0298 1 -8 0 2 30.2091 9.1266 1 7 0 -2 837.281 37.041 1 7 0 -2 930.831 34.634 4 -7 0 2 878.392 38.468 1 6 0 -2 2183.47 60.89 4 6 0 -2 2165.39 64.76 1 -6 0 2 2101.36 65.32 1 -6 0 2 2149.10 52.35 2 5 0 -2 264.792 16.091 1 5 0 -2 276.766 14.390 4 5 0 -2 243.928 16.367 1 -5 0 2 290.467 11.119 2 -5 0 2 280.568 16.941 1 4 0 -2 -4.0831 3.2041 4 4 0 -2 7.20148 3.95816 1 4 0 -2 -0.2763 3.7859 1 -4 0 2 -1.9116 3.5786 1 3 0 -2 111.875 5.567 2 3 0 -2 117.703 9.027 1 3 0 -2 116.775 9.198 1 -3 0 2 128.630 10.904 1 -3 0 2 119.185 8.585 1 -3 0 2 105.368 6.720 4 2 0 -2 230.236 12.487 1 2 0 -2 210.220 10.756 1 -2 0 2 222.118 12.001 1 -2 0 2 212.523 10.309 1 -2 0 2 208.860 7.018 6 1 0 -2 2386.10 56.94 1 1 0 -2 2373.87 57.54 1 1 0 -2 2415.78 53.36 6 -1 0 2 2448.93 57.04 1 -1 0 2 2403.00 57.39 1 0 0 -2 500.225 16.800 1 0 0 -2 512.382 16.620 1 0 0 2 503.222 16.856 1 0 0 2 517.438 16.582 1 -1 0 -2 668.213 21.539 1 -1 0 -2 682.017 21.740 1 1 0 2 714.575 22.099 1 1 0 2 662.316 21.560 1 -2 0 -2 478.144 18.226 1 -2 0 -2 462.573 18.119 1 2 0 2 477.082 18.222 1 2 0 2 488.296 18.659 1 -3 0 -2 330.039 16.078 1 -3 0 -2 341.904 16.161 1 3 0 2 298.388 15.496 1 3 0 2 310.071 15.708 1 -4 0 -2 8.84854 5.18773 1 4 0 2 5.82777 5.16013 1 5 0 2 0.97448 5.86074 1 5 0 2 3.67806 5.10790 1 -6 0 -2 888.457 37.975 1 6 0 2 910.188 37.661 1 -7 0 -2 491.130 28.318 1 7 0 2 454.812 27.167 1 -8 0 -2 -1.8651 7.5095 1 9 0 2 259.151 23.090 1 9 0 2 296.832 24.512 4 10 -1 -2 -13.111 9.950 1 -10 1 2 -6.5702 9.0716 1 9 -1 -2 225.076 21.495 1 -9 1 2 216.713 21.613 1 8 -1 -2 615.805 26.575 4 8 -1 -2 599.973 32.543 1 -8 1 2 596.929 33.452 1 7 -1 -2 112.844 9.767 4 7 -1 -2 116.885 13.051 1 -7 1 2 121.818 13.720 1 6 -1 -2 502.481 26.047 1 6 -1 -2 568.745 21.392 4 -6 1 2 547.151 27.661 1 5 -1 -2 225.539 15.118 1 -5 1 2 231.894 15.719 1 4 -1 -2 4697.45 114.96 1 4 -1 -2 4728.45 116.04 1 -4 1 2 4893.28 116.56 1 3 -1 -2 4736.59 109.07 1 3 -1 -2 4591.29 109.74 1 -3 1 2 4627.54 109.61 1 -3 1 2 4526.77 108.33 1 2 -1 -2 7866.69 174.96 1 1 -1 -2 4.20835 3.12613 6 1 -1 -2 3.29500 3.66454 1 1 -1 -2 12.7125 4.5558 1 0 -1 -2 514.859 17.404 1 0 -1 -2 515.452 17.246 1 0 1 2 526.335 17.308 1 0 1 2 513.867 17.605 1 -1 -1 -2 -0.8899 2.5721 1 -1 -1 -2 2.41618 1.18988 5 -1 -1 -2 3.55829 2.86677 1 1 1 2 -1.7662 2.5191 1 1 1 2 7.35370 3.33689 1 -2 -1 -2 372.968 15.866 1 -2 -1 -2 385.773 16.010 1 2 1 2 358.193 15.758 1 2 1 2 395.993 12.419 5 2 1 2 393.259 16.193 1 -3 -1 -2 188.796 11.455 1 3 1 2 187.495 11.605 1 3 1 2 189.883 9.371 5 3 1 2 167.120 11.682 1 -4 -1 -2 37.4025 6.5434 1 4 1 2 50.9896 7.6037 1 4 1 2 54.0830 5.9833 5 4 1 2 47.9879 7.4557 1 -5 -1 -2 201.189 15.031 1 5 1 2 216.688 13.410 5 5 1 2 175.492 14.246 1 5 1 2 209.951 15.787 1 -6 -1 -2 367.869 22.426 1 6 1 2 371.710 19.672 5 6 1 2 367.815 22.016 1 -7 -1 -2 24.3055 7.9468 1 7 1 2 22.1714 7.1532 5 8 1 2 87.8413 13.6490 1 8 1 2 81.0189 14.2076 4 9 1 2 463.288 30.486 1 9 1 2 496.852 33.538 4 10 -2 -2 4.85929 7.06441 1 -10 2 2 18.8770 9.3143 1 9 -2 -2 285.925 23.810 1 -9 2 2 284.964 24.382 1 8 -2 -2 8.11126 7.93774 1 -8 2 2 -7.7506 8.5257 1 7 -2 -2 139.549 14.412 1 -7 2 2 134.142 14.663 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33.76 1 -3 -2 -2 481.375 19.826 1 3 2 2 491.581 17.864 5 3 2 2 484.916 20.169 1 3 2 2 478.077 20.355 1 -4 -2 -2 679.751 26.834 1 4 2 2 715.315 27.391 1 4 2 2 666.909 23.998 5 4 2 2 638.021 26.986 1 -5 -2 -2 -5.3733 5.0714 1 5 2 2 8.79001 4.68199 5 5 2 2 -1.8532 5.7068 1 -6 -2 -2 29.6840 7.4296 1 6 2 2 20.6728 5.6575 5 6 2 2 18.3921 6.8054 1 7 2 2 78.6065 11.9371 1 7 2 2 68.7359 13.7910 4 7 2 2 89.0268 11.2181 5 8 2 2 824.467 44.403 4 8 2 2 781.565 38.752 1 10 -3 -2 74.2349 13.5047 1 -10 3 2 68.5588 13.8277 1 9 -3 -2 706.835 38.434 1 -9 3 2 609.602 37.246 1 8 -3 -2 73.2510 12.9918 1 -8 3 2 82.5117 13.8426 1 7 -3 -2 50.0179 10.5123 1 -7 3 2 53.6758 11.1571 1 6 -3 -2 -14.548 7.667 1 -6 3 2 0.99001 7.07824 1 -6 3 2 -0.1349 4.9259 6 5 -3 -2 19.1570 7.1249 1 -5 3 2 14.2625 5.4009 6 4 -3 -2 192.963 8.381 3 4 -3 -2 187.216 7.749 2 4 -3 -2 207.219 13.650 1 -4 3 2 205.704 14.116 1 -4 3 2 174.579 12.121 6 3 -3 -2 1040.73 29.46 2 3 -3 -2 1055.45 34.86 1 3 -3 -2 1104.00 30.36 3 3 -3 -2 1079.92 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19.574 1 -1 6 -3 -9.9735 5.2851 2 -1 6 -3 2.32245 2.65271 1 -1 6 -3 2.57640 2.98165 1 -1 6 -3 -0.9107 5.3750 6 1 -6 3 -2.4316 2.2194 1 1 -6 3 2.68311 2.10855 1 -2 6 -3 18.1016 5.3689 1 -2 6 -3 17.4138 7.3935 6 -2 6 -3 9.09670 5.91977 2 -2 6 -3 7.74365 3.84325 1 -3 6 -3 28.4830 6.8711 2 -3 6 -3 6.27682 5.42038 6 -3 6 -3 17.5738 6.4495 1 -3 6 -3 25.5606 5.1990 1 3 -6 3 12.9893 5.0322 1 -4 6 -3 206.241 16.291 1 -4 6 -3 240.845 15.868 2 4 -6 3 199.456 15.213 1 -5 6 -3 349.614 22.933 1 -5 6 -3 329.818 18.360 2 5 -6 3 327.673 21.004 1 -6 6 -3 2.58905 3.45000 2 -6 6 -3 -6.6792 8.5922 1 6 -6 3 6.84176 7.53673 1 -7 6 -3 236.900 22.096 1 -7 6 -3 221.048 14.698 2 7 -6 3 229.053 20.199 1 -8 6 -3 74.1601 8.4740 2 -8 6 -3 65.7665 14.8197 1 8 -6 3 89.8452 14.9111 1 -9 6 -3 89.9027 15.4433 1 9 -6 3 65.2795 12.9132 1 -10 6 -3 278.362 28.454 1 10 -6 3 283.422 27.256 1 8 5 -3 140.886 18.492 5 7 5 -3 96.8212 10.7033 1 7 5 -3 120.508 15.180 5 6 5 -3 72.9408 8.6039 1 6 5 -3 74.9370 11.5953 5 6 5 -3 74.4498 13.6549 4 5 5 -3 430.214 19.077 1 5 5 -3 469.396 29.108 4 5 5 -3 464.380 26.623 5 -5 -5 3 458.655 25.508 3 4 5 -3 21.9081 9.0161 4 4 5 -3 6.30437 2.80776 1 4 5 -3 2.03585 3.16006 1 4 5 -3 -3.9514 5.1106 5 -4 -5 3 11.5061 6.7296 3 -4 -5 3 6.81983 3.07074 1 3 5 -3 -4.6200 6.5068 5 3 5 -3 5.39483 2.42550 1 3 5 -3 13.5564 7.9848 2 -3 -5 3 8.33065 2.46988 1 -3 -5 3 7.66429 2.22654 1 2 5 -3 1383.97 44.29 5 2 5 -3 1349.54 41.98 6 2 5 -3 1312.11 33.28 1 2 5 -3 1391.53 47.08 2 -2 -5 3 1378.73 41.13 6 -2 -5 3 1276.82 33.16 1 -2 -5 3 1383.92 33.14 1 1 5 -3 114.005 11.073 5 1 5 -3 104.914 9.533 6 1 5 -3 98.2555 5.3778 1 1 5 -3 104.481 11.052 2 -1 -5 3 88.2902 8.2638 6 -1 -5 3 80.6050 4.8301 1 -1 -5 3 87.7188 4.7191 1 0 5 -3 736.218 21.484 1 0 5 -3 693.198 29.050 2 0 5 -3 714.186 27.216 6 0 5 -3 730.924 21.675 1 0 -5 3 752.825 26.842 6 0 -5 3 695.990 20.814 1 0 -5 3 699.274 20.671 1 -1 5 -3 1137.29 39.48 2 -1 5 -3 1209.46 33.91 1 -1 5 -3 1276.56 35.42 1 -1 5 -3 1200.55 39.18 6 1 -5 3 1153.23 33.68 1 1 -5 3 1258.87 33.60 1 -2 5 -3 316.182 17.948 6 -2 5 -3 341.663 16.204 1 -2 5 -3 317.566 17.451 2 -2 5 -3 310.160 15.197 1 2 -5 3 307.335 14.915 1 2 -5 3 314.371 15.051 1 -3 5 -3 558.414 23.537 1 -3 5 -3 615.154 25.006 2 -3 5 -3 612.982 25.596 1 3 -5 3 590.301 24.386 1 -4 5 -3 12.2605 5.6395 1 4 -5 3 7.46586 4.39875 1 -5 5 -3 -7.3482 5.6920 1 5 -5 3 -2.6857 4.6894 1 -6 5 -3 92.2752 12.7788 1 6 -5 3 72.4967 10.8708 1 -7 5 -3 556.428 33.212 1 7 -5 3 529.369 30.842 1 -8 5 -3 240.277 23.203 1 8 -5 3 248.965 22.565 1 -9 5 -3 71.6152 15.3017 1 9 -5 3 75.6036 14.7101 1 10 -5 3 -3.4220 9.4137 1 8 4 -3 53.9181 12.9002 5 8 4 -3 49.9599 9.7687 1 7 4 -3 3.81276 4.92224 1 7 4 -3 -5.9503 8.3259 5 6 4 -3 24.8960 9.6283 4 6 4 -3 23.9056 9.1518 5 6 4 -3 19.5924 6.0440 1 5 4 -3 30.0738 8.7372 5 5 4 -3 22.0414 5.6118 1 5 4 -3 21.9670 8.6242 4 -5 -4 3 23.4152 5.4350 1 -5 -4 3 33.5920 7.4868 3 4 4 -3 242.379 17.332 5 4 4 -3 236.813 17.648 4 4 4 -3 226.183 12.431 1 4 4 -3 219.218 15.919 2 4 4 -3 205.565 12.217 1 -4 -4 3 227.956 12.526 1 -4 -4 3 200.665 14.817 3 -4 -4 3 226.826 13.307 6 3 4 -3 157.022 8.993 1 3 4 -3 151.467 9.152 1 3 4 -3 129.306 12.646 2 3 4 -3 152.226 12.438 5 -3 -4 3 154.130 10.044 6 -3 -4 3 136.294 8.446 1 -3 -4 3 147.941 8.461 1 2 4 -3 -1.1386 2.9352 6 2 4 -3 3.22234 2.27345 1 2 4 -3 12.7792 6.2441 2 -2 -4 3 3.20914 1.87868 1 -2 -4 3 0.05756 2.54434 6 -2 -4 3 0.72315 2.01511 1 1 4 -3 496.703 22.079 2 1 4 -3 489.606 15.670 1 1 4 -3 487.838 16.089 1 1 4 -3 487.500 20.649 5 1 4 -3 504.175 19.038 6 -1 -4 3 497.345 20.932 5 -1 -4 3 481.883 18.197 6 -1 -4 3 471.027 21.164 4 -1 -4 3 499.099 15.409 1 -1 -4 3 455.148 15.393 1 -1 -4 3 481.699 20.976 2 0 4 -3 14.8342 4.8636 6 0 4 -3 14.0795 3.3354 1 0 4 -3 13.0656 3.1468 1 0 4 -3 24.1893 6.1986 2 0 -4 3 13.5892 2.8090 1 0 -4 3 14.3990 3.6329 5 -1 4 -3 3300.65 81.49 2 -1 4 -3 3380.64 78.19 1 -1 4 -3 3139.94 80.25 6 -1 4 -3 3149.14 76.75 1 1 -4 3 3095.00 76.71 1 1 -4 3 3254.64 76.46 1 -2 4 -3 5635.44 133.46 1 -2 4 -3 6290.47 136.52 1 2 -4 3 5758.68 134.12 1 2 -4 3 5483.03 132.84 1 -3 4 -3 156.519 12.062 1 -3 4 -3 143.896 11.410 1 3 -4 3 146.269 11.214 1 -4 4 -3 148.967 12.951 1 4 -4 3 155.502 12.656 1 -5 4 -3 67.2595 11.3302 1 5 -4 3 77.8066 11.2443 1 -6 4 -3 127.814 14.882 1 6 -4 3 135.413 14.490 1 -7 4 -3 798.966 39.623 1 7 -4 3 765.620 37.410 1 -8 4 -3 24.8658 8.8933 1 8 -4 3 37.2496 9.7973 1 -9 4 -3 136.303 18.060 1 9 -4 3 141.700 17.640 1 -10 4 -3 108.380 17.351 1 10 -4 3 95.3409 16.2858 1 9 3 -3 194.442 18.539 1 9 3 -3 209.088 20.778 5 8 3 -3 115.860 13.653 1 8 3 -3 108.021 15.110 5 7 3 -3 181.200 17.876 5 7 3 -3 164.105 14.302 1 6 3 -3 -4.7809 5.4890 5 6 3 -3 3.41657 6.57052 4 6 3 -3 5.10804 4.12326 1 -6 -3 3 12.4558 5.0447 1 5 3 -3 54.8295 9.7099 4 5 3 -3 58.3302 7.7813 1 5 3 -3 70.7758 9.9178 5 5 3 -3 78.1884 8.9833 1 -5 -3 3 75.6116 8.7402 3 -5 -3 3 83.9084 8.1625 6 -5 -3 3 77.8015 8.9820 1 4 3 -3 239.305 16.413 5 4 3 -3 249.688 13.711 1 4 3 -3 240.391 13.892 1 4 3 -3 218.798 14.565 2 -4 -3 3 207.262 13.306 3 -4 -3 3 249.703 13.711 1 -4 -3 3 255.515 15.001 2 -4 -3 3 225.985 11.909 6 3 3 -3 1136.02 36.69 2 3 3 -3 1135.09 33.67 1 3 3 -3 1080.94 36.39 5 3 3 -3 1127.24 32.77 1 -3 -3 3 1039.18 30.52 6 -3 -3 3 1102.84 35.64 2 -3 -3 3 1106.16 32.18 1 -3 -3 3 1123.94 32.95 1 2 3 -3 128.087 8.189 1 2 3 -3 137.695 10.897 2 2 3 -3 146.809 10.444 5 2 3 -3 159.710 8.561 1 -2 -3 3 143.999 10.873 4 -2 -3 3 158.215 7.862 6 -2 -3 3 134.191 7.760 1 -2 -3 3 153.106 8.586 1 -2 -3 3 147.264 10.587 2 1 3 -3 194.566 9.533 1 1 3 -3 183.389 11.457 5 1 3 -3 189.247 9.288 1 1 3 -3 187.434 12.109 2 1 3 -3 187.984 9.109 6 -1 -3 3 218.232 12.079 5 -1 -3 3 192.097 9.359 1 -1 -3 3 198.399 9.024 6 -1 -3 3 186.235 8.818 1 0 3 -3 823.552 25.854 5 0 3 -3 832.288 25.087 6 0 3 -3 842.449 25.067 1 0 3 -3 845.479 28.269 2 0 3 -3 789.548 24.400 1 0 -3 3 807.754 24.629 1 0 -3 3 817.975 25.643 5 0 -3 3 827.453 24.310 1 -1 3 -3 1763.65 45.38 1 -1 3 -3 1679.22 44.52 1 1 -3 3 1622.39 44.27 1 1 -3 3 1603.83 43.66 1 -2 3 -3 392.465 17.834 1 -2 3 -3 360.758 16.542 1 2 -3 3 410.169 17.772 1 2 -3 3 351.259 16.174 1 -3 3 -3 413.309 19.305 1 -3 3 -3 422.292 20.123 1 3 -3 3 387.894 19.065 1 3 -3 3 405.334 19.518 1 -4 3 -3 37.8398 8.3870 1 -5 3 -3 152.051 14.690 1 5 -3 3 155.241 14.407 1 -6 3 -3 504.770 27.771 1 6 -3 3 481.666 26.885 1 7 -3 3 9.32505 8.41370 1 -8 3 -3 66.1280 13.7163 1 8 -3 3 69.0872 13.4937 1 -9 3 -3 124.281 16.980 1 9 -3 3 123.821 16.743 1 -10 3 -3 46.1985 12.7714 1 10 -3 3 70.1670 14.4421 1 9 2 -3 73.1109 12.8224 5 9 2 -3 49.6343 11.2660 1 8 2 -3 367.423 24.271 1 8 2 -3 364.594 26.029 5 7 2 -3 52.3850 9.9872 5 7 2 -3 44.4083 9.0503 1 -7 -2 3 34.0532 8.3502 1 6 2 -3 69.9519 11.3504 5 6 2 -3 70.3163 9.8993 1 -6 -2 3 64.1206 7.4502 2 -6 -2 3 54.9314 8.8420 1 5 2 -3 230.356 14.743 1 5 2 -3 222.944 15.437 1 5 2 -3 233.653 13.862 2 5 2 -3 220.089 15.839 5 -5 -2 3 233.782 12.752 3 -5 -2 3 240.479 13.587 2 -5 -2 3 240.661 15.391 1 4 2 -3 790.697 27.990 1 4 2 -3 786.801 29.929 5 4 2 -3 854.061 28.213 2 4 2 -3 792.137 29.173 1 -4 -2 3 788.928 24.002 6 -4 -2 3 832.317 27.727 2 -4 -2 3 773.474 28.215 1 -4 -2 3 775.860 25.814 3 3 2 -3 481.531 20.661 5 3 2 -3 473.949 18.761 1 3 2 -3 484.514 19.442 1 3 2 -3 503.113 19.768 2 -3 -2 3 494.986 18.616 1 -3 -2 3 456.762 14.481 6 -3 -2 3 513.110 19.489 1 -3 -2 3 466.991 19.932 4 2 2 -3 118.446 8.495 2 2 2 -3 105.377 8.468 5 2 2 -3 121.362 8.093 1 2 2 -3 127.858 8.213 1 -2 -2 3 127.216 8.965 4 -2 -2 3 116.809 4.859 6 -2 -2 3 115.706 7.331 1 -2 -2 3 118.132 8.094 1 1 2 -3 1685.44 42.46 1 1 2 -3 1588.23 38.39 6 1 2 -3 1676.29 42.97 1 1 2 -3 1577.97 41.82 5 -1 -2 3 1609.58 42.11 5 -1 -2 3 1659.16 41.97 1 -1 -2 3 1696.25 42.85 1 0 2 -3 290.924 12.964 1 0 2 -3 298.546 13.277 1 0 2 -3 314.646 12.416 5 0 -2 3 307.784 12.074 5 0 -2 3 318.612 13.128 1 0 -2 3 315.400 13.415 1 -1 2 -3 626.395 21.935 1 -1 2 -3 633.760 22.259 1 1 -2 3 646.392 22.210 1 1 -2 3 599.102 17.932 5 1 -2 3 612.696 21.597 1 -2 2 -3 301.469 14.914 1 -2 2 -3 302.971 15.661 1 2 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3 13.9427 5.9117 1 -2 6 3 15.2456 4.4884 1 1 -6 -3 275.031 15.364 1 -1 6 3 281.051 15.030 1 -1 6 3 304.582 17.170 1 -1 6 3 277.710 19.116 4 0 -6 -3 58.8427 6.8300 1 0 6 3 59.8565 11.2176 4 0 6 3 51.0438 7.0324 1 -1 -6 -3 1207.69 36.71 1 1 6 3 1217.90 37.63 1 1 6 3 1168.02 48.78 4 2 6 3 188.105 18.976 4 2 6 3 184.663 11.816 1 3 6 3 155.104 18.191 4 3 6 3 130.592 10.393 1 4 6 3 23.4662 5.5500 1 4 6 3 47.8555 12.0315 4 5 6 3 225.935 24.848 4 10 -7 -3 9.56947 9.70347 1 -10 7 3 -18.086 12.982 1 -10 7 3 -7.8373 6.4562 6 9 -7 -3 102.239 16.388 1 -9 7 3 121.785 17.054 6 -9 7 3 119.863 19.631 1 -8 7 3 44.4600 10.0820 6 -8 7 3 54.6821 12.5509 1 7 -7 -3 32.8878 8.6036 1 -7 7 3 17.5381 8.1166 1 -7 7 3 14.2812 9.1845 6 6 -7 -3 194.571 17.861 1 -6 7 3 192.016 18.903 6 -6 7 3 199.557 19.536 1 5 -7 -3 1.86282 5.16105 3 -5 7 3 4.33017 7.79014 6 4 -7 -3 37.3015 7.7265 1 4 -7 -3 39.4203 9.3304 3 -4 7 3 39.8056 8.6387 1 -4 7 3 45.6031 10.6999 6 -4 7 3 38.0118 6.1907 4 3 -7 -3 547.342 28.750 3 3 -7 -3 537.194 24.745 1 -3 7 3 552.356 25.225 4 -3 7 3 542.044 26.488 1 -3 7 3 544.846 31.714 6 2 -7 -3 503.701 22.522 1 -2 7 3 437.995 24.121 4 -2 7 3 456.865 22.925 1 -2 7 3 466.885 29.963 6 1 -7 -3 97.3216 9.1502 1 -1 7 3 116.794 13.555 4 -1 7 3 89.6786 9.6306 1 0 7 3 1763.45 50.19 1 0 7 3 1659.41 61.23 4 1 7 3 1.02593 3.38665 1 1 7 3 3.89770 6.70983 4 2 7 3 105.621 16.614 4 2 7 3 111.102 8.587 1 3 7 3 84.8644 14.8513 4 4 7 3 309.404 28.103 4 10 -8 -3 12.2702 10.5717 1 -10 8 3 3.84500 7.14660 6 -10 8 3 33.0509 14.2893 1 9 -8 -3 112.934 17.074 1 -9 8 3 96.4662 18.4637 1 -9 8 3 109.618 16.270 6 8 -8 -3 40.3109 11.4884 1 -8 8 3 44.8619 12.0886 6 -8 8 3 58.0279 14.3441 1 7 -8 -3 160.900 17.749 1 -7 8 3 187.470 20.417 6 -7 8 3 165.318 19.684 1 6 -8 -3 17.0554 7.8376 1 6 -8 -3 12.3295 6.1777 3 -6 8 3 -0.2670 7.8512 1 -6 8 3 31.9001 10.6481 6 5 -8 -3 21.9475 7.9730 3 -5 8 3 5.27399 6.85411 1 -5 8 3 15.7510 8.9472 6 4 -8 -3 48.7246 8.4373 1 4 -8 -3 35.2770 9.8244 3 -4 8 3 44.0983 11.8984 6 -4 8 3 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4 43.6991 10.7942 6 5 -7 -4 2.52281 5.86097 1 -5 7 4 12.6803 7.1095 6 -5 7 4 23.9380 9.1737 1 -4 7 4 30.2975 10.4233 6 -4 7 4 27.1967 7.4427 1 3 -7 -4 364.899 21.273 1 -3 7 4 370.129 23.051 1 -3 7 4 343.044 25.881 6 -3 7 4 391.440 21.515 4 2 -7 -4 428.712 22.336 1 -2 7 4 424.707 23.988 1 -2 7 4 390.773 23.907 4 -1 7 4 98.5087 11.0489 1 -1 7 4 63.7924 12.2778 4 0 7 4 187.299 14.130 1 0 7 4 179.311 18.917 4 1 7 4 317.889 17.994 1 1 7 4 355.425 27.426 4 2 7 4 73.3868 8.5073 1 2 7 4 67.1980 13.7845 4 3 7 4 9.46516 8.42216 4 -9 8 4 36.5200 12.1946 6 -9 8 4 45.1842 14.3573 1 8 -8 -4 16.6573 9.5175 1 -8 8 4 10.2878 9.3848 6 -8 8 4 40.2210 13.1892 1 7 -8 -4 608.405 35.235 1 -7 8 4 632.532 38.247 1 -7 8 4 686.010 38.770 6 6 -8 -4 27.4704 8.8552 1 -6 8 4 23.0905 10.2218 1 -5 8 4 7.87812 7.73505 1 -5 8 4 4.86338 8.62728 6 4 -8 -4 4.15366 5.08660 1 -4 8 4 1.90743 8.57006 6 -4 8 4 0.51628 4.15320 4 -4 8 4 -8.2935 6.7995 1 -3 8 4 360.305 28.407 6 -3 8 4 390.014 23.635 1 -3 8 4 389.272 23.087 4 -2 8 4 63.9666 11.6260 4 -2 8 4 56.5968 9.2007 1 -1 8 4 127.156 12.404 1 -1 8 4 115.503 15.522 4 0 8 4 77.9026 9.2643 1 0 8 4 78.3169 14.9218 4 1 8 4 44.6697 12.9310 4 2 8 4 -17.284 11.202 4 9 -9 -4 38.5839 12.1724 1 -9 9 4 15.9689 9.7774 6 -9 9 4 36.2399 13.9638 1 8 -9 -4 377.731 28.917 1 -8 9 4 415.907 32.273 6 -8 9 4 387.598 31.713 1 7 -9 -4 104.221 15.393 1 -7 9 4 154.264 19.653 6 -7 9 4 135.321 19.028 1 -6 9 4 20.2662 11.5770 6 -6 9 4 18.8008 9.7042 1 -5 9 4 45.1904 11.1137 1 -4 9 4 70.2258 12.0458 1 -4 9 4 82.3497 14.8763 6 -3 9 4 21.1337 8.3849 4 -2 9 4 162.444 14.702 1 -2 9 4 154.735 17.010 4 -1 9 4 14.5167 5.6335 1 -1 9 4 7.08543 8.54218 4 0 9 4 215.480 22.521 4 1 9 4 22.3680 9.8239 4 -7 10 4 12.6577 11.1135 6 -7 10 4 19.6963 10.8677 1 -6 10 4 86.5922 17.4716 6 -6 10 4 105.457 15.623 1 -5 10 4 88.0477 13.8264 1 -5 10 4 112.858 19.124 6 -4 10 4 25.1216 8.7436 1 -4 10 4 57.1750 15.3640 6 -3 10 4 16.6554 6.8213 1 -2 10 4 28.5067 9.7006 4 -1 10 4 33.6596 11.7874 4 -5 11 4 302.071 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54.8734 12.0746 1 5 5 -10 72.1106 14.3089 5 5 5 -10 48.2228 11.8893 2 4 5 -10 254.786 21.230 1 4 5 -10 204.612 20.708 2 4 5 -10 242.760 21.352 5 -4 -5 10 248.881 21.242 1 3 5 -10 228.070 18.572 5 3 5 -10 254.997 20.288 1 3 5 -10 201.710 19.959 2 -3 -5 10 246.900 20.098 1 2 5 -10 60.4168 11.7564 1 2 5 -10 30.0609 8.3622 5 -2 -5 10 48.2377 10.6286 1 1 5 -10 28.6978 7.7768 5 1 5 -10 31.2092 10.4092 1 0 5 -10 31.5459 10.3454 1 0 -5 10 -1.5012 6.8477 1 -1 5 -10 107.301 15.270 1 1 -5 10 91.4168 14.4030 1 -2 5 -10 245.212 21.854 1 2 -5 10 238.570 21.441 1 -3 5 -10 9.35849 7.24442 1 3 -5 10 14.7517 7.7330 1 -4 5 -10 15.8340 8.1722 1 4 -5 10 26.5808 9.5602 1 -5 5 -10 50.0679 12.2588 1 5 -5 10 57.7233 12.8880 1 -6 5 -10 141.395 20.303 1 6 -5 10 185.963 23.444 1 7 4 -10 105.910 17.485 5 7 4 -10 130.473 17.460 1 6 4 -10 9.27705 9.94128 5 6 4 -10 2.95689 8.71426 1 5 4 -10 78.3885 13.3349 5 5 4 -10 88.6557 13.2282 1 5 4 -10 69.4612 12.8222 2 -5 -4 10 78.4146 12.7896 1 4 4 -10 66.7566 11.4197 2 4 4 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474.854 35.170 1 -8 1 10 464.988 36.186 1 7 -1 -10 7.68829 7.67634 1 -7 1 10 2.92220 7.41806 1 6 -1 -10 0.53758 8.87902 1 -6 1 10 5.49730 9.93272 1 5 -1 -10 86.3436 15.9202 1 -5 1 10 98.2506 16.8933 1 4 -1 -10 259.223 23.692 1 -4 1 10 234.930 24.396 1 3 -1 -10 32.6403 11.1610 1 -3 1 10 25.4831 11.1205 1 2 -1 -10 34.3825 10.5115 1 -2 1 10 32.2555 11.8219 1 1 -1 -10 -5.2083 6.0514 1 -1 1 10 -2.1196 6.3915 1 0 -1 -10 24.9949 9.8457 1 0 1 10 10.6595 9.3909 1 -1 -1 -10 192.390 20.212 1 1 1 10 194.966 21.393 1 -2 -1 -10 151.770 17.824 1 2 1 10 177.319 20.043 1 3 1 10 8.20318 9.42921 1 8 -2 -10 23.7091 11.6060 1 -8 2 10 1.2108 10.5362 1 7 -2 -10 -5.3529 7.8067 1 -7 2 10 2.04637 7.57427 1 6 -2 -10 39.4372 12.5852 1 -6 2 10 32.1353 13.0413 1 5 -2 -10 98.0947 16.5577 1 -5 2 10 128.243 19.435 1 4 -2 -10 -2.6263 6.1467 1 -4 2 10 18.8546 9.0336 1 3 -2 -10 27.8980 9.4107 1 -3 2 10 41.8201 12.2248 1 2 -2 -10 357.484 26.506 1 -2 2 10 342.864 27.208 1 1 -2 -10 678.591 37.929 1 -1 2 10 669.369 39.506 1 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303.921 22.013 1 3 9 -11 317.998 30.091 2 2 9 -11 39.1052 14.2722 2 2 9 -11 60.7873 11.0129 1 1 9 -11 244.419 25.998 2 1 9 -11 232.867 19.517 1 0 9 -11 3.09632 7.13215 1 0 9 -11 1.27790 7.30812 2 -1 9 -11 4.08985 7.76456 1 -1 9 -11 16.4532 11.2906 2 -2 9 -11 374.170 26.637 6 -2 9 -11 378.295 30.959 2 -2 9 -11 382.217 28.561 1 2 -9 11 336.741 26.410 1 -3 9 -11 128.567 18.204 1 -3 9 -11 82.7332 17.2461 2 3 -9 11 108.444 16.016 1 -4 9 -11 3.47043 7.56403 1 4 -9 11 -6.1757 7.2597 1 -5 9 -11 49.4194 12.9044 1 5 -9 11 61.5709 13.8202 1 4 8 -11 37.3382 10.1306 1 4 8 -11 29.1358 12.7331 2 4 8 -11 55.9997 12.1619 5 3 8 -11 70.5915 12.1640 1 3 8 -11 66.1589 14.1459 5 3 8 -11 86.5793 16.9023 2 2 8 -11 22.5444 11.6711 2 2 8 -11 2.25044 7.07474 1 1 8 -11 26.5135 12.6455 2 1 8 -11 -8.1448 7.7931 1 0 8 -11 64.5653 13.7351 2 0 8 -11 76.4943 12.9115 1 0 -8 11 59.5659 11.2385 1 -1 8 -11 80.9386 12.4393 6 -1 8 -11 86.0247 16.6627 2 -1 8 -11 59.6997 13.0925 1 1 -8 11 55.2165 12.1040 1 -2 8 -11 128.987 17.537 1 2 -8 11 123.241 16.905 1 -3 8 -11 15.9766 9.5715 1 3 -8 11 30.4508 10.3063 1 -4 8 -11 -10.962 10.114 1 4 -8 11 -2.5433 9.0269 1 -5 8 -11 2.42742 7.43417 1 -5 8 -11 26.8753 11.0418 1 5 -8 11 8.58523 7.83938 1 5 7 -11 -5.7469 6.9027 1 5 7 -11 3.21688 6.91257 5 4 7 -11 247.096 20.945 1 4 7 -11 220.115 21.472 5 4 7 -11 214.874 22.898 2 3 7 -11 18.6444 8.8307 1 3 7 -11 49.6737 13.8054 2 3 7 -11 8.45880 8.79363 5 2 7 -11 10.4061 9.3700 2 2 7 -11 15.7573 6.9779 1 2 7 -11 9.92919 7.50190 5 1 7 -11 106.510 14.791 1 1 7 -11 128.667 18.467 2 -1 -7 11 117.250 15.281 1 0 7 -11 24.1506 8.5045 1 0 -7 11 43.0487 9.7656 1 -1 7 -11 289.658 24.369 1 1 -7 11 278.866 23.861 1 -2 7 -11 138.405 18.616 1 2 -7 11 128.222 17.314 1 -3 7 -11 86.3440 16.1909 1 3 -7 11 71.7715 14.2425 1 -4 7 -11 47.6434 13.7634 1 4 -7 11 50.5607 13.5301 1 -5 7 -11 31.5775 11.2382 1 5 -7 11 40.7584 12.1624 1 5 6 -11 278.475 24.200 5 5 6 -11 250.126 21.918 1 5 6 -11 272.323 25.143 2 4 6 -11 264.776 23.858 2 4 6 -11 296.473 24.230 5 4 6 -11 296.088 23.550 1 3 6 -11 10.0931 7.8338 5 3 6 -11 23.0660 9.4271 1 3 6 -11 38.4828 12.1322 2 -3 -6 11 19.2403 8.9227 1 2 6 -11 17.3360 6.5454 5 2 6 -11 22.5708 9.5677 1 2 6 -11 7.17871 9.46249 2 -2 -6 11 10.2815 6.9530 1 1 6 -11 -8.3527 8.2346 1 -1 -6 11 -19.573 9.082 1 0 6 -11 109.225 15.896 1 0 -6 11 89.3088 14.4273 1 -1 6 -11 58.0031 12.5847 1 1 -6 11 38.8477 10.5361 1 -2 6 -11 9.50572 7.41064 1 2 -6 11 10.2542 7.4857 1 -3 6 -11 171.419 20.674 1 3 -6 11 140.575 18.967 1 -4 6 -11 -1.2505 8.8928 1 4 -6 11 22.2233 11.5817 1 -5 6 -11 72.0394 15.9160 1 5 -6 11 80.8498 16.2628 1 6 5 -11 43.5337 12.1994 1 6 5 -11 45.2696 13.1870 5 5 5 -11 171.750 18.950 5 5 5 -11 151.291 18.392 2 5 5 -11 158.543 18.506 1 4 5 -11 83.4914 13.2484 1 4 5 -11 98.8562 14.9393 2 4 5 -11 95.6150 14.5169 5 -4 -5 11 106.746 14.641 1 3 5 -11 -6.5009 8.1432 1 3 5 -11 4.49614 8.83061 2 3 5 -11 5.30172 5.68104 5 -3 -5 11 10.8433 7.9525 1 2 5 -11 28.3764 10.2069 1 2 5 -11 29.9880 8.8314 5 -2 -5 11 30.3532 10.1768 1 1 5 -11 41.2743 11.5302 1 1 5 -11 22.1186 6.2740 5 -1 -5 11 35.1550 10.6501 1 0 5 -11 89.6453 14.2682 1 0 -5 11 122.699 16.083 1 -1 5 -11 27.1687 8.9517 1 1 -5 11 22.8087 8.6039 1 -2 5 -11 104.920 15.592 1 2 -5 11 95.6594 15.0829 1 -3 5 -11 183.497 20.863 1 3 -5 11 185.944 20.985 1 -4 5 -11 54.5315 13.6610 1 4 -5 11 64.3042 14.6582 1 -5 5 -11 8.5405 10.5835 1 5 -5 11 -3.9381 9.7790 1 6 4 -11 -4.2802 9.3512 5 6 4 -11 12.1579 9.7036 1 5 4 -11 64.4259 12.8549 2 5 4 -11 79.8720 14.2926 1 5 4 -11 104.467 14.660 5 -5 -4 11 79.3891 14.4781 1 4 4 -11 -1.1280 7.4564 5 4 4 -11 8.90756 8.98208 2 4 4 -11 -0.1558 8.3520 1 -4 -4 11 8.23657 8.98427 1 3 4 -11 164.785 17.776 1 3 4 -11 120.011 13.979 5 -3 -4 11 131.499 16.182 1 2 4 -11 169.964 18.581 1 2 4 -11 174.873 15.180 5 -2 -4 11 196.939 20.046 1 1 4 -11 296.176 18.726 5 1 4 -11 336.988 26.376 1 -1 -4 11 301.725 25.075 1 0 4 -11 50.7286 12.0025 1 0 -4 11 55.4368 12.6547 1 1 -4 11 1.82920 8.80780 1 -2 4 -11 360.889 28.603 1 2 -4 11 394.509 30.006 1 -3 4 -11 43.3606 12.9381 1 3 -4 11 23.2126 11.2773 1 -4 4 -11 3.69342 9.44782 1 4 -4 11 18.8419 10.9415 1 -5 4 -11 413.431 34.232 1 5 -4 11 436.406 34.492 1 7 3 -11 24.1842 9.4986 1 7 3 -11 38.6244 11.1678 5 6 3 -11 21.9650 10.8335 5 6 3 -11 -19.019 10.191 1 5 3 -11 17.5491 7.5935 5 5 3 -11 32.7186 11.5612 1 5 3 -11 14.8815 8.9610 2 -5 -3 11 31.9523 11.2318 1 4 3 -11 18.8588 9.7521 1 4 3 -11 14.9256 8.3035 5 -4 -3 11 9.16595 8.46038 1 3 3 -11 18.4212 7.3116 5 3 3 -11 28.6469 10.3789 1 -3 -3 11 18.5478 8.8251 1 2 3 -11 91.7444 10.8500 5 2 3 -11 95.2027 15.0429 1 -2 -3 11 74.5844 14.1253 1 1 3 -11 3.95507 3.97021 5 1 3 -11 13.1579 9.4441 1 -1 -3 11 2.37701 8.28067 1 0 3 -11 -20.185 10.215 1 0 -3 11 -10.865 9.629 1 1 -3 11 18.1479 9.9460 1 -2 3 -11 4.84630 6.34729 1 2 -3 11 5.65043 6.82496 1 -3 3 -11 0.54477 6.01687 1 3 -3 11 0.49991 6.27648 1 -4 3 -11 393.960 32.164 1 4 -3 11 377.278 31.598 1 -5 3 -11 142.948 21.015 1 5 -3 11 170.863 22.562 1 7 2 -11 2.44301 8.36577 5 7 2 -11 8.89817 8.36882 1 -7 -2 11 10.2020 8.0094 1 6 2 -11 16.9221 10.8924 1 6 2 -11 31.1697 11.4700 5 -6 -2 11 4.25779 9.40407 1 5 2 -11 31.5734 8.7099 5 5 2 -11 37.5244 11.3644 1 4 2 -11 7.04874 6.90262 5 4 2 -11 -12.224 9.444 1 -4 -2 11 -13.020 9.502 1 3 2 -11 5.10651 5.87388 5 3 2 -11 -22.950 11.177 1 -3 -2 11 -2.2020 8.7547 1 2 2 -11 211.741 15.272 5 2 2 -11 215.829 21.262 1 -2 -2 11 217.731 22.085 1 1 2 -11 32.7614 10.8778 1 1 2 -11 31.9862 5.6435 5 -1 -2 11 21.4114 9.5992 1 0 2 -11 59.0715 12.8880 1 -1 2 -11 123.347 17.434 1 1 -2 11 137.995 18.834 1 -2 2 -11 5.14459 8.08409 1 2 -2 11 7.75745 9.51939 1 -3 2 -11 42.8457 11.3262 1 3 -2 11 36.8899 10.9821 1 -4 2 -11 250.397 25.774 1 4 -2 11 247.330 26.025 1 7 1 -11 1.82340 9.63796 1 7 1 -11 14.9265 10.6853 5 -7 -1 11 1.6143 10.3067 1 6 1 -11 71.9599 13.8243 5 6 1 -11 78.4020 14.4228 1 -6 -1 11 60.2937 13.3404 1 5 1 -11 18.0439 10.4216 1 -5 -1 11 46.9797 13.5513 1 4 1 -11 1.67707 8.74435 1 -4 -1 11 -8.1133 9.5611 1 3 1 -11 111.937 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13.5911 1 -2 0 -11 142.185 18.115 1 2 0 11 168.988 20.336 1 3 0 11 75.9477 16.2872 1 7 -1 -11 82.0979 16.2898 1 -7 1 11 80.8668 16.7981 1 6 -1 -11 -5.8387 10.9147 1 -6 1 11 6.7816 10.6584 1 5 -1 -11 13.3241 10.5111 1 4 -1 -11 -11.166 6.375 5 -4 1 11 2.36723 9.08905 1 3 -1 -11 162.475 19.963 1 -3 1 11 188.476 22.557 1 2 -1 -11 539.407 34.179 1 -2 1 11 478.449 34.235 1 -1 1 11 9.45862 9.98103 1 0 -1 -11 35.4085 11.3853 1 0 1 11 7.5740 10.2665 1 -1 -1 -11 394.997 30.724 1 1 1 11 463.906 33.810 1 -2 -1 -11 348.297 29.478 1 2 1 11 423.762 33.423 1 6 -2 -11 -8.9930 7.9705 1 -6 2 11 10.7048 8.9633 1 5 -2 -11 4.24771 7.06528 1 -5 2 11 5.8660 10.1062 1 4 -2 -11 24.4865 10.9688 1 -4 2 11 42.4365 13.2365 1 3 -2 -11 207.828 22.381 1 -3 2 11 207.460 23.432 1 2 -2 -11 -9.1220 8.7997 1 -2 2 11 12.9009 10.3988 1 1 -2 -11 50.5361 11.6047 1 -1 2 11 32.1130 10.3611 1 0 -2 -11 549.092 35.807 1 0 2 11 544.326 37.475 1 -1 -2 -11 372.340 30.275 1 1 2 11 386.755 32.275 1 6 -3 -11 4.9187 10.2211 1 -6 3 11 -8.7229 11.8867 1 5 -3 -11 14.3780 11.2254 1 -5 3 11 9.1637 11.9385 1 4 -3 -11 14.5156 9.9279 1 -4 3 11 18.2537 11.4317 1 3 -3 -11 34.1905 12.0492 1 -3 3 11 47.1542 14.4178 1 2 -3 -11 5.48321 8.39192 1 -2 3 11 1.93047 9.61990 1 1 -3 -11 193.948 22.563 1 -1 3 11 190.380 23.229 1 0 3 11 252.988 25.570 1 4 -4 -11 171.778 21.294 1 -4 4 11 188.440 24.192 1 3 -4 -11 75.6486 14.9137 1 0 10 -12 9.9569 11.5073 2 0 10 -12 11.0853 8.4498 1 -1 10 -12 8.98096 8.75713 2 -1 10 -12 18.8549 8.9735 1 -2 10 -12 29.2662 13.2970 2 -3 10 -12 267.234 25.261 1 -3 10 -12 269.861 25.114 6 2 9 -12 97.9290 13.6615 1 2 9 -12 107.033 19.096 2 1 9 -12 41.2888 10.2090 1 1 9 -12 17.4171 9.6739 2 0 9 -12 -6.8741 7.9070 1 0 9 -12 -3.4068 7.7180 2 -1 9 -12 -2.6284 9.9318 2 -1 9 -12 19.5101 8.5405 1 -2 9 -12 51.2058 14.4653 2 -2 9 -12 48.0034 11.8488 1 -3 9 -12 105.241 17.793 1 3 -9 12 109.366 17.540 1 -4 9 -12 45.9561 14.4187 1 4 -9 12 16.7865 11.2772 1 3 8 -12 26.2992 12.9049 2 3 8 -12 39.0550 10.2594 5 2 8 -12 146.681 20.969 2 2 8 -12 180.482 18.870 1 1 8 -12 12.9289 9.0225 1 1 8 -12 13.1305 11.2650 2 0 8 -12 4.3471 10.4124 2 0 8 -12 -3.6285 7.3893 1 -1 8 -12 3.69631 8.76123 1 -2 8 -12 34.0128 12.5928 1 2 -8 12 38.7759 11.8942 1 -3 8 -12 -6.3679 9.9092 1 3 -8 12 0.29016 7.71797 1 -4 8 -12 16.1519 10.3274 1 4 -8 12 6.53497 8.62761 1 4 7 -12 -10.020 9.370 5 4 7 -12 3.14202 7.84120 1 3 7 -12 218.835 21.414 5 3 7 -12 237.876 22.666 1 3 7 -12 220.618 24.228 2 2 7 -12 17.2858 9.7379 1 2 7 -12 17.4678 10.8844 2 1 7 -12 2.32578 7.80973 1 1 7 -12 9.1014 10.4391 2 -1 -7 12 -11.375 7.985 1 0 7 -12 121.373 17.110 1 0 -7 12 154.769 18.614 1 -1 7 -12 50.9221 13.1854 1 1 -7 12 74.4599 14.5989 1 -2 7 -12 76.3819 14.9774 1 2 -7 12 63.2073 13.6670 1 -3 7 -12 -7.2220 10.0239 1 3 -7 12 7.34857 9.26328 1 -4 7 -12 50.7231 14.2644 1 4 -7 12 69.5446 14.8686 1 4 6 -12 168.767 21.007 2 4 6 -12 184.018 19.334 5 4 6 -12 184.476 19.254 1 3 6 -12 68.1594 12.7546 5 3 6 -12 93.9718 14.9690 1 3 6 -12 89.8178 16.4241 2 2 6 -12 6.06102 6.30250 5 2 6 -12 11.2509 7.6915 1 -2 -6 12 -4.5207 6.0488 1 1 6 -12 -3.1152 8.6485 1 -1 -6 12 8.21073 8.88851 1 0 6 -12 114.743 16.984 1 0 -6 12 122.180 16.864 1 -1 6 -12 337.373 27.626 1 1 -6 12 341.112 27.853 1 -2 6 -12 183.494 21.017 1 2 -6 12 180.534 20.867 1 -3 6 -12 8.1647 10.2959 1 -4 6 -12 24.9193 12.6112 1 4 -6 12 -6.0774 10.4343 1 5 5 -12 28.8757 11.3854 2 4 5 -12 198.240 19.996 5 4 5 -12 198.368 21.815 2 4 5 -12 188.533 20.834 1 -4 -5 12 205.568 21.990 1 3 5 -12 8.37415 6.50090 5 3 5 -12 -4.6617 9.1557 1 -3 -5 12 -8.8281 8.5049 1 2 5 -12 12.5211 6.9534 5 -2 -5 12 7.50725 8.69425 1 1 5 -12 307.952 25.830 1 -1 -5 12 262.896 24.430 1 0 5 -12 157.340 19.095 1 0 -5 12 197.112 21.423 1 -1 5 -12 258.962 24.989 1 1 -5 12 244.096 24.303 1 -2 5 -12 29.9237 12.0884 1 2 -5 12 35.2182 12.2892 1 -3 5 -12 67.1067 14.0709 1 3 -5 12 68.4982 14.3247 1 -4 5 -12 361.633 31.753 1 4 -5 12 349.482 31.316 1 5 4 -12 29.3005 10.2223 5 -5 -4 12 36.8819 12.0517 1 4 4 -12 14.3375 10.5346 1 4 4 -12 27.3762 10.0025 5 -4 -4 12 16.0537 9.5719 1 3 4 -12 -7.6837 9.2031 1 -3 -4 12 27.7301 11.0158 1 2 4 -12 339.553 27.129 1 2 4 -12 291.078 20.132 5 -2 -4 12 281.075 25.465 1 1 4 -12 145.917 19.228 1 -1 -4 12 176.155 21.000 1 0 4 -12 52.7348 11.6856 1 0 -4 12 49.7442 11.4161 1 -1 4 -12 0.81436 7.17626 1 1 -4 12 -0.8033 7.8246 1 -2 4 -12 -18.516 10.916 1 2 -4 12 27.1329 12.1603 1 -3 4 -12 492.471 37.011 1 3 -4 12 485.309 36.543 1 -4 4 -12 128.073 20.356 1 4 -4 12 140.801 21.191 1 6 3 -12 77.1692 14.7574 1 6 3 -12 59.7905 13.8286 5 5 3 -12 34.3151 10.8398 5 -5 -3 12 40.8523 12.8868 1 4 3 -12 5.79213 6.79221 5 4 3 -12 -2.0815 9.4630 1 -4 -3 12 16.4912 10.5324 1 3 3 -12 45.0893 12.5975 1 3 3 -12 36.0289 7.8525 5 -3 -3 12 34.8852 12.2653 1 2 3 -12 228.666 22.742 1 2 3 -12 229.130 16.839 5 -2 -3 12 213.992 22.286 1 1 3 -12 77.8952 15.6534 1 -1 -3 12 49.8424 13.5576 1 0 3 -12 -20.543 10.504 1 0 -3 12 -24.847 11.049 1 -1 3 -12 4.69638 9.79225 1 1 -3 12 10.0356 10.5952 1 -2 3 -12 99.5531 17.1750 1 2 -3 12 115.947 18.652 1 -3 3 -12 100.938 18.400 1 3 -3 12 150.246 21.489 1 6 2 -12 10.5061 8.9896 5 6 2 -12 27.2711 12.6001 1 -6 -2 12 25.0552 12.0387 1 5 2 -12 1.69805 6.85785 1 5 2 -12 2.49867 7.82439 5 -5 -2 12 -5.6524 7.8702 1 4 2 -12 16.2504 7.0376 5 4 2 -12 33.5037 10.4188 1 -4 -2 12 2.09558 6.82750 1 3 2 -12 163.999 14.942 5 3 2 -12 180.253 20.879 1 -3 -2 12 149.585 20.334 1 2 2 -12 34.4417 12.3112 1 -2 -2 12 47.2705 13.0883 1 1 2 -12 -5.4564 9.6817 1 -1 -2 12 24.3709 11.0923 1 0 2 -12 233.558 23.717 1 0 -2 12 225.119 24.185 1 1 -2 12 5.10061 9.47518 1 -2 2 -12 27.9817 11.5112 1 2 -2 12 11.6694 9.9904 1 -3 2 -12 60.1222 15.1123 1 3 -2 12 52.6956 14.4041 1 6 1 -12 14.6262 9.0883 1 6 1 -12 -3.3337 6.2023 5 -6 -1 12 -7.9682 8.4450 1 5 1 -12 14.5995 7.3181 5 5 1 -12 -16.439 11.188 1 -5 -1 12 26.9559 12.5144 1 4 1 -12 171.621 16.489 5 4 1 -12 185.775 21.838 1 -4 -1 12 175.146 22.381 1 3 1 -12 111.998 16.520 1 -3 -1 12 105.285 16.440 1 2 1 -12 188.358 21.518 1 -2 -1 12 175.087 21.680 1 1 1 -12 36.2393 12.5373 1 -1 -1 12 50.4754 13.7811 1 0 1 -12 3.89850 8.65009 1 0 -1 12 -2.5036 9.5531 1 -1 1 -12 9.5291 10.2730 1 1 -1 12 -12.198 10.540 1 -2 1 -12 43.2193 13.0005 1 2 -1 12 57.1340 14.7658 1 6 0 -12 -2.0581 9.3792 1 6 0 -12 -3.5719 8.1469 5 -6 0 12 13.1992 11.8833 1 5 0 -12 77.2264 12.5051 5 5 0 -12 59.4125 15.3327 1 -5 0 12 85.9942 17.7762 1 4 0 -12 392.531 31.356 1 -4 0 12 411.959 33.764 1 3 0 -12 22.4921 9.2781 1 -3 0 12 26.6367 10.3888 1 2 0 -12 2.09859 8.66637 1 -2 0 12 21.3704 12.1227 1 1 0 -12 183.493 22.178 1 -1 0 12 159.558 21.379 1 0 0 -12 62.1112 13.9807 1 0 0 12 75.8414 16.4277 1 1 0 12 4.7590 10.1424 1 5 -1 -12 185.715 23.140 1 -5 1 12 231.476 26.525 1 4 -1 -12 8.76912 9.31716 1 -4 1 12 30.4093 13.4171 1 -3 1 12 32.7072 13.2742 1 2 -1 -12 120.726 17.321 1 -2 1 12 115.284 17.949 1 1 -1 -12 124.884 18.935 1 -1 1 12 148.203 21.023 1 0 -1 -12 42.7711 11.1537 1 0 1 12 10.0743 8.2613 1 4 -2 -12 12.6632 10.2322 1 -4 2 12 30.6640 12.8953 1 3 -2 -12 3.56436 9.84026 1 -3 2 12 13.7040 11.4798 1 2 -2 -12 75.0831 15.5728 1 -2 2 12 104.422 18.711 1 1 8 -13 60.2860 12.4507 1 0 8 -13 18.5514 8.5006 1 0 8 -13 -18.516 12.518 2 -1 8 -13 51.1528 13.7426 1 -2 8 -13 35.0741 12.7975 1 2 -8 13 48.1113 13.9111 1 2 7 -13 0.76910 8.07010 1 2 7 -13 2.28802 7.66617 2 1 7 -13 5.72466 8.59422 1 -1 -7 13 30.8138 10.9535 1 0 7 -13 6.39368 9.46412 1 0 -7 13 3.94963 8.92066 1 -1 7 -13 -4.4122 7.2435 1 1 -7 13 17.5222 8.7634 1 -2 7 -13 6.9854 10.4441 1 2 -7 13 9.7233 10.4557 1 3 6 -13 4.13972 7.01443 1 3 6 -13 0.94703 9.92988 2 3 6 -13 2.76349 6.02548 5 2 6 -13 38.8812 10.6900 1 -2 -6 13 42.0871 11.2153 1 1 6 -13 50.1051 12.7639 1 -1 -6 13 52.6549 12.7219 1 0 6 -13 -13.082 11.070 1 0 -6 13 1.39228 8.93460 1 -1 6 -13 14.2284 8.1574 1 1 -6 13 13.7351 8.9149 1 -2 6 -13 272.119 27.556 1 2 -6 13 265.813 27.150 1 4 5 -13 10.7025 8.1343 2 4 5 -13 12.6136 9.3972 1 4 5 -13 32.6946 10.8621 5 3 5 -13 72.9266 15.1898 1 3 5 -13 60.1694 11.5883 5 -3 -5 13 73.9604 15.0479 1 2 5 -13 2.68842 6.21844 5 2 5 -13 4.88882 8.59575 1 1 5 -13 24.4040 10.5867 1 0 5 -13 51.8756 14.1344 1 0 -5 13 36.8399 12.7112 1 -1 5 -13 95.8327 16.2009 1 1 -5 13 98.7561 16.3116 1 -2 5 -13 258.636 26.762 1 2 -5 13 270.410 27.854 1 4 4 -13 26.9817 9.8379 1 4 4 -13 23.0831 7.6811 5 -4 -4 13 33.1243 11.4954 1 3 4 -13 13.6980 9.2741 1 3 4 -13 4.19801 6.21276 5 -3 -4 13 4.42866 8.37284 1 2 4 -13 131.202 18.108 1 -2 -4 13 115.849 17.228 1 1 4 -13 320.078 28.458 1 -1 -4 13 337.813 29.787 1 0 4 -13 77.6401 14.6458 1 0 -4 13 89.5494 15.5986 1 -1 4 -13 84.1029 16.8730 1 1 -4 13 86.5519 17.0517 1 -2 4 -13 -21.008 11.863 1 2 -4 13 -10.764 11.002 1 4 3 -13 25.5537 9.1199 5 4 3 -13 26.2069 11.1420 1 -4 -3 13 31.7015 12.1990 1 3 3 -13 118.473 18.206 1 -3 -3 13 90.6711 16.6601 1 2 3 -13 138.164 19.665 1 -2 -3 13 154.711 20.947 1 1 3 -13 229.367 23.521 1 -1 -3 13 220.187 23.923 1 0 3 -13 22.3206 11.4718 1 0 -3 13 -6.9839 10.7176 1 -1 3 -13 5.9714 10.4169 1 1 -3 13 -0.6230 9.7691 1 4 2 -13 -6.4278 10.8184 1 -4 -2 13 33.1445 13.1875 1 3 2 -13 -0.2352 8.3028 1 -3 -2 13 14.3699 10.7378 1 2 2 -13 105.701 17.680 1 -2 -2 13 116.156 18.610 1 1 2 -13 24.9428 12.0522 1 -1 -2 13 16.0575 12.1749 1 0 2 -13 -11.073 10.351 1 0 -2 13 3.01298 9.74412 1 -1 2 -13 322.701 29.827 1 1 -2 13 362.588 31.986 1 4 1 -13 43.7379 13.6370 1 -4 -1 13 66.8562 16.0665 1 3 1 -13 49.3613 13.8687 1 -3 -1 13 49.8034 14.4430 1 2 1 -13 114.873 17.524 1 -2 -1 13 114.525 18.105 1 1 1 -13 6.8082 10.1497 1 0 1 -13 74.3679 16.0843 1 0 -1 13 95.5282 18.1966 1 3 0 -13 144.320 20.591 1 -3 0 13 122.974 20.514 1 2 0 -13 13.1992 10.8117 1 -2 0 13 8.3495 10.5396 1 0 0 0 0.00 0.00 0 ; #END Tags that were not found in dictionaries loop_ _symmetry_equiv_pos_as_xyz 'x, y, z' '-x, -y, -z' loop_ _atom_site_label _atom_site_type_symbol _atom_site_fract_x _atom_site_fract_y _atom_site_fract_z _atom_site_U_iso_or_equiv _atom_site_adp_type _atom_site_occupancy _atom_site_symmetry_multiplicity _atom_site_calc_flag _atom_site_refinement_flags _atom_site_disorder_assembly _atom_site_disorder_group Si1 Si 0.38093(6) 0.39018(5) 0.11700(5) 0.01594(14) Uani 1 1 d . . . O1 O 0.31425(16) 0.33333(13) -0.04928(13) 0.0207(3) Uani 1 1 d . A . O2 O 0.42557(16) 0.47759(13) -0.17642(13) 0.0204(3) Uani 1 1 d . . . B1 B 0.3021(2) 0.3648(2) -0.1623(2) 0.0156(4) Uani 1 1 d . . . C1 C 0.4057(2) 0.23112(19) 0.14622(19) 0.0199(4) Uani 1 1 d . . . C2 C 0.2421(3) 0.0900(2) 0.0774(2) 0.0297(5) Uani 1 1 d . . . H2A H 0.2615 0.0099 0.0931 0.045 Uiso 1 1 calc R . . H2B H 0.2146 0.0657 -0.0212 0.045 Uiso 1 1 calc R . . H2C H 0.1459 0.1044 0.1164 0.045 Uiso 1 1 calc R . . C3 C 0.5542(3) 0.2060(2) 0.0818(2) 0.0300(5) Uani 1 1 d . . . H3A H 0.5744 0.1266 0.0983 0.045 Uiso 1 1 calc R . . H3B H 0.6592 0.2957 0.1231 0.045 Uiso 1 1 calc R . . H3C H 0.5234 0.1796 -0.0170 0.045 Uiso 1 1 calc R . . C4 C 0.4542(3) 0.2661(2) 0.3002(2) 0.0349(5) Uani 1 1 d . . . H4A H 0.3572 0.2746 0.3414 0.052 Uiso 1 1 calc R . . H4B H 0.5553 0.3586 0.3446 0.052 Uiso 1 1 calc R . . H4C H 0.4808 0.1874 0.3127 0.052 Uiso 1 1 calc R . . C5 C 0.2316(2) 0.4725(2) 0.2000(2) 0.0231(4) Uani 1 1 d . . . C6 C 0.2965(3) 0.5470(2) 0.3570(2) 0.0339(5) Uani 1 1 d . . . H6A H 0.2234 0.5973 0.3964 0.051 Uiso 1 1 calc R . . H6B H 0.4157 0.6181 0.3806 0.051 Uiso 1 1 calc R . . H6C H 0.2915 0.4729 0.3938 0.051 Uiso 1 1 calc R . . C7 C 0.2304(3) 0.5912(2) 0.1465(2) 0.0339(5) Uani 1 1 d . . . H7A H 0.1891 0.5462 0.0467 0.051 Uiso 1 1 calc R . . H7B H 0.3475 0.6662 0.1710 0.051 Uiso 1 1 calc R . . H7C H 0.1538 0.6363 0.1879 0.051 Uiso 1 1 calc R . . C8 C 0.0462(3) 0.3589(3) 0.1633(3) 0.0366(5) Uani 1 1 d . . . H8A H 0.0435 0.2856 0.2006 0.055 Uiso 1 1 calc R . . H8B H 0.0052 0.3109 0.0636 0.055 Uiso 1 1 calc R . . H8C H -0.0284 0.4076 0.2024 0.055 Uiso 1 1 calc R . . C9A C 0.1398(14) 0.2712(14) -0.2935(10) 0.0185(13) Uani 0.298(5) 1 d PGU A 1 C10A C 0.1314(12) 0.3042(12) -0.4087(11) 0.0178(12) Uani 0.298(5) 1 d PGU A 1 H10A H 0.2235 0.3835 -0.4131 0.021 Uiso 0.298(5) 1 calc PR A 1 C11A C -0.0119(12) 0.2211(11) -0.5175(9) 0.0172(12) Uani 0.298(5) 1 d PGU A 1 H11A H -0.0177 0.2437 -0.5963 0.021 Uiso 0.298(5) 1 calc PR A 1 C12A C -0.1467(11) 0.1052(10) -0.5112(8) 0.0184(12) Uani 0.298(5) 1 d PGU A 1 C13A C -0.1383(14) 0.0722(10) -0.3960(9) 0.0180(12) Uani 0.298(5) 1 d PGU A 1 H13A H -0.2305 -0.0071 -0.3916 0.022 Uiso 0.298(5) 1 calc PR A 1 C14A C 0.0050(16) 0.1553(13) -0.2871(9) 0.0171(11) Uani 0.298(5) 1 d PGU A 1 H14A H 0.0107 0.1327 -0.2084 0.021 Uiso 0.298(5) 1 calc PR A 1 O3A O -0.4302(8) -0.0794(7) -0.6313(6) 0.0456(17) Uani 0.298(5) 1 d PU A 1 C15A C -0.2976(13) 0.0163(10) -0.6295(10) 0.0245(14) Uani 0.298(5) 1 d PU A 1 H15A H -0.2905 0.0353 -0.7101 0.029 Uiso 0.298(5) 1 calc PR A 1 C9B C 0.1319(6) 0.2623(6) -0.2818(4) 0.0138(7) Uani 0.702(5) 1 d PGU A 2 C10B C 0.1112(5) 0.2906(5) -0.3988(4) 0.0196(7) Uani 0.702(5) 1 d PGU A 2 H10B H 0.1983 0.3697 -0.4079 0.023 Uiso 0.702(5) 1 calc PR A 2 C11B C -0.0370(5) 0.2030(4) -0.5026(3) 0.0219(7) Uani 0.702(5) 1 d PGU A 2 H11B H -0.0512 0.2223 -0.5825 0.026 Uiso 0.702(5) 1 calc PR A 2 C12B C -0.1644(4) 0.0871(4) -0.4893(3) 0.0196(7) Uani 0.702(5) 1 d PGU A 2 C13B C -0.1437(6) 0.0589(4) -0.3723(4) 0.0203(7) Uani 0.702(5) 1 d PGU A 2 H13B H -0.2308 -0.0203 -0.3633 0.024 Uiso 0.702(5) 1 calc PR A 2 C14B C 0.0045(7) 0.1464(5) -0.2686(4) 0.0183(7) Uani 0.702(5) 1 d PGU A 2 H14B H 0.0186 0.1271 -0.1886 0.022 Uiso 0.702(5) 1 calc PR A 2 O3B O -0.3549(3) -0.0010(3) -0.7097(3) 0.0431(8) Uani 0.702(5) 1 d PU A 2 C15B C -0.3235(5) -0.0101(4) -0.6006(4) 0.0272(8) Uani 0.702(5) 1 d PU A 2 H15B H -0.4076 -0.0857 -0.5846 0.033 Uiso 0.702(5) 1 calc PR A 2 loop_ _atom_site_aniso_label _atom_site_aniso_U_11 _atom_site_aniso_U_22 _atom_site_aniso_U_33 _atom_site_aniso_U_23 _atom_site_aniso_U_13 _atom_site_aniso_U_12 Si1 0.0144(2) 0.0154(2) 0.0143(2) 0.00557(19) 0.00002(18) 0.00245(18) O1 0.0209(6) 0.0188(6) 0.0170(6) 0.0067(5) -0.0001(5) 0.0031(5) O2 0.0178(6) 0.0182(6) 0.0193(7) 0.0071(5) -0.0006(5) 0.0015(5) B1 0.0146(9) 0.0138(9) 0.0168(10) 0.0040(8) 0.0035(8) 0.0058(7) C1 0.0202(9) 0.0178(9) 0.0203(9) 0.0090(7) 0.0017(7) 0.0051(7) C2 0.0250(10) 0.0190(10) 0.0402(12) 0.0134(9) 0.0022(9) 0.0023(8) C3 0.0249(10) 0.0246(11) 0.0437(13) 0.0160(10) 0.0089(9) 0.0109(8) C4 0.0503(14) 0.0311(12) 0.0256(11) 0.0154(9) 0.0015(10) 0.0162(10) C5 0.0197(9) 0.0250(10) 0.0236(10) 0.0088(8) 0.0041(8) 0.0085(8) C6 0.0397(12) 0.0389(13) 0.0243(11) 0.0083(9) 0.0091(9) 0.0208(10) C7 0.0377(12) 0.0362(12) 0.0390(13) 0.0179(10) 0.0111(10) 0.0240(10) C8 0.0213(10) 0.0400(13) 0.0447(14) 0.0129(11) 0.0108(10) 0.0106(9) C9A 0.0159(17) 0.0145(18) 0.0203(18) 0.0049(15) 0.0076(16) 0.0016(15) C10A 0.0203(18) 0.0182(17) 0.0151(17) 0.0106(14) 0.0022(16) 0.0043(15) C11A 0.0214(19) 0.0184(17) 0.0136(17) 0.0125(14) 0.0043(15) 0.0036(15) C12A 0.0203(17) 0.0199(17) 0.0163(17) 0.0079(14) 0.0014(15) 0.0092(14) C13A 0.0186(17) 0.0163(17) 0.0182(19) 0.0098(15) 0.0043(16) 0.0028(15) C14A 0.0197(17) 0.0174(17) 0.0163(18) 0.0099(14) 0.0023(16) 0.0069(15) O3A 0.037(2) 0.042(2) 0.044(3) 0.0119(18) 0.0004(19) 0.0080(19) C15A 0.023(2) 0.026(2) 0.022(2) 0.0086(17) 0.0019(18) 0.0078(17) C9B 0.0165(11) 0.0145(12) 0.0117(11) 0.0057(9) 0.0018(10) 0.0074(9) C10B 0.0206(13) 0.0173(13) 0.0182(13) 0.0088(10) 0.0045(10) 0.0026(10) C11B 0.0256(15) 0.0228(14) 0.0167(12) 0.0101(10) 0.0016(10) 0.0073(11) C12B 0.0178(11) 0.0175(12) 0.0207(13) 0.0051(10) 0.0018(10) 0.0067(9) C13B 0.0187(11) 0.0180(12) 0.0209(14) 0.0101(10) 0.0032(11) 0.0014(9) C14B 0.0195(11) 0.0167(12) 0.0169(13) 0.0086(10) 0.0023(11) 0.0034(9) O3B 0.0414(13) 0.0442(13) 0.0337(14) 0.0090(10) -0.0119(10) 0.0164(10) C15B 0.0219(15) 0.0255(15) 0.0275(15) 0.0069(11) -0.0014(12) 0.0070(12) loop_ _atom_type_symbol _atom_type_description _atom_type_scat_dispersion_real _atom_type_scat_dispersion_imag _atom_type_scat_source C C 0.0033 0.0016 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' H H 0.0000 0.0000 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' B B 0.0013 0.0007 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' O O 0.0106 0.0060 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' Si Si 0.0817 0.0704 'International Tables Vol C Tables 4.2.6.8 and 6.1.1.4' loop_ _geom_angle_atom_site_label_1 _geom_angle_atom_site_label_2 _geom_angle_atom_site_label_3 _geom_angle _geom_angle_site_symmetry_1 _geom_angle_site_symmetry_3 O1 Si1 O2 112.49(7) . 2_665 O1 Si1 C5 107.15(8) . . O2 Si1 C5 105.74(8) 2_665 . O1 Si1 C1 105.83(8) . . O2 Si1 C1 105.23(8) 2_665 . C5 Si1 C1 120.55(8) . . B1 O1 Si1 149.22(12) . . B1 O2 Si1 148.54(13) . 2_665 O2 B1 O1 123.15(17) . . O2 B1 C9B 119.8(2) . . O1 B1 C9B 117.0(2) . . O2 B1 C9A 113.3(4) . . O1 B1 C9A 123.5(4) . . C2 C1 C4 109.67(16) . . C2 C1 C3 108.34(16) . . C4 C1 C3 108.41(17) . . C2 C1 Si1 112.18(13) . . C4 C1 Si1 111.10(13) . . C3 C1 Si1 107.00(12) . . C1 C2 H2A 109.5 . . C1 C2 H2B 109.5 . . H2A C2 H2B 109.5 . . C1 C2 H2C 109.5 . . H2A C2 H2C 109.5 . . H2B C2 H2C 109.5 . . C1 C3 H3A 109.5 . . C1 C3 H3B 109.5 . . H3A C3 H3B 109.5 . . C1 C3 H3C 109.5 . . H3A C3 H3C 109.5 . . H3B C3 H3C 109.5 . . C1 C4 H4A 109.5 . . C1 C4 H4B 109.5 . . H4A C4 H4B 109.5 . . C1 C4 H4C 109.5 . . H4A C4 H4C 109.5 . . H4B C4 H4C 109.5 . . C8 C5 C6 109.37(17) . . C8 C5 C7 108.30(17) . . C6 C5 C7 108.00(17) . . C8 C5 Si1 112.25(14) . . C6 C5 Si1 111.32(14) . . C7 C5 Si1 107.44(13) . . C5 C6 H6A 109.5 . . C5 C6 H6B 109.5 . . H6A C6 H6B 109.5 . . C5 C6 H6C 109.5 . . H6A C6 H6C 109.5 . . H6B C6 H6C 109.5 . . C5 C7 H7A 109.5 . . C5 C7 H7B 109.5 . . H7A C7 H7B 109.5 . . C5 C7 H7C 109.5 . . H7A C7 H7C 109.5 . . H7B C7 H7C 109.5 . . C5 C8 H8A 109.5 . . C5 C8 H8B 109.5 . . H8A C8 H8B 109.5 . . C5 C8 H8C 109.5 . . H8A C8 H8C 109.5 . . H8B C8 H8C 109.5 . . C10A C9A C14A 120.0 . . C10A C9A B1 122.5(6) . . C14A C9A B1 117.5(6) . . C11A C10A C9A 120.0 . . C11A C10A H10A 120.0 . . C9A C10A H10A 120.0 . . C12A C11A C10A 120.0 . . C12A C11A H11A 120.0 . . C10A C11A H11A 120.0 . . C11A C12A C13A 120.0 . . C11A C12A C15A 119.2(6) . . C13A C12A C15A 120.8(6) . . C14A C13A C12A 120.0 . . C14A C13A H13A 120.0 . . C12A C13A H13A 120.0 . . C13A C14A C9A 120.0 . . C13A C14A H14A 120.0 . . C9A C14A H14A 120.0 . . O3A C15A C12A 125.2(9) . . O3A C15A H15A 117.4 . . C12A C15A H15A 117.4 . . C10B C9B C14B 120.0 . . C10B C9B B1 119.6(3) . . C14B C9B B1 120.4(3) . . C11B C10B C9B 120.0 . . C11B C10B H10B 120.0 . . C9B C10B H10B 120.0 . . C12B C11B C10B 120.0 . . C12B C11B H11B 120.0 . . C10B C11B H11B 120.0 . . C11B C12B C13B 120.0 . . C11B C12B C15B 120.9(2) . . C13B C12B C15B 119.1(2) . . C14B C13B C12B 120.0 . . C14B C13B H13B 120.0 . . C12B C13B H13B 120.0 . . C13B C14B C9B 120.0 . . C13B C14B H14B 120.0 . . C9B C14B H14B 120.0 . . O3B C15B C12B 125.8(4) . . O3B C15B H15B 117.1 . . C12B C15B H15B 117.1 . . loop_ _geom_bond_atom_site_label_1 _geom_bond_atom_site_label_2 _geom_bond_distance _geom_bond_site_symmetry_2 Si1 O1 1.6431(13) . Si1 O2 1.6443(13) 2_665 Si1 C5 1.8864(19) . Si1 C1 1.8876(18) . O1 B1 1.361(2) . O2 B1 1.357(2) . O2 Si1 1.6443(13) 2_665 B1 C9B 1.601(3) . B1 C9A 1.622(7) . C1 C2 1.536(3) . C1 C4 1.541(3) . C1 C3 1.542(3) . C2 H2A 0.9800 . C2 H2B 0.9800 . C2 H2C 0.9800 . C3 H3A 0.9800 . C3 H3B 0.9800 . C3 H3C 0.9800 . C4 H4A 0.9800 . C4 H4B 0.9800 . C4 H4C 0.9800 . C5 C8 1.534(3) . C5 C6 1.543(3) . C5 C7 1.550(3) . C6 H6A 0.9800 . C6 H6B 0.9800 . C6 H6C 0.9800 . C7 H7A 0.9800 . C7 H7B 0.9800 . C7 H7C 0.9800 . C8 H8A 0.9800 . C8 H8B 0.9800 . C8 H8C 0.9800 . C9A C10A 1.3900 . C9A C14A 1.3900 . C10A C11A 1.3900 . C10A H10A 0.9500 . C11A C12A 1.3900 . C11A H11A 0.9500 . C12A C13A 1.3900 . C12A C15A 1.486(12) . C13A C14A 1.3900 . C13A H13A 0.9500 . C14A H14A 0.9500 . O3A C15A 1.223(11) . C15A H15A 0.9500 . C9B C10B 1.3900 . C9B C14B 1.3900 . C10B C11B 1.3900 . C10B H10B 0.9500 . C11B C12B 1.3900 . C11B H11B 0.9500 . C12B C13B 1.3900 . C12B C15B 1.495(5) . C13B C14B 1.3900 . C13B H13B 0.9500 . C14B H14B 0.9500 . O3B C15B 1.215(5) . C15B H15B 0.9500 . loop_ _geom_torsion_atom_site_label_1 _geom_torsion_atom_site_label_2 _geom_torsion_atom_site_label_3 _geom_torsion_atom_site_label_4 _geom_torsion _geom_torsion_site_symmetry_1 O2 Si1 O1 B1 -40.1(3) 2_665 C5 Si1 O1 B1 75.7(3) . C1 Si1 O1 B1 -154.5(2) . Si1 O2 B1 O1 7.2(4) 2_665 Si1 O2 B1 C9B -173.2(3) 2_665 Si1 O2 B1 C9A -172.5(7) 2_665 Si1 O1 B1 O2 32.8(4) . Si1 O1 B1 C9B -146.8(3) . Si1 O1 B1 C9A -147.5(8) . O1 Si1 C1 C2 -52.29(15) . O2 Si1 C1 C2 -171.59(13) 2_665 C5 Si1 C1 C2 69.25(16) . O1 Si1 C1 C4 -175.46(13) . O2 Si1 C1 C4 65.25(15) 2_665 C5 Si1 C1 C4 -53.91(17) . O1 Si1 C1 C3 66.38(14) . O2 Si1 C1 C3 -52.91(14) 2_665 C5 Si1 C1 C3 -172.07(13) . O1 Si1 C5 C8 64.23(16) . O2 Si1 C5 C8 -175.57(14) 2_665 C1 Si1 C5 C8 -56.67(18) . O1 Si1 C5 C6 -172.79(13) . O2 Si1 C5 C6 -52.59(15) 2_665 C1 Si1 C5 C6 66.31(16) . O1 Si1 C5 C7 -54.73(15) . O2 Si1 C5 C7 65.47(15) 2_665 C1 Si1 C5 C7 -175.63(13) . O2 B1 C9A C10A 0.7(10) . O1 B1 C9A C10A -179.1(5) . C9B B1 C9A C10A 175(8) . O2 B1 C9A C14A -178.6(5) . O1 B1 C9A C14A 1.6(11) . C9B B1 C9A C14A -4(7) . C14A C9A C10A C11A 0.0 . B1 C9A C10A C11A -179.3(12) . C9A C10A C11A C12A 0.0 . C10A C11A C12A C13A 0.0 . C10A C11A C12A C15A -179.1(10) . C11A C12A C13A C14A 0.0 . C15A C12A C13A C14A 179.1(10) . C12A C13A C14A C9A 0.0 . C10A C9A C14A C13A 0.0 . B1 C9A C14A C13A 179.3(12) . C11A C12A C15A O3A -173.0(9) . C13A C12A C15A O3A 7.9(14) . O2 B1 C9B C10B -0.6(5) . O1 B1 C9B C10B 179.0(2) . C9A B1 C9B C10B -6(7) . O2 B1 C9B C14B -180.0(2) . O1 B1 C9B C14B -0.4(4) . C9A B1 C9B C14B 174(8) . C14B C9B C10B C11B 0.0 . B1 C9B C10B C11B -179.4(5) . C9B C10B C11B C12B 0.0 . C10B C11B C12B C13B 0.0 . C10B C11B C12B C15B -179.0(4) . C11B C12B C13B C14B 0.0 . C15B C12B C13B C14B 179.0(4) . C12B C13B C14B C9B 0.0 . C10B C9B C14B C13B 0.0 . B1 C9B C14B C13B 179.4(5) . C11B C12B C15B O3B 1.8(6) . C13B C12B C15B O3B -177.2(4) .